Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbon

Abstract Here, we report the fabrication of flake-like rice husk-derived chemically activated graphitic carbon (RCAGC) for metal-free degradation of MO under visible light conditions. RCAGC has been synthesised from biomass feedstock rice husk and characterized by Fourier transform infrared spectros...

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Main Authors: Kumkum Priyadarshini Sahu, Subhash Banerjee
Format: Article
Language:English
Published: Springer 2025-07-01
Series:Discover Materials
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Online Access:https://doi.org/10.1007/s43939-025-00325-4
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author Kumkum Priyadarshini Sahu
Subhash Banerjee
author_facet Kumkum Priyadarshini Sahu
Subhash Banerjee
author_sort Kumkum Priyadarshini Sahu
collection DOAJ
description Abstract Here, we report the fabrication of flake-like rice husk-derived chemically activated graphitic carbon (RCAGC) for metal-free degradation of MO under visible light conditions. RCAGC has been synthesised from biomass feedstock rice husk and characterized by Fourier transform infrared spectroscopy, powder X-ray diffraction, and field emission scanning electron microscopy. Flake-like RCAGC demonstrated remarkable efficiency in the degradation of MO, and 100% degradation of MO was achieved within 9 min of illumination under visible light. Moreover, real-time analysis of RCAGC-catalysed dye degradation was performed by the flow method using a column packed with an alternate layer of RCAGC and silica, followed by passing a solution of MO (20 ppm) through the column. A completely degraded colourless eluent was obtained, demonstrating the practical application of RCAGC material for the remediation of organic dyes in domestic water. The role of reactive species in the degradation was established by scavenger test, and it was observed that electron plays a crucial role in the degradation of MO under visible light.
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spelling doaj-art-b97335758402489fba655f5ed35a0d8a2025-08-20T03:46:24ZengSpringerDiscover Materials2730-77272025-07-015111310.1007/s43939-025-00325-4Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbonKumkum Priyadarshini Sahu0Subhash Banerjee1Department of Chemistry, Guru Ghasidas VishwavidyalayaDepartment of Chemistry, Guru Ghasidas VishwavidyalayaAbstract Here, we report the fabrication of flake-like rice husk-derived chemically activated graphitic carbon (RCAGC) for metal-free degradation of MO under visible light conditions. RCAGC has been synthesised from biomass feedstock rice husk and characterized by Fourier transform infrared spectroscopy, powder X-ray diffraction, and field emission scanning electron microscopy. Flake-like RCAGC demonstrated remarkable efficiency in the degradation of MO, and 100% degradation of MO was achieved within 9 min of illumination under visible light. Moreover, real-time analysis of RCAGC-catalysed dye degradation was performed by the flow method using a column packed with an alternate layer of RCAGC and silica, followed by passing a solution of MO (20 ppm) through the column. A completely degraded colourless eluent was obtained, demonstrating the practical application of RCAGC material for the remediation of organic dyes in domestic water. The role of reactive species in the degradation was established by scavenger test, and it was observed that electron plays a crucial role in the degradation of MO under visible light.https://doi.org/10.1007/s43939-025-00325-4Chemically activated graphitic carbonBiomass feedstockMethyl orange, photocatalytic dye degradationVisible light
spellingShingle Kumkum Priyadarshini Sahu
Subhash Banerjee
Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbon
Discover Materials
Chemically activated graphitic carbon
Biomass feedstock
Methyl orange, photocatalytic dye degradation
Visible light
title Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbon
title_full Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbon
title_fullStr Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbon
title_full_unstemmed Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbon
title_short Metal-free degradation of methyl orange: unprecedented catalytic efficiency of rice husk-derived graphitic carbon
title_sort metal free degradation of methyl orange unprecedented catalytic efficiency of rice husk derived graphitic carbon
topic Chemically activated graphitic carbon
Biomass feedstock
Methyl orange, photocatalytic dye degradation
Visible light
url https://doi.org/10.1007/s43939-025-00325-4
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AT subhashbanerjee metalfreedegradationofmethylorangeunprecedentedcatalyticefficiencyofricehuskderivedgraphiticcarbon