Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and Analysis

Coal resource extraction and utilization are essential for sustainable development and economic growth. This study integrates a pseudo-triaxial mechanical loading system with low-field nuclear magnetic resonance (NMR) to enable the preliminary visualization of coal’s pore-fracture structure (PFS) un...

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Main Authors: Zelin Liu, Senlin Xie, Yajun Yin, Teng Su
Format: Article
Language:English
Published: MDPI AG 2025-02-01
Series:Fractal and Fractional
Subjects:
Online Access:https://www.mdpi.com/2504-3110/9/2/93
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author Zelin Liu
Senlin Xie
Yajun Yin
Teng Su
author_facet Zelin Liu
Senlin Xie
Yajun Yin
Teng Su
author_sort Zelin Liu
collection DOAJ
description Coal resource extraction and utilization are essential for sustainable development and economic growth. This study integrates a pseudo-triaxial mechanical loading system with low-field nuclear magnetic resonance (NMR) to enable the preliminary visualization of coal’s pore-fracture structure (PFS) under mechanical stress. Pseudo-triaxial and cyclic loading–unloading tests were combined with real-time NMR monitoring to model porosity recovery, pore size evolution, and energy dissipation, while also calculating the fractal dimensions of pores in relation to stress. The results show that during the compaction phase, primary pores are compressed with limited recovery after unloading. In the elastic phase, both adsorption and seepage pores transform significantly, with most recovering post-unloading. After yield stress, new fractures and pores form, and unloading enhances fracture connectivity. Seepage pore porosity shows a negative exponential relationship with axial strain before yielding, and a logarithmic relationship afterward. The fractal dimension of adsorption pores decreases during compaction and increases afterward, while the fractal dimension of seepage pores decreases before yielding and increases post-yielding. These findings provide new insights into the flow patterns of methane in coal seams.
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series Fractal and Fractional
spelling doaj-art-bcfe4776158b47ad8b5d45ec3747e59a2025-08-20T03:12:08ZengMDPI AGFractal and Fractional2504-31102025-02-01929310.3390/fractalfract9020093Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and AnalysisZelin Liu0Senlin Xie1Yajun Yin2Teng Su3Department of Engineering Mechanics, Tsinghua University, Beijing 100084, ChinaCollege of Energy Engineering, Xi’an University of Science and Technology, Xi’an 710054, ChinaDepartment of Engineering Mechanics, Tsinghua University, Beijing 100084, ChinaSchool of Civil and Ocean Engineering, Jiangsu Ocean University, Lianyungang 222005, ChinaCoal resource extraction and utilization are essential for sustainable development and economic growth. This study integrates a pseudo-triaxial mechanical loading system with low-field nuclear magnetic resonance (NMR) to enable the preliminary visualization of coal’s pore-fracture structure (PFS) under mechanical stress. Pseudo-triaxial and cyclic loading–unloading tests were combined with real-time NMR monitoring to model porosity recovery, pore size evolution, and energy dissipation, while also calculating the fractal dimensions of pores in relation to stress. The results show that during the compaction phase, primary pores are compressed with limited recovery after unloading. In the elastic phase, both adsorption and seepage pores transform significantly, with most recovering post-unloading. After yield stress, new fractures and pores form, and unloading enhances fracture connectivity. Seepage pore porosity shows a negative exponential relationship with axial strain before yielding, and a logarithmic relationship afterward. The fractal dimension of adsorption pores decreases during compaction and increases afterward, while the fractal dimension of seepage pores decreases before yielding and increases post-yielding. These findings provide new insights into the flow patterns of methane in coal seams.https://www.mdpi.com/2504-3110/9/2/93triaxial cyclic loading–unloadingpore-fracture structurenuclear magnetic resonance imagingseepagefractal dimension
spellingShingle Zelin Liu
Senlin Xie
Yajun Yin
Teng Su
Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and Analysis
Fractal and Fractional
triaxial cyclic loading–unloading
pore-fracture structure
nuclear magnetic resonance imaging
seepage
fractal dimension
title Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and Analysis
title_full Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and Analysis
title_fullStr Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and Analysis
title_full_unstemmed Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and Analysis
title_short Fractal Characterization and Pore Evolution in Coal Under Tri-Axial Cyclic Loading–Unloading: Insights from Low-Field NMR Imaging and Analysis
title_sort fractal characterization and pore evolution in coal under tri axial cyclic loading unloading insights from low field nmr imaging and analysis
topic triaxial cyclic loading–unloading
pore-fracture structure
nuclear magnetic resonance imaging
seepage
fractal dimension
url https://www.mdpi.com/2504-3110/9/2/93
work_keys_str_mv AT zelinliu fractalcharacterizationandporeevolutionincoalundertriaxialcyclicloadingunloadinginsightsfromlowfieldnmrimagingandanalysis
AT senlinxie fractalcharacterizationandporeevolutionincoalundertriaxialcyclicloadingunloadinginsightsfromlowfieldnmrimagingandanalysis
AT yajunyin fractalcharacterizationandporeevolutionincoalundertriaxialcyclicloadingunloadinginsightsfromlowfieldnmrimagingandanalysis
AT tengsu fractalcharacterizationandporeevolutionincoalundertriaxialcyclicloadingunloadinginsightsfromlowfieldnmrimagingandanalysis