Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 Nanoparticles
Plant extracts have been widely explored as a safer alternative to conventional procedures for the manufacture of metal oxide nanoparticles. The present research concentrated on the synthesis and characterization of Titanium dioxide nanoparticles (TiO2NPs) using an environmentally friendly green sy...
Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
University of Baghdad, College of Science for Women
2024-05-01
|
| Series: | مجلة بغداد للعلوم |
| Subjects: | |
| Online Access: | https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/8089 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| _version_ | 1849248915293995008 |
|---|---|
| author | Hind Fadhil Oleiwi Aseel J. Rahma Siham I. Salih Ammar A. Beddai |
| author_facet | Hind Fadhil Oleiwi Aseel J. Rahma Siham I. Salih Ammar A. Beddai |
| author_sort | Hind Fadhil Oleiwi |
| collection | DOAJ |
| description |
Plant extracts have been widely explored as a safer alternative to conventional procedures for the manufacture of metal oxide nanoparticles. The present research concentrated on the synthesis and characterization of Titanium dioxide nanoparticles (TiO2NPs) using an environmentally friendly green synthesis approach (orange peel extract) compared with another technique (Sol-Gel method) at room temperature. The TiO2 nanoparticles were analyzed using an X-ray Diffraction (XRD) to determine the polycrystalline with Tetragonal structure anatase phase and average crystallite size 30.2 nm and 24.2nm of the sample prepared from Sol-gel and green methods respectively. FTIR spectroscopy was used to determine the functional groups of TiO2 nanoparticles and their bonding nature. UV-Vis for optical properties shows the band gap energy of 2.85 eV and 3 eV for TiO2 nanoparticles were prepared using sol-gel and green methods respectively. FESEM analysis identified the morphology of the surface of TiO2 nanoparticles with the diameters of nanoparticles in the range of 60-80 nm and 75-85 nm were prepared via sol-gel and green methods respectively.
|
| format | Article |
| id | doaj-art-b82bffec0d7d4b40ac26b1f06a4e14af |
| institution | Kabale University |
| issn | 2078-8665 2411-7986 |
| language | English |
| publishDate | 2024-05-01 |
| publisher | University of Baghdad, College of Science for Women |
| record_format | Article |
| series | مجلة بغداد للعلوم |
| spelling | doaj-art-b82bffec0d7d4b40ac26b1f06a4e14af2025-08-20T03:57:43ZengUniversity of Baghdad, College of Science for Womenمجلة بغداد للعلوم2078-86652411-79862024-05-0121510.21123/bsj.2023.8089Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 NanoparticlesHind Fadhil Oleiwi 0Aseel J. Rahma 1https://orcid.org/0000-0001-6138-8342Siham I. Salih 2https://orcid.org/0000-0002-1901-1530Ammar A. Beddai3https://orcid.org/0000-0002-4630-9746Department of Physics, College of Science for Women, University of Baghdad, Fuel and Energy Department, Engineering Technical Collage, Middle Technical University, Baghdad, Iraq. College of Engineering, Mustansiriyah University, Baghdad, Iraq. Middle Technical University, Baghdad, Iraq. Plant extracts have been widely explored as a safer alternative to conventional procedures for the manufacture of metal oxide nanoparticles. The present research concentrated on the synthesis and characterization of Titanium dioxide nanoparticles (TiO2NPs) using an environmentally friendly green synthesis approach (orange peel extract) compared with another technique (Sol-Gel method) at room temperature. The TiO2 nanoparticles were analyzed using an X-ray Diffraction (XRD) to determine the polycrystalline with Tetragonal structure anatase phase and average crystallite size 30.2 nm and 24.2nm of the sample prepared from Sol-gel and green methods respectively. FTIR spectroscopy was used to determine the functional groups of TiO2 nanoparticles and their bonding nature. UV-Vis for optical properties shows the band gap energy of 2.85 eV and 3 eV for TiO2 nanoparticles were prepared using sol-gel and green methods respectively. FESEM analysis identified the morphology of the surface of TiO2 nanoparticles with the diameters of nanoparticles in the range of 60-80 nm and 75-85 nm were prepared via sol-gel and green methods respectively. https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/8089FTIR, Green syntheses, Nanoparticles, Orange peel extract, Sol-Gel, TiO2 |
| spellingShingle | Hind Fadhil Oleiwi Aseel J. Rahma Siham I. Salih Ammar A. Beddai Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 Nanoparticles مجلة بغداد للعلوم FTIR, Green syntheses, Nanoparticles, Orange peel extract, Sol-Gel, TiO2 |
| title | Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 Nanoparticles |
| title_full | Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 Nanoparticles |
| title_fullStr | Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 Nanoparticles |
| title_full_unstemmed | Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 Nanoparticles |
| title_short | Comparative Study of Sol-Gel and Green Synthesis Technique Using Orange Peel Extract to Prepare TiO2 Nanoparticles |
| title_sort | comparative study of sol gel and green synthesis technique using orange peel extract to prepare tio2 nanoparticles |
| topic | FTIR, Green syntheses, Nanoparticles, Orange peel extract, Sol-Gel, TiO2 |
| url | https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/8089 |
| work_keys_str_mv | AT hindfadhiloleiwi comparativestudyofsolgelandgreensynthesistechniqueusingorangepeelextracttopreparetio2nanoparticles AT aseeljrahma comparativestudyofsolgelandgreensynthesistechniqueusingorangepeelextracttopreparetio2nanoparticles AT sihamisalih comparativestudyofsolgelandgreensynthesistechniqueusingorangepeelextracttopreparetio2nanoparticles AT ammarabeddai comparativestudyofsolgelandgreensynthesistechniqueusingorangepeelextracttopreparetio2nanoparticles |