Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membrane

In this study, graphene oxide (GO) nanoparticles were synthesized from a graphite precursor using a simplified Hummer method, and their surfaces were functionalized with chitosan to improve their dispersion and compatibility with the polymer matrix. The functionalized nanoparticles were then incorpo...

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Main Authors: Iman Khonsha, kobra salehi
Format: Article
Language:English
Published: Iranian Research Organization for Science and Technology (IROST) 2025-07-01
Series:Advances in Environmental Technology
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Online Access:https://aet.irost.ir/article_1540_4f46fa3a106f1390b64d89d4952a5800.pdf
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author Iman Khonsha
kobra salehi
author_facet Iman Khonsha
kobra salehi
author_sort Iman Khonsha
collection DOAJ
description In this study, graphene oxide (GO) nanoparticles were synthesized from a graphite precursor using a simplified Hummer method, and their surfaces were functionalized with chitosan to improve their dispersion and compatibility with the polymer matrix. The functionalized nanoparticles were then incorporated into polyethersulphone (PES) membranes to enhance their properties and provide mixed-matrix membranes. For the fabrication of the polyethersulfone membranes and their performance, an experimental design was performed using Minitab 17 software, applying the Taguchi method with an L9 orthogonal array. The parameters influencing membrane performance, including the polymer and GO concentrations in the membrane casting solution and operating pressure during the separation process, were selected at three levels. The results showed that increasing the polymer concentration enhanced Cu removal but reduced the permeate flux, whereas higher pressure increased the flux but decreased the separation efficiency. In addition, contour plots representing the permeate flux and Cu removal% as a function of the polymer concentration and the operating pressure indicated that the maximum Cu removal (> 70 wt. %) occurred within the pressure range of 6 to 6.2 bar and polymer concentration of 18 to 20 wt.% in the casting solution.
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id doaj-art-b5dc67f24ffe449c86464f912e943bce
institution Kabale University
issn 2476-6674
2476-4779
language English
publishDate 2025-07-01
publisher Iranian Research Organization for Science and Technology (IROST)
record_format Article
series Advances in Environmental Technology
spelling doaj-art-b5dc67f24ffe449c86464f912e943bce2025-08-20T03:26:57ZengIranian Research Organization for Science and Technology (IROST)Advances in Environmental Technology2476-66742476-47792025-07-0111332934010.22104/aet.2025.7217.19871540Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membraneIman Khonsha0kobra salehi1Department of Chemical Engineering, Shiraz Branch, Islamic Azad University, Shiraz, Fars, Iran;Department of Chemical Engineering, Darab Branch, Islamic Azad University, Darab, Fars, Iran;In this study, graphene oxide (GO) nanoparticles were synthesized from a graphite precursor using a simplified Hummer method, and their surfaces were functionalized with chitosan to improve their dispersion and compatibility with the polymer matrix. The functionalized nanoparticles were then incorporated into polyethersulphone (PES) membranes to enhance their properties and provide mixed-matrix membranes. For the fabrication of the polyethersulfone membranes and their performance, an experimental design was performed using Minitab 17 software, applying the Taguchi method with an L9 orthogonal array. The parameters influencing membrane performance, including the polymer and GO concentrations in the membrane casting solution and operating pressure during the separation process, were selected at three levels. The results showed that increasing the polymer concentration enhanced Cu removal but reduced the permeate flux, whereas higher pressure increased the flux but decreased the separation efficiency. In addition, contour plots representing the permeate flux and Cu removal% as a function of the polymer concentration and the operating pressure indicated that the maximum Cu removal (> 70 wt. %) occurred within the pressure range of 6 to 6.2 bar and polymer concentration of 18 to 20 wt.% in the casting solution.https://aet.irost.ir/article_1540_4f46fa3a106f1390b64d89d4952a5800.pdfgraphene oxidechitosanpolyethersulfone (pes) membranemixed matrix membrane
spellingShingle Iman Khonsha
kobra salehi
Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membrane
Advances in Environmental Technology
graphene oxide
chitosan
polyethersulfone (pes) membrane
mixed matrix membrane
title Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membrane
title_full Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membrane
title_fullStr Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membrane
title_full_unstemmed Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membrane
title_short Cu removal from wastewater using a polyethersulfone- graphene oxide nanoparticles functionalized with chitosan membrane
title_sort cu removal from wastewater using a polyethersulfone graphene oxide nanoparticles functionalized with chitosan membrane
topic graphene oxide
chitosan
polyethersulfone (pes) membrane
mixed matrix membrane
url https://aet.irost.ir/article_1540_4f46fa3a106f1390b64d89d4952a5800.pdf
work_keys_str_mv AT imankhonsha curemovalfromwastewaterusingapolyethersulfonegrapheneoxidenanoparticlesfunctionalizedwithchitosanmembrane
AT kobrasalehi curemovalfromwastewaterusingapolyethersulfonegrapheneoxidenanoparticlesfunctionalizedwithchitosanmembrane