Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.

This study systematically investigated the effects of modified ultrafine fly ash, ultrafine silica fume, nano-SiO2, and polycarboxylate superplasticizer on the performance of cement-based grouting materials. Using a five-level orthogonal experimental, the optimal mix ratio was determined: 5.00 wt.%...

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Main Authors: Yijiang Zong, Dong Zhu, Liang Yue, Xiangling Tao, Min Chen
Format: Article
Language:English
Published: Public Library of Science (PLoS) 2025-01-01
Series:PLoS ONE
Online Access:https://doi.org/10.1371/journal.pone.0327032
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author Yijiang Zong
Dong Zhu
Liang Yue
Xiangling Tao
Min Chen
author_facet Yijiang Zong
Dong Zhu
Liang Yue
Xiangling Tao
Min Chen
author_sort Yijiang Zong
collection DOAJ
description This study systematically investigated the effects of modified ultrafine fly ash, ultrafine silica fume, nano-SiO2, and polycarboxylate superplasticizer on the performance of cement-based grouting materials. Using a five-level orthogonal experimental, the optimal mix ratio was determined: 5.00 wt.% modified ultrafine fly ash, 10.00 wt.% ultrafine silica fume, 9.00 wt.% nano-SiO2, and 0.05 wt.% polycarboxylate superplasticizer. This formulation enabled the preparation of a cement-based grouting material with high-flowability and ultra-early-strength (HFUES) characteristics. Experimental results demonstrated that, compared to ordinary silicate grouting materials, the HFUES grouting material significantly enhanced the reinforcement of fractured sandstone. The reinforced specimens exhibited an average 67.42% increment in tensile strength, 123.17% increment in the uniaxial compressive strength, and 94.00% increment in elastic modulus compared to intact specimens. Microstructural analysis revealed that the grouting material was uniformly distributed within the sandstone matrix, forming a dense interfacial bond and generating a substantial amount of fibrous network-like hydration products. The volume fraction of the consolidated matrix was 1.33-1.47 times that of ordinary silicate grouting materials, while the fracture volume fraction was only 0.36-0.73 times. The study demonstrates that the HFUES grouting material exhibits excellent mechanical properties and interfacial bonding characteristics, significantly improving the reinforcement effectiveness of fractured sandstone.
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spelling doaj-art-b509460b95fc49fca34fabfff0fab2df2025-08-20T03:27:56ZengPublic Library of Science (PLoS)PLoS ONE1932-62032025-01-01207e032703210.1371/journal.pone.0327032Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.Yijiang ZongDong ZhuLiang YueXiangling TaoMin ChenThis study systematically investigated the effects of modified ultrafine fly ash, ultrafine silica fume, nano-SiO2, and polycarboxylate superplasticizer on the performance of cement-based grouting materials. Using a five-level orthogonal experimental, the optimal mix ratio was determined: 5.00 wt.% modified ultrafine fly ash, 10.00 wt.% ultrafine silica fume, 9.00 wt.% nano-SiO2, and 0.05 wt.% polycarboxylate superplasticizer. This formulation enabled the preparation of a cement-based grouting material with high-flowability and ultra-early-strength (HFUES) characteristics. Experimental results demonstrated that, compared to ordinary silicate grouting materials, the HFUES grouting material significantly enhanced the reinforcement of fractured sandstone. The reinforced specimens exhibited an average 67.42% increment in tensile strength, 123.17% increment in the uniaxial compressive strength, and 94.00% increment in elastic modulus compared to intact specimens. Microstructural analysis revealed that the grouting material was uniformly distributed within the sandstone matrix, forming a dense interfacial bond and generating a substantial amount of fibrous network-like hydration products. The volume fraction of the consolidated matrix was 1.33-1.47 times that of ordinary silicate grouting materials, while the fracture volume fraction was only 0.36-0.73 times. The study demonstrates that the HFUES grouting material exhibits excellent mechanical properties and interfacial bonding characteristics, significantly improving the reinforcement effectiveness of fractured sandstone.https://doi.org/10.1371/journal.pone.0327032
spellingShingle Yijiang Zong
Dong Zhu
Liang Yue
Xiangling Tao
Min Chen
Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.
PLoS ONE
title Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.
title_full Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.
title_fullStr Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.
title_full_unstemmed Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.
title_short Preparation of high-flowability ultra-early-strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone.
title_sort preparation of high flowability ultra early strength grouting material and investigation of its mechanical properties in reinforcing fractured sandstone
url https://doi.org/10.1371/journal.pone.0327032
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AT liangyue preparationofhighflowabilityultraearlystrengthgroutingmaterialandinvestigationofitsmechanicalpropertiesinreinforcingfracturedsandstone
AT xianglingtao preparationofhighflowabilityultraearlystrengthgroutingmaterialandinvestigationofitsmechanicalpropertiesinreinforcingfracturedsandstone
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