Spectrophometric Determination of Nelfinavir Mesylate

Two new simple, sensitive, rapid and economical Spectrophotometric Methods (A and B) have been developed for the determination of Nelfinavir Mesylate in pharmaceutical bulk and tablet dosage form. The method A is based on the reaction of Nelfinavir with ferric chloride, potassium ferricyanide and hy...

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Main Authors: K. Vanitha Prakash, Jangala Venkateswara Rao
Format: Article
Language:English
Published: Wiley 2006-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2006/160909
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author K. Vanitha Prakash
Jangala Venkateswara Rao
author_facet K. Vanitha Prakash
Jangala Venkateswara Rao
author_sort K. Vanitha Prakash
collection DOAJ
description Two new simple, sensitive, rapid and economical Spectrophotometric Methods (A and B) have been developed for the determination of Nelfinavir Mesylate in pharmaceutical bulk and tablet dosage form. The method A is based on the reaction of Nelfinavir with ferric chloride, potassium ferricyanide and hydrochloric acid to form a bluish green colored chromogen. The Method B is based on the formation of blood red colored chromogen with Ferric chloride and 1,10-phenanthroline. The absorbances of the chromogen were measured at their respective wavelength of maximum absorbance against the corresponding reagent blank. The proposed methods have been successfully applied to the analysis of the bulk drug and its tablet dosage form. The methods have been statistically evaluated and were found to be precise and accurate.
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spelling doaj-art-bb5f677294d74452a8499aa5c5d6411e2025-08-20T03:23:07ZengWileyE-Journal of Chemistry0973-49452090-98102006-01-0132788210.1155/2006/160909Spectrophometric Determination of Nelfinavir MesylateK. Vanitha Prakash0Jangala Venkateswara Rao1Department of Pharmaceutical Chemistry, Sultan-Ul-Uloom College of Pharmacy, Mount Pleasant, Road No. 3, Banjara Hills, Hyderabad-500 034, IndiaDepartment of Pharmaceutical Chemistry, Sultan-Ul-Uloom College of Pharmacy, Mount Pleasant, Road No. 3, Banjara Hills, Hyderabad-500 034, IndiaTwo new simple, sensitive, rapid and economical Spectrophotometric Methods (A and B) have been developed for the determination of Nelfinavir Mesylate in pharmaceutical bulk and tablet dosage form. The method A is based on the reaction of Nelfinavir with ferric chloride, potassium ferricyanide and hydrochloric acid to form a bluish green colored chromogen. The Method B is based on the formation of blood red colored chromogen with Ferric chloride and 1,10-phenanthroline. The absorbances of the chromogen were measured at their respective wavelength of maximum absorbance against the corresponding reagent blank. The proposed methods have been successfully applied to the analysis of the bulk drug and its tablet dosage form. The methods have been statistically evaluated and were found to be precise and accurate.http://dx.doi.org/10.1155/2006/160909
spellingShingle K. Vanitha Prakash
Jangala Venkateswara Rao
Spectrophometric Determination of Nelfinavir Mesylate
E-Journal of Chemistry
title Spectrophometric Determination of Nelfinavir Mesylate
title_full Spectrophometric Determination of Nelfinavir Mesylate
title_fullStr Spectrophometric Determination of Nelfinavir Mesylate
title_full_unstemmed Spectrophometric Determination of Nelfinavir Mesylate
title_short Spectrophometric Determination of Nelfinavir Mesylate
title_sort spectrophometric determination of nelfinavir mesylate
url http://dx.doi.org/10.1155/2006/160909
work_keys_str_mv AT kvanithaprakash spectrophometricdeterminationofnelfinavirmesylate
AT jangalavenkateswararao spectrophometricdeterminationofnelfinavirmesylate