Synthese von Nonaheptafulvalen-Vorstufen

Possible precursors of the attractive nonaheptafulvalene (3) are prepared by reaction of acetoxy-tropylium-fluoroborate (5a) as well as of bromo-tropylium-bromide (5b) with lithium-cyclononatetraenide. The structure of the substituted cycloheptatrienyl-cyclononatetraenes 6 has been proved by NMR-sp...

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Main Authors: Markus Neuenschwander, Alfred Frey
Format: Article
Language:deu
Published: Swiss Chemical Society 1977-08-01
Series:CHIMIA
Online Access:https://www.chimia.ch/chimia/article/view/9379
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author Markus Neuenschwander
Alfred Frey
author_facet Markus Neuenschwander
Alfred Frey
author_sort Markus Neuenschwander
collection DOAJ
description Possible precursors of the attractive nonaheptafulvalene (3) are prepared by reaction of acetoxy-tropylium-fluoroborate (5a) as well as of bromo-tropylium-bromide (5b) with lithium-cyclononatetraenide. The structure of the substituted cycloheptatrienyl-cyclononatetraenes 6 has been proved by NMR-spectroscopy as well as by valence-isomerisation to acetoxycycloheptatrienyl- and bromocycloheptatrienyl-cyclononatetraenes 7a and 7b respectively.
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publishDate 1977-08-01
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spelling doaj-art-b286e12756d94f63b95064cff815eb122025-08-20T02:29:54ZdeuSwiss Chemical SocietyCHIMIA0009-42932673-24241977-08-0131810.2533/chimia.1977.333Synthese von Nonaheptafulvalen-VorstufenMarkus Neuenschwander0Alfred Frey1Institut für Organische Chemie, Universität BernInstitut für Organische Chemie, Universität Bern Possible precursors of the attractive nonaheptafulvalene (3) are prepared by reaction of acetoxy-tropylium-fluoroborate (5a) as well as of bromo-tropylium-bromide (5b) with lithium-cyclononatetraenide. The structure of the substituted cycloheptatrienyl-cyclononatetraenes 6 has been proved by NMR-spectroscopy as well as by valence-isomerisation to acetoxycycloheptatrienyl- and bromocycloheptatrienyl-cyclononatetraenes 7a and 7b respectively. https://www.chimia.ch/chimia/article/view/9379
spellingShingle Markus Neuenschwander
Alfred Frey
Synthese von Nonaheptafulvalen-Vorstufen
CHIMIA
title Synthese von Nonaheptafulvalen-Vorstufen
title_full Synthese von Nonaheptafulvalen-Vorstufen
title_fullStr Synthese von Nonaheptafulvalen-Vorstufen
title_full_unstemmed Synthese von Nonaheptafulvalen-Vorstufen
title_short Synthese von Nonaheptafulvalen-Vorstufen
title_sort synthese von nonaheptafulvalen vorstufen
url https://www.chimia.ch/chimia/article/view/9379
work_keys_str_mv AT markusneuenschwander synthesevonnonaheptafulvalenvorstufen
AT alfredfrey synthesevonnonaheptafulvalenvorstufen