Microstructure of ultrafine graded cemented carbides with cubic rich surface

The microstructure and mechanical properties of the WC‒10TiC‒0.5VC‒0.5Cr2C3‒12Co and WC‒12Co cemented carbides in the functionally graded and uniform structure were systematically investigated by sintering in nitrogen-rich atmosphere. The scanning electron microscope (SEM), energy disperse spectrosc...

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Main Authors: CHEN Jian, HUANG Yi-ping, ZHU Rui, ZHOU Li, DENG Xin, WU Shang-hua, LIU Bing-yao
Format: Article
Language:zho
Published: Editorial Office of Powder Metallurgy Technology 2021-04-01
Series:Fenmo yejin jishu
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Online Access:https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2020010005
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author CHEN Jian
HUANG Yi-ping
ZHU Rui
ZHOU Li
DENG Xin
WU Shang-hua
LIU Bing-yao
author_facet CHEN Jian
HUANG Yi-ping
ZHU Rui
ZHOU Li
DENG Xin
WU Shang-hua
LIU Bing-yao
author_sort CHEN Jian
collection DOAJ
description The microstructure and mechanical properties of the WC‒10TiC‒0.5VC‒0.5Cr2C3‒12Co and WC‒12Co cemented carbides in the functionally graded and uniform structure were systematically investigated by sintering in nitrogen-rich atmosphere. The scanning electron microscope (SEM), energy disperse spectroscope (EDS), and X-ray diffractometer (XRD) were used for the microstructure observation and phase composition analysis, and the hardness and fracture toughness tests were made in both the surface and the center of the cemented carbides. The results show that, different from the WC‒12Co cemented carbides in uniform structure, the surface layer of the WC‒10TiC‒0.5VC‒0.5Cr2C3‒12Co cemented carbides in the gradient structure is rich in TiCN cubic phase, which is about 12 μm in thickness, and there is a cobalt-rich and coarse-grain intermediate layer below the surface layer of the WC‒10TiC‒0.5VC‒0.5Cr2C3‒12Co cemented carbides. Such gradient and ultrafine cemented carbides show the advantage as the high hardness in the surface layer, the high fracture toughness in the core, and the ultrafine and uniform WC grain.
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institution OA Journals
issn 1001-3784
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publisher Editorial Office of Powder Metallurgy Technology
record_format Article
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spelling doaj-art-b3dcbfbbc95548f79b8a35a91263cce22025-08-20T02:34:19ZzhoEditorial Office of Powder Metallurgy TechnologyFenmo yejin jishu1001-37842021-04-0139211712110.19591/j.cnki.cn11-1974/tf.2020010005Microstructure of ultrafine graded cemented carbides with cubic rich surfaceCHEN JianHUANG Yi-pingZHU RuiZHOU LiDENG XinWU Shang-huaLIU Bing-yaoThe microstructure and mechanical properties of the WC‒10TiC‒0.5VC‒0.5Cr2C3‒12Co and WC‒12Co cemented carbides in the functionally graded and uniform structure were systematically investigated by sintering in nitrogen-rich atmosphere. The scanning electron microscope (SEM), energy disperse spectroscope (EDS), and X-ray diffractometer (XRD) were used for the microstructure observation and phase composition analysis, and the hardness and fracture toughness tests were made in both the surface and the center of the cemented carbides. The results show that, different from the WC‒12Co cemented carbides in uniform structure, the surface layer of the WC‒10TiC‒0.5VC‒0.5Cr2C3‒12Co cemented carbides in the gradient structure is rich in TiCN cubic phase, which is about 12 μm in thickness, and there is a cobalt-rich and coarse-grain intermediate layer below the surface layer of the WC‒10TiC‒0.5VC‒0.5Cr2C3‒12Co cemented carbides. Such gradient and ultrafine cemented carbides show the advantage as the high hardness in the surface layer, the high fracture toughness in the core, and the ultrafine and uniform WC grain.https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2020010005cemented carbidesgradient structuremicrostructuregrain size
spellingShingle CHEN Jian
HUANG Yi-ping
ZHU Rui
ZHOU Li
DENG Xin
WU Shang-hua
LIU Bing-yao
Microstructure of ultrafine graded cemented carbides with cubic rich surface
Fenmo yejin jishu
cemented carbides
gradient structure
microstructure
grain size
title Microstructure of ultrafine graded cemented carbides with cubic rich surface
title_full Microstructure of ultrafine graded cemented carbides with cubic rich surface
title_fullStr Microstructure of ultrafine graded cemented carbides with cubic rich surface
title_full_unstemmed Microstructure of ultrafine graded cemented carbides with cubic rich surface
title_short Microstructure of ultrafine graded cemented carbides with cubic rich surface
title_sort microstructure of ultrafine graded cemented carbides with cubic rich surface
topic cemented carbides
gradient structure
microstructure
grain size
url https://pmt.ustb.edu.cn/article/doi/10.19591/j.cnki.cn11-1974/tf.2020010005
work_keys_str_mv AT chenjian microstructureofultrafinegradedcementedcarbideswithcubicrichsurface
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AT zhouli microstructureofultrafinegradedcementedcarbideswithcubicrichsurface
AT dengxin microstructureofultrafinegradedcementedcarbideswithcubicrichsurface
AT wushanghua microstructureofultrafinegradedcementedcarbideswithcubicrichsurface
AT liubingyao microstructureofultrafinegradedcementedcarbideswithcubicrichsurface