Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere Soils

This study examined the regulatory mechanism of calcium (Ca) amendment on the dynamics of soil organic carbon (SOC) fractions and extracellular enzyme activities, elucidating the role of Ca in soil carbon cycling processes. A field experiment with maize was conducted, comparing treatments of low cal...

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Main Authors: Zhaoquan He, Xue Shang, Xiaoze Jin
Format: Article
Language:English
Published: MDPI AG 2025-07-01
Series:Agronomy
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Online Access:https://www.mdpi.com/2073-4395/15/7/1680
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author Zhaoquan He
Xue Shang
Xiaoze Jin
author_facet Zhaoquan He
Xue Shang
Xiaoze Jin
author_sort Zhaoquan He
collection DOAJ
description This study examined the regulatory mechanism of calcium (Ca) amendment on the dynamics of soil organic carbon (SOC) fractions and extracellular enzyme activities, elucidating the role of Ca in soil carbon cycling processes. A field experiment with maize was conducted, comparing treatments of low calcium (T1), high calcium (T2), and a calcium-free control (CK). Measurements included inter-root SOC fractions—soluble organic carbon (DOC), microbial biomass carbon (MBC), and readily oxidizable organic carbon (ROC)—and the activities of the following extracellular enzymes: β-xylanase, β-glucosidase (β-glu), phenol oxidase (Phox), peroxidase (Pero), phosphatase (Phos), acetylaminoglucosidase (NAG), and urease. The main findings indicated the following: (1) Calcium addition significantly increased SOC content (115.04% and 99.22% higher in T1 and T2, respectively, than CK during the entire reproductive period) and enhanced microbial activity (elevated DOC and MBC). However, SOC decreased by 8.44% (T1) and 16.38% (T2) relative to CK in the late reproductive stage (irrigation–ripening), potentially reflecting microbial utilization (supported by the inverse correlation between SOC and MBC/DOC), and maize carbon reallocation during grain filling. (2) Calcium activated β-glu, Phox, Phos, NAG, and urease (<i>p</i> < 0.05), with pronounced increases in Phox (241.13 IU·L<sup>−1</sup>) and Phos (1126.65 U·L<sup>−1</sup>), indicating enhanced organic matter mineralization and phosphorus availability. (3) Calcium-driven MBC and ROC accumulation was associated with the positive regulation of Phox (path coefficient > 0.8) and the negative regulation of Phos. SOC was co-regulated by β-glu and Phos (R<sup>2</sup> = 0.753). (4) Calcium dynamically optimized the short-term carbon distribution through enzyme activity while promoting long-term sequestration. Our study provides new evidence supporting multi-pathway interactions through which calcium mediates enzyme networks to influence the soil carbon cycle. The findings provide a theoretical foundation for calcium fertilizer management and soil carbon sequestration strategies in agriculture, advancing academic and practical goals for sustainable development and carbon neutrality.
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spelling doaj-art-bcbf3fba3f714a30a928c686294f23352025-08-20T02:45:42ZengMDPI AGAgronomy2073-43952025-07-01157168010.3390/agronomy15071680Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere SoilsZhaoquan He0Xue Shang1Xiaoze Jin2School of Life Sciences, Yan’an University, Yan’an 716000, ChinaSchool of Life Sciences, Yan’an University, Yan’an 716000, ChinaSchool of Life Sciences, Yan’an University, Yan’an 716000, ChinaThis study examined the regulatory mechanism of calcium (Ca) amendment on the dynamics of soil organic carbon (SOC) fractions and extracellular enzyme activities, elucidating the role of Ca in soil carbon cycling processes. A field experiment with maize was conducted, comparing treatments of low calcium (T1), high calcium (T2), and a calcium-free control (CK). Measurements included inter-root SOC fractions—soluble organic carbon (DOC), microbial biomass carbon (MBC), and readily oxidizable organic carbon (ROC)—and the activities of the following extracellular enzymes: β-xylanase, β-glucosidase (β-glu), phenol oxidase (Phox), peroxidase (Pero), phosphatase (Phos), acetylaminoglucosidase (NAG), and urease. The main findings indicated the following: (1) Calcium addition significantly increased SOC content (115.04% and 99.22% higher in T1 and T2, respectively, than CK during the entire reproductive period) and enhanced microbial activity (elevated DOC and MBC). However, SOC decreased by 8.44% (T1) and 16.38% (T2) relative to CK in the late reproductive stage (irrigation–ripening), potentially reflecting microbial utilization (supported by the inverse correlation between SOC and MBC/DOC), and maize carbon reallocation during grain filling. (2) Calcium activated β-glu, Phox, Phos, NAG, and urease (<i>p</i> < 0.05), with pronounced increases in Phox (241.13 IU·L<sup>−1</sup>) and Phos (1126.65 U·L<sup>−1</sup>), indicating enhanced organic matter mineralization and phosphorus availability. (3) Calcium-driven MBC and ROC accumulation was associated with the positive regulation of Phox (path coefficient > 0.8) and the negative regulation of Phos. SOC was co-regulated by β-glu and Phos (R<sup>2</sup> = 0.753). (4) Calcium dynamically optimized the short-term carbon distribution through enzyme activity while promoting long-term sequestration. Our study provides new evidence supporting multi-pathway interactions through which calcium mediates enzyme networks to influence the soil carbon cycle. The findings provide a theoretical foundation for calcium fertilizer management and soil carbon sequestration strategies in agriculture, advancing academic and practical goals for sustainable development and carbon neutrality.https://www.mdpi.com/2073-4395/15/7/1680Ca additionsoil organic carbonsoil extracellular enzymesmaizerhizosphere soils
spellingShingle Zhaoquan He
Xue Shang
Xiaoze Jin
Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere Soils
Agronomy
Ca addition
soil organic carbon
soil extracellular enzymes
maize
rhizosphere soils
title Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere Soils
title_full Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere Soils
title_fullStr Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere Soils
title_full_unstemmed Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere Soils
title_short Effect of Calcium Addition on Extracellular Enzymes and Soil Organic Carbon in Maize Rhizosphere Soils
title_sort effect of calcium addition on extracellular enzymes and soil organic carbon in maize rhizosphere soils
topic Ca addition
soil organic carbon
soil extracellular enzymes
maize
rhizosphere soils
url https://www.mdpi.com/2073-4395/15/7/1680
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AT xiaozejin effectofcalciumadditiononextracellularenzymesandsoilorganiccarboninmaizerhizospheresoils