TiO2 paste for DSSC photoanode: preparation and optimization of application method

We propose a simple method of TiO2 paste preparation from titania powder (Degussa) and organic binders (terpineol, ethyl cellulose) for making a continuous photoactive layer of a dye-sensitized solar cell (DSSC). The prepared paste was characterized by using thermogravimetric and X-ray diffraction m...

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Main Authors: I. O. Selyanin, A. S. Steparuk, R. A. Irgashev, A. V. Mekhaev, G. L. Rusinov, A. S. Vorokh
Format: Article
Language:English
Published: Ural Federal University 2020-10-01
Series:Chimica Techno Acta
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Online Access:https://chimicatechnoacta.ru/article/view/4420
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author I. O. Selyanin
A. S. Steparuk
R. A. Irgashev
A. V. Mekhaev
G. L. Rusinov
A. S. Vorokh
author_facet I. O. Selyanin
A. S. Steparuk
R. A. Irgashev
A. V. Mekhaev
G. L. Rusinov
A. S. Vorokh
author_sort I. O. Selyanin
collection DOAJ
description We propose a simple method of TiO2 paste preparation from titania powder (Degussa) and organic binders (terpineol, ethyl cellulose) for making a continuous photoactive layer of a dye-sensitized solar cell (DSSC). The prepared paste was characterized by using thermogravimetric and X-ray diffraction methods for comparison with commercial paste (Solaronix). The TiO2 layer parameters for applying and annealing were optimized by varying the layer thickness and using different masks. The surface morphology of annealed layers was controlled by optical microscopy. Before TiO2 paste applying and after annealing, the conductive glass (fluorine-tin oxide – FTO) was treated by TiCl4 hydrochloric acid solution. The structure of DSSCs were composed FTO-glass / TiO2 layer sensitized Ruthenium complex (N719 dye)/ iodide-based electrolyte / Pt counter electrode/ FTO glass. The DSSC photovoltaic characteristics were measured under AM 1.5G irradiation and demonstrated to be close to those of photoanodes based on the prepared and commercial pastes.
format Article
id doaj-art-b4640102a1174bfc9ed1337fad7e193f
institution Kabale University
issn 2411-1414
language English
publishDate 2020-10-01
publisher Ural Federal University
record_format Article
series Chimica Techno Acta
spelling doaj-art-b4640102a1174bfc9ed1337fad7e193f2025-08-20T03:24:34ZengUral Federal UniversityChimica Techno Acta2411-14142020-10-017414014910.15826/chimtech.2020.7.4.013662TiO2 paste for DSSC photoanode: preparation and optimization of application methodI. O. Selyanin0A. S. Steparuk1R. A. Irgashev2A. V. Mekhaev3G. L. Rusinov4A. S. Vorokh5Institute of Solid State Chemistry UB RAS, Ekaterinburg; Ural Federal University, EkaterinburgPostovsky Institute of Organic Synthesis, EkaterinburgUral Federal University, Ekaterinburg; Postovsky Institute of Organic Synthesis, EkaterinburgPostovsky Institute of Organic Synthesis, EkaterinburgUral Federal University, Ekaterinburg; Postovsky Institute of Organic Synthesis, EkaterinburgInstitute of Solid State Chemistry UB RAS, Ekaterinburg; Ural Federal University, EkaterinburgWe propose a simple method of TiO2 paste preparation from titania powder (Degussa) and organic binders (terpineol, ethyl cellulose) for making a continuous photoactive layer of a dye-sensitized solar cell (DSSC). The prepared paste was characterized by using thermogravimetric and X-ray diffraction methods for comparison with commercial paste (Solaronix). The TiO2 layer parameters for applying and annealing were optimized by varying the layer thickness and using different masks. The surface morphology of annealed layers was controlled by optical microscopy. Before TiO2 paste applying and after annealing, the conductive glass (fluorine-tin oxide – FTO) was treated by TiCl4 hydrochloric acid solution. The structure of DSSCs were composed FTO-glass / TiO2 layer sensitized Ruthenium complex (N719 dye)/ iodide-based electrolyte / Pt counter electrode/ FTO glass. The DSSC photovoltaic characteristics were measured under AM 1.5G irradiation and demonstrated to be close to those of photoanodes based on the prepared and commercial pastes.https://chimicatechnoacta.ru/article/view/4420dsscgratzel celltio2 pastephotoanodeopen-circuit photo voltageshort-circuit photocurrent densityi-v characteristics
spellingShingle I. O. Selyanin
A. S. Steparuk
R. A. Irgashev
A. V. Mekhaev
G. L. Rusinov
A. S. Vorokh
TiO2 paste for DSSC photoanode: preparation and optimization of application method
Chimica Techno Acta
dssc
gratzel cell
tio2 paste
photoanode
open-circuit photo voltage
short-circuit photocurrent density
i-v characteristics
title TiO2 paste for DSSC photoanode: preparation and optimization of application method
title_full TiO2 paste for DSSC photoanode: preparation and optimization of application method
title_fullStr TiO2 paste for DSSC photoanode: preparation and optimization of application method
title_full_unstemmed TiO2 paste for DSSC photoanode: preparation and optimization of application method
title_short TiO2 paste for DSSC photoanode: preparation and optimization of application method
title_sort tio2 paste for dssc photoanode preparation and optimization of application method
topic dssc
gratzel cell
tio2 paste
photoanode
open-circuit photo voltage
short-circuit photocurrent density
i-v characteristics
url https://chimicatechnoacta.ru/article/view/4420
work_keys_str_mv AT ioselyanin tio2pastefordsscphotoanodepreparationandoptimizationofapplicationmethod
AT assteparuk tio2pastefordsscphotoanodepreparationandoptimizationofapplicationmethod
AT rairgashev tio2pastefordsscphotoanodepreparationandoptimizationofapplicationmethod
AT avmekhaev tio2pastefordsscphotoanodepreparationandoptimizationofapplicationmethod
AT glrusinov tio2pastefordsscphotoanodepreparationandoptimizationofapplicationmethod
AT asvorokh tio2pastefordsscphotoanodepreparationandoptimizationofapplicationmethod