Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel Shell

Microwave pyrolysis is a potential for producing alternative fuel from biomass, such as palm kernel shell (PKS). However, the resulting microwave pyrolytic oil (bio-oil) was highly acidic and has low calorific value and therefore must undergo additional process to improve the physicochemical propert...

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Main Authors: Sharifah Mona Abdul Aziz, Rafeah Wahi, Zainab Ngaini, Sinin Hamdan, Syamila Aimi Yahaya
Format: Article
Language:English
Published: Wiley 2017-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2017/8359238
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author Sharifah Mona Abdul Aziz
Rafeah Wahi
Zainab Ngaini
Sinin Hamdan
Syamila Aimi Yahaya
author_facet Sharifah Mona Abdul Aziz
Rafeah Wahi
Zainab Ngaini
Sinin Hamdan
Syamila Aimi Yahaya
author_sort Sharifah Mona Abdul Aziz
collection DOAJ
description Microwave pyrolysis is a potential for producing alternative fuel from biomass, such as palm kernel shell (PKS). However, the resulting microwave pyrolytic oil (bio-oil) was highly acidic and has low calorific value and therefore must undergo additional process to improve the physicochemical properties. In this study, attempt was made to improve the pH and calorific value of bio-oil produced from PKS via esterification process. The effect of esterification with ethanol in the presence of sulphuric acid as a catalyst on selected biodiesel qualities was also investigated. The esterification process has successfully improved the pH value from 3.37 to 5.09–5.12 and the calorific value was increased from 27.19 to 34.78–41.52 MJ/kg. Conclusively, the EO has comparatively better properties in terms of its smell, pH, calorific value, and absence of environmentally undesirable compounds. However, future works should include ASTM 6751 specifications tests for biodiesel to evaluate the bio-oil’s suitability for commercial use.
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institution DOAJ
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language English
publishDate 2017-01-01
publisher Wiley
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series Journal of Chemistry
spelling doaj-art-b98d37dfdfe34a5696721e960c501fc82025-08-20T03:23:14ZengWileyJournal of Chemistry2090-90632090-90712017-01-01201710.1155/2017/83592388359238Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel ShellSharifah Mona Abdul Aziz0Rafeah Wahi1Zainab Ngaini2Sinin Hamdan3Syamila Aimi Yahaya4Centre of Pre-University Studies, Universiti Malaysia Sarawak, 94300 Kota Samarahan, Sarawak, MalaysiaDepartment of Chemistry, Faculty of Resource Science and Technology, Universiti Malaysia Sarawak, 94300 Kota Samarahan, Sarawak, MalaysiaDepartment of Chemistry, Faculty of Resource Science and Technology, Universiti Malaysia Sarawak, 94300 Kota Samarahan, Sarawak, MalaysiaDepartment of Mechanical and Manufacturing Engineering, Faculty of Engineering, Universiti Malaysia Sarawak, 94300 Kota Samarahan, Sarawak, MalaysiaDepartment of Chemistry, Faculty of Resource Science and Technology, Universiti Malaysia Sarawak, 94300 Kota Samarahan, Sarawak, MalaysiaMicrowave pyrolysis is a potential for producing alternative fuel from biomass, such as palm kernel shell (PKS). However, the resulting microwave pyrolytic oil (bio-oil) was highly acidic and has low calorific value and therefore must undergo additional process to improve the physicochemical properties. In this study, attempt was made to improve the pH and calorific value of bio-oil produced from PKS via esterification process. The effect of esterification with ethanol in the presence of sulphuric acid as a catalyst on selected biodiesel qualities was also investigated. The esterification process has successfully improved the pH value from 3.37 to 5.09–5.12 and the calorific value was increased from 27.19 to 34.78–41.52 MJ/kg. Conclusively, the EO has comparatively better properties in terms of its smell, pH, calorific value, and absence of environmentally undesirable compounds. However, future works should include ASTM 6751 specifications tests for biodiesel to evaluate the bio-oil’s suitability for commercial use.http://dx.doi.org/10.1155/2017/8359238
spellingShingle Sharifah Mona Abdul Aziz
Rafeah Wahi
Zainab Ngaini
Sinin Hamdan
Syamila Aimi Yahaya
Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel Shell
Journal of Chemistry
title Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel Shell
title_full Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel Shell
title_fullStr Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel Shell
title_full_unstemmed Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel Shell
title_short Esterification of Microwave Pyrolytic Oil from Palm Oil Kernel Shell
title_sort esterification of microwave pyrolytic oil from palm oil kernel shell
url http://dx.doi.org/10.1155/2017/8359238
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AT rafeahwahi esterificationofmicrowavepyrolyticoilfrompalmoilkernelshell
AT zainabngaini esterificationofmicrowavepyrolyticoilfrompalmoilkernelshell
AT sininhamdan esterificationofmicrowavepyrolyticoilfrompalmoilkernelshell
AT syamilaaimiyahaya esterificationofmicrowavepyrolyticoilfrompalmoilkernelshell