Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate

Beam-based additive manufacturing has challenges in fabricating pure copper due to high reflectivity. Material extrusion additive manufacturing (MEAM) avoids these issues with low costs, making it suitable to fabricate complex structures in pure copper. In this work, the effects of several printing...

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Main Authors: Jiangtao Li, Zhijie Huang, Bing He, Shuhan Li, Bing Lu, Zemin Wang, Xiangyou Li
Format: Article
Language:English
Published: Elsevier 2024-11-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785424022506
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author Jiangtao Li
Zhijie Huang
Bing He
Shuhan Li
Bing Lu
Zemin Wang
Xiangyou Li
author_facet Jiangtao Li
Zhijie Huang
Bing He
Shuhan Li
Bing Lu
Zemin Wang
Xiangyou Li
author_sort Jiangtao Li
collection DOAJ
description Beam-based additive manufacturing has challenges in fabricating pure copper due to high reflectivity. Material extrusion additive manufacturing (MEAM) avoids these issues with low costs, making it suitable to fabricate complex structures in pure copper. In this work, the effects of several printing parameters on the geometry of the samples are studied from single line, thin wall to cube using homemade copper feedstocks with high powder loading rate (65 vol%). The results show that the single line is most affected by layer thickness, while the thin wall has stricter requirements for printing temperature and printing speed. The geometric accuracy of the cube demonstrates large parametric tolerance due to the overlap and support between the lines. Central composite face-centered (CCF) design and central composite design (CCD) are used to analyze and optimize process parameters for densification. The measured porosity at the optimized printing (printing temperature = 177 °C, air gap = −0.05 mm, layer thickness = 0.3 mm) and sintering parameters (sintering temperature = 1045 °C, holding time = 4 h) is in good agreement with the predicted values. Air gap and sintering temperature have the greatest influence on the porosity, and other parameters within a certain range of on-demand adjustments do not have a significant effect. The ultimate tensile strength and elongation of the sintered samples under the optimal parameters are 153.9 ± 6.1 MPa and 31.36 ± 3.24%, respectively. No printing defects are found at the fracture and the elongation is good, showing the effectiveness of the parameter optimization.
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spelling doaj-art-b2bfac4e4d2846838c5707d10dc73cb02025-08-20T02:39:15ZengElsevierJournal of Materials Research and Technology2238-78542024-11-01332568257910.1016/j.jmrt.2024.09.245Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rateJiangtao Li0Zhijie Huang1Bing He2Shuhan Li3Bing Lu4Zemin Wang5Xiangyou Li6Wuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology (HUST), Wuhan, 430074, PR ChinaWuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology (HUST), Wuhan, 430074, PR ChinaWuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology (HUST), Wuhan, 430074, PR ChinaWuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology (HUST), Wuhan, 430074, PR ChinaWuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology (HUST), Wuhan, 430074, PR ChinaWuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology (HUST), Wuhan, 430074, PR ChinaCorresponding author.; Wuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology (HUST), Wuhan, 430074, PR ChinaBeam-based additive manufacturing has challenges in fabricating pure copper due to high reflectivity. Material extrusion additive manufacturing (MEAM) avoids these issues with low costs, making it suitable to fabricate complex structures in pure copper. In this work, the effects of several printing parameters on the geometry of the samples are studied from single line, thin wall to cube using homemade copper feedstocks with high powder loading rate (65 vol%). The results show that the single line is most affected by layer thickness, while the thin wall has stricter requirements for printing temperature and printing speed. The geometric accuracy of the cube demonstrates large parametric tolerance due to the overlap and support between the lines. Central composite face-centered (CCF) design and central composite design (CCD) are used to analyze and optimize process parameters for densification. The measured porosity at the optimized printing (printing temperature = 177 °C, air gap = −0.05 mm, layer thickness = 0.3 mm) and sintering parameters (sintering temperature = 1045 °C, holding time = 4 h) is in good agreement with the predicted values. Air gap and sintering temperature have the greatest influence on the porosity, and other parameters within a certain range of on-demand adjustments do not have a significant effect. The ultimate tensile strength and elongation of the sintered samples under the optimal parameters are 153.9 ± 6.1 MPa and 31.36 ± 3.24%, respectively. No printing defects are found at the fracture and the elongation is good, showing the effectiveness of the parameter optimization.http://www.sciencedirect.com/science/article/pii/S2238785424022506Additive manufacturingPure copperOptimizationPorositySintering
spellingShingle Jiangtao Li
Zhijie Huang
Bing He
Shuhan Li
Bing Lu
Zemin Wang
Xiangyou Li
Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate
Journal of Materials Research and Technology
Additive manufacturing
Pure copper
Optimization
Porosity
Sintering
title Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate
title_full Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate
title_fullStr Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate
title_full_unstemmed Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate
title_short Experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate
title_sort experimental investigation of material extrusion additive manufacturing of copper with high powder loading rate
topic Additive manufacturing
Pure copper
Optimization
Porosity
Sintering
url http://www.sciencedirect.com/science/article/pii/S2238785424022506
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AT binglu experimentalinvestigationofmaterialextrusionadditivemanufacturingofcopperwithhighpowderloadingrate
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