Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles
1,2,4-Trisubstituted pyrroles were synthesized with an original one-pot domino allylic amination/palladium-catalysed Sonogashira cross-coupling and heterocyclisation process. 1H and 13C NMR spectra were assigned for twelve new compounds containing different substituents in positions 1 and 2, and a c...
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| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Wiley
2013-01-01
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| Series: | Journal of Spectroscopy |
| Online Access: | http://dx.doi.org/10.1155/2013/146541 |
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| author | Elsa Anselmi Mohamed Abarbri Alain Duchêne Sandrine Lamandé-Langle Jérôme Thibonnet |
| author_facet | Elsa Anselmi Mohamed Abarbri Alain Duchêne Sandrine Lamandé-Langle Jérôme Thibonnet |
| author_sort | Elsa Anselmi |
| collection | DOAJ |
| description | 1,2,4-Trisubstituted pyrroles were synthesized with an original one-pot domino allylic amination/palladium-catalysed Sonogashira cross-coupling and heterocyclisation process. 1H and 13C NMR spectra were assigned for twelve new compounds containing different substituents in positions 1 and 2, and a carboxylic acid or ester group in position 4. Each assignment was based on the combination of one, and two-dimensional experiments (APT, COSY, HMBC). |
| format | Article |
| id | doaj-art-b682240dd3da49c0984583ee56f5a59f |
| institution | Kabale University |
| issn | 2314-4920 2314-4939 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Spectroscopy |
| spelling | doaj-art-b682240dd3da49c0984583ee56f5a59f2025-02-03T06:12:18ZengWileyJournal of Spectroscopy2314-49202314-49392013-01-01201310.1155/2013/146541146541Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted PyrrolesElsa Anselmi0Mohamed Abarbri1Alain Duchêne2Sandrine Lamandé-Langle3Jérôme Thibonnet4Equipe “Recherche et Innovation en Chimie Médicinale”, Laboratoire d’Infectiologie et Santé Publique (UMR UFR/INRA 1282), Faculté des Sciences et Techniques, Université François Rabelais, Parc de Grandmont, 37200 Tours, FranceEquipe “Recherche et Innovation en Chimie Médicinale”, Laboratoire d’Infectiologie et Santé Publique (UMR UFR/INRA 1282), Faculté des Sciences et Techniques, Université François Rabelais, Parc de Grandmont, 37200 Tours, FranceEquipe “Recherche et Innovation en Chimie Médicinale”, Laboratoire d’Infectiologie et Santé Publique (UMR UFR/INRA 1282), Faculté des Sciences et Techniques, Université François Rabelais, Parc de Grandmont, 37200 Tours, FranceGroupe S.U.C.R.E.S-UMR 7565, Nancy Université-CNRS, BP 70239, 54506 Nancy Vandoeuvre, FranceEquipe “Recherche et Innovation en Chimie Médicinale”, Laboratoire d’Infectiologie et Santé Publique (UMR UFR/INRA 1282), Faculté des Sciences et Techniques, Université François Rabelais, Parc de Grandmont, 37200 Tours, France1,2,4-Trisubstituted pyrroles were synthesized with an original one-pot domino allylic amination/palladium-catalysed Sonogashira cross-coupling and heterocyclisation process. 1H and 13C NMR spectra were assigned for twelve new compounds containing different substituents in positions 1 and 2, and a carboxylic acid or ester group in position 4. Each assignment was based on the combination of one, and two-dimensional experiments (APT, COSY, HMBC).http://dx.doi.org/10.1155/2013/146541 |
| spellingShingle | Elsa Anselmi Mohamed Abarbri Alain Duchêne Sandrine Lamandé-Langle Jérôme Thibonnet Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles Journal of Spectroscopy |
| title | Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles |
| title_full | Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles |
| title_fullStr | Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles |
| title_full_unstemmed | Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles |
| title_short | Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles |
| title_sort | complete assignment of h1 and c13 nmr spectra of 1 2 4 trisubstituted pyrroles |
| url | http://dx.doi.org/10.1155/2013/146541 |
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