Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological properties

Friction surfacing (FS) is a solid-state additive manufacturing method that uses high-temperature plastic deformation to produce fully dense multilayer samples with a fine-grained microstructure. This study uses the FS process to fabricate composite samples of AA2024-T4 reinforced with 1.5 wt% nano-...

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Main Authors: Milad Abbasi Nahr, Seyyed Ehsan Mirsalehi, Ahmad Papi
Format: Article
Language:English
Published: Elsevier 2025-05-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425012797
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author Milad Abbasi Nahr
Seyyed Ehsan Mirsalehi
Ahmad Papi
author_facet Milad Abbasi Nahr
Seyyed Ehsan Mirsalehi
Ahmad Papi
author_sort Milad Abbasi Nahr
collection DOAJ
description Friction surfacing (FS) is a solid-state additive manufacturing method that uses high-temperature plastic deformation to produce fully dense multilayer samples with a fine-grained microstructure. This study uses the FS process to fabricate composite samples of AA2024-T4 reinforced with 1.5 wt% nano-Al2O3 alongside non-composite counterparts for comparison. This study aims to improve microstructure by examining deposition parameters, including rod rotational speeds (600–1200 rpm), travel speed (70–85 mm/min), and feeding rate (30–45 mm/min), which affect the heat input during FS. Evaluations of the consumable rod and deposition multilayer samples included macro- and microstructural analyses using OM, XRD, and SEM equipped with EDS, along with evaluation of hardness and wear properties. Results demonstrated that successfully produced defect-free multilayer AA2024/Al2O3 nanocomposites with well-bonded layers, uniform Al2O3, and precipitates distribution, fragmented intermetallic compounds, and fine-grained microstructure with an average grain size of 3–10 μm. The FS-produced composites exhibited improved hardness and wear resistance compared to non-composites. Increasing rotational speed widened samples (3.7 mm) and reduced thickness (4.56 mm). The optimal microstructure, achieved at a rotational, traverse and feed speed of 1000 rpm, 80 mm/min, and 40 mm/min, features a grain size of 3.74 ± 1.01 μm, a hardness of 123.75 ± 9.28 HV, and a wear rate of 6.6 × 10−4 mg/N·m. Additionally, of the 14 samples produced, this particular sample showed a hardness increase of 20.5 % and 20.3 %, a grain size reduction of 22.9 % and 17.8 %, and a wear rate decline of 5.7 % and 12.9 % compared to the non-composite counterpart and the highest-performing samples, respectively.
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issn 2238-7854
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spelling doaj-art-bd598689fc034fddb3579ef2dc8566612025-08-20T01:55:30ZengElsevierJournal of Materials Research and Technology2238-78542025-05-01368609863110.1016/j.jmrt.2025.05.124Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological propertiesMilad Abbasi Nahr0Seyyed Ehsan Mirsalehi1Ahmad Papi2Department of Materials and Metallurgical Engineering, Amirkabir University of Technology (Tehran Polytechnic), Tehran, 15875-4413, IranCorresponding author.; Department of Materials and Metallurgical Engineering, Amirkabir University of Technology (Tehran Polytechnic), Tehran, 15875-4413, IranDepartment of Materials and Metallurgical Engineering, Amirkabir University of Technology (Tehran Polytechnic), Tehran, 15875-4413, IranFriction surfacing (FS) is a solid-state additive manufacturing method that uses high-temperature plastic deformation to produce fully dense multilayer samples with a fine-grained microstructure. This study uses the FS process to fabricate composite samples of AA2024-T4 reinforced with 1.5 wt% nano-Al2O3 alongside non-composite counterparts for comparison. This study aims to improve microstructure by examining deposition parameters, including rod rotational speeds (600–1200 rpm), travel speed (70–85 mm/min), and feeding rate (30–45 mm/min), which affect the heat input during FS. Evaluations of the consumable rod and deposition multilayer samples included macro- and microstructural analyses using OM, XRD, and SEM equipped with EDS, along with evaluation of hardness and wear properties. Results demonstrated that successfully produced defect-free multilayer AA2024/Al2O3 nanocomposites with well-bonded layers, uniform Al2O3, and precipitates distribution, fragmented intermetallic compounds, and fine-grained microstructure with an average grain size of 3–10 μm. The FS-produced composites exhibited improved hardness and wear resistance compared to non-composites. Increasing rotational speed widened samples (3.7 mm) and reduced thickness (4.56 mm). The optimal microstructure, achieved at a rotational, traverse and feed speed of 1000 rpm, 80 mm/min, and 40 mm/min, features a grain size of 3.74 ± 1.01 μm, a hardness of 123.75 ± 9.28 HV, and a wear rate of 6.6 × 10−4 mg/N·m. Additionally, of the 14 samples produced, this particular sample showed a hardness increase of 20.5 % and 20.3 %, a grain size reduction of 22.9 % and 17.8 %, and a wear rate decline of 5.7 % and 12.9 % compared to the non-composite counterpart and the highest-performing samples, respectively.http://www.sciencedirect.com/science/article/pii/S2238785425012797Friction surfacing (FS)Additive manufacturing (AM)Multilayer depositionHeat inputAluminum alloy compositesAluminum oxide (Al2O3)
spellingShingle Milad Abbasi Nahr
Seyyed Ehsan Mirsalehi
Ahmad Papi
Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological properties
Journal of Materials Research and Technology
Friction surfacing (FS)
Additive manufacturing (AM)
Multilayer deposition
Heat input
Aluminum alloy composites
Aluminum oxide (Al2O3)
title Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological properties
title_full Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological properties
title_fullStr Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological properties
title_full_unstemmed Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological properties
title_short Additive manufacturing of AA2024/Al2O3 nanocomposites via friction surfacing: Investigating metallurgical, mechanical, and tribological properties
title_sort additive manufacturing of aa2024 al2o3 nanocomposites via friction surfacing investigating metallurgical mechanical and tribological properties
topic Friction surfacing (FS)
Additive manufacturing (AM)
Multilayer deposition
Heat input
Aluminum alloy composites
Aluminum oxide (Al2O3)
url http://www.sciencedirect.com/science/article/pii/S2238785425012797
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AT seyyedehsanmirsalehi additivemanufacturingofaa2024al2o3nanocompositesviafrictionsurfacinginvestigatingmetallurgicalmechanicalandtribologicalproperties
AT ahmadpapi additivemanufacturingofaa2024al2o3nanocompositesviafrictionsurfacinginvestigatingmetallurgicalmechanicalandtribologicalproperties