Applications of Transition Metal NMR Spectroscopy in Coordination Chemistry

It is an intriguing task, to probe a complex compound at the metal centre itself instead of relying on secondary informations obtained from the periphery built up by the coordination sphere. Nonetheless, NMR spectroscopy still anchors in (mostly) routine measurements concerned with ligand nuclei su...

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Main Author: Dieter Rehder
Format: Article
Language:deu
Published: Swiss Chemical Society 1986-05-01
Series:CHIMIA
Online Access:https://www.chimia.ch/chimia/article/view/9733
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author Dieter Rehder
author_facet Dieter Rehder
author_sort Dieter Rehder
collection DOAJ
description It is an intriguing task, to probe a complex compound at the metal centre itself instead of relying on secondary informations obtained from the periphery built up by the coordination sphere. Nonetheless, NMR spectroscopy still anchors in (mostly) routine measurements concerned with ligand nuclei such as 1H, 13C, 19F, and 31P. Only very cautiously, inorganic chemists are moving into the promising area of metal NMR. But what is it really, a chemist, working in the fields of coordination chemistry, organometallic chemistry, bioinorganic chemistry or related disciplines, can get out of a metal-NMR spectrum? We shall try to answer this question by (i) elucidating the interpretive background and (ii) presenting a number of illustrative examples where transition metal NMR is exploited to solve problems which otherwise could not easily be dealt with.
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spelling doaj-art-b43aefd6414441ad94800b47b4ea401c2025-08-20T01:47:43ZdeuSwiss Chemical SocietyCHIMIA0009-42932673-24241986-05-0140510.2533/chimia.1986.186Applications of Transition Metal NMR Spectroscopy in Coordination ChemistryDieter Rehder0Institut für Anorganische und Angewandte Chemie Universität Hamburg Martin-Luther-King-Platz 6, D-2000 Hamburg 13 (Bundesrepublik Deutschland) It is an intriguing task, to probe a complex compound at the metal centre itself instead of relying on secondary informations obtained from the periphery built up by the coordination sphere. Nonetheless, NMR spectroscopy still anchors in (mostly) routine measurements concerned with ligand nuclei such as 1H, 13C, 19F, and 31P. Only very cautiously, inorganic chemists are moving into the promising area of metal NMR. But what is it really, a chemist, working in the fields of coordination chemistry, organometallic chemistry, bioinorganic chemistry or related disciplines, can get out of a metal-NMR spectrum? We shall try to answer this question by (i) elucidating the interpretive background and (ii) presenting a number of illustrative examples where transition metal NMR is exploited to solve problems which otherwise could not easily be dealt with. https://www.chimia.ch/chimia/article/view/9733
spellingShingle Dieter Rehder
Applications of Transition Metal NMR Spectroscopy in Coordination Chemistry
CHIMIA
title Applications of Transition Metal NMR Spectroscopy in Coordination Chemistry
title_full Applications of Transition Metal NMR Spectroscopy in Coordination Chemistry
title_fullStr Applications of Transition Metal NMR Spectroscopy in Coordination Chemistry
title_full_unstemmed Applications of Transition Metal NMR Spectroscopy in Coordination Chemistry
title_short Applications of Transition Metal NMR Spectroscopy in Coordination Chemistry
title_sort applications of transition metal nmr spectroscopy in coordination chemistry
url https://www.chimia.ch/chimia/article/view/9733
work_keys_str_mv AT dieterrehder applicationsoftransitionmetalnmrspectroscopyincoordinationchemistry