Fluorescently Tagged Poly(methyl methacrylate)s

Plastic pollution is a global problem affecting the environment and, consequently, people’s well-being. Careful and timely end-of-life plastic recycling is certainly a way, albeit a partial one, to remedy the problem. The immediate identification and selection of the different types of plastic mater...

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Main Authors: Fabia Grisi, Rubina Troiano, Donatella Fiore, Patrizia Gazzerro, Mariateresa Lettieri, Vincenzo Venditto, Stefania Pragliola
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:Molecules
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Online Access:https://www.mdpi.com/1420-3049/29/24/5940
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author Fabia Grisi
Rubina Troiano
Donatella Fiore
Patrizia Gazzerro
Mariateresa Lettieri
Vincenzo Venditto
Stefania Pragliola
author_facet Fabia Grisi
Rubina Troiano
Donatella Fiore
Patrizia Gazzerro
Mariateresa Lettieri
Vincenzo Venditto
Stefania Pragliola
author_sort Fabia Grisi
collection DOAJ
description Plastic pollution is a global problem affecting the environment and, consequently, people’s well-being. Careful and timely end-of-life plastic recycling is certainly a way, albeit a partial one, to remedy the problem. The immediate identification and selection of the different types of plastic materials in the recycling process certainly facilitate its recovery and reuse, allowing the damage caused by plastic emission into the environment to be limited. Recently, new technologies for automatic sorting of plastics based upon fluorescent tagging have been considered. This article reports the synthesis and characterization of fluorescent copolymers of poly(methyl methacrylate) (PMMA) that could be potentially used as fluorescent markers of commercial PMMA. Poly(methylmetacrylate-<i>co</i>-2-(9-carbazolyl)ethyl methacrylate) (P(MMA-<i>co</i>-CEMA)) and poly(methylmetacrylate-<i>co</i>-7-methacryloyloxycoumarin) (P(MMA-<i>co</i>-MAOC)) samples containing a small number of fluorescent units (<4%) were synthesized by free-radical polymerization. All copolymer samples show chemico-physical properties like those of pure PMMA and produce fluorescence emission under 290 nm wavelength excitation. P(MMA-<i>co</i>-CEMA)s and P(MMA-<i>co</i>-MAOC)s were also tested as fluorescent dyes for PMMA identification. The experimental results demonstrate that PMMA/P(MMA-<i>co</i>-CEMA) and PMMA/P(MMA-<i>co</i>-MAOC) blends prepared using 1% by weight of fluorescent copolymer show a homogeneous morphology completely similar to pure PMMA and are still optically active.
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spelling doaj-art-b17df3cce6824867a67d0901c3e014b62025-08-20T02:51:07ZengMDPI AGMolecules1420-30492024-12-012924594010.3390/molecules29245940Fluorescently Tagged Poly(methyl methacrylate)sFabia Grisi0Rubina Troiano1Donatella Fiore2Patrizia Gazzerro3Mariateresa Lettieri4Vincenzo Venditto5Stefania Pragliola6Dipartimento di Chimica e Biologia, and INSTM Research Unit, Università di Salerno, Via Giovanni Paolo II 132, I-84084 Fisciano, SA, ItalyDipartimento di Chimica e Biologia, and INSTM Research Unit, Università di Salerno, Via Giovanni Paolo II 132, I-84084 Fisciano, SA, ItalyDipartimento di Farmacia, Università di Salerno, Via Giovanni Paolo II, 132, I-84084 Fisciano, SA, ItalyDipartimento di Farmacia, Università di Salerno, Via Giovanni Paolo II, 132, I-84084 Fisciano, SA, ItalyCNR-SPIN, c/o Dipartimento di Fisica, Università di Salerno, Via Giovanni Paolo II, 132, I-84084 Fisciano, SA, ItalyDipartimento di Chimica e Biologia, and INSTM Research Unit, Università di Salerno, Via Giovanni Paolo II 132, I-84084 Fisciano, SA, ItalyDipartimento di Chimica e Biologia, and INSTM Research Unit, Università di Salerno, Via Giovanni Paolo II 132, I-84084 Fisciano, SA, ItalyPlastic pollution is a global problem affecting the environment and, consequently, people’s well-being. Careful and timely end-of-life plastic recycling is certainly a way, albeit a partial one, to remedy the problem. The immediate identification and selection of the different types of plastic materials in the recycling process certainly facilitate its recovery and reuse, allowing the damage caused by plastic emission into the environment to be limited. Recently, new technologies for automatic sorting of plastics based upon fluorescent tagging have been considered. This article reports the synthesis and characterization of fluorescent copolymers of poly(methyl methacrylate) (PMMA) that could be potentially used as fluorescent markers of commercial PMMA. Poly(methylmetacrylate-<i>co</i>-2-(9-carbazolyl)ethyl methacrylate) (P(MMA-<i>co</i>-CEMA)) and poly(methylmetacrylate-<i>co</i>-7-methacryloyloxycoumarin) (P(MMA-<i>co</i>-MAOC)) samples containing a small number of fluorescent units (<4%) were synthesized by free-radical polymerization. All copolymer samples show chemico-physical properties like those of pure PMMA and produce fluorescence emission under 290 nm wavelength excitation. P(MMA-<i>co</i>-CEMA)s and P(MMA-<i>co</i>-MAOC)s were also tested as fluorescent dyes for PMMA identification. The experimental results demonstrate that PMMA/P(MMA-<i>co</i>-CEMA) and PMMA/P(MMA-<i>co</i>-MAOC) blends prepared using 1% by weight of fluorescent copolymer show a homogeneous morphology completely similar to pure PMMA and are still optically active.https://www.mdpi.com/1420-3049/29/24/5940poly(methyl metacrylate)carbazolecoumarinfluorescent taggingplastic recycling
spellingShingle Fabia Grisi
Rubina Troiano
Donatella Fiore
Patrizia Gazzerro
Mariateresa Lettieri
Vincenzo Venditto
Stefania Pragliola
Fluorescently Tagged Poly(methyl methacrylate)s
Molecules
poly(methyl metacrylate)
carbazole
coumarin
fluorescent tagging
plastic recycling
title Fluorescently Tagged Poly(methyl methacrylate)s
title_full Fluorescently Tagged Poly(methyl methacrylate)s
title_fullStr Fluorescently Tagged Poly(methyl methacrylate)s
title_full_unstemmed Fluorescently Tagged Poly(methyl methacrylate)s
title_short Fluorescently Tagged Poly(methyl methacrylate)s
title_sort fluorescently tagged poly methyl methacrylate s
topic poly(methyl metacrylate)
carbazole
coumarin
fluorescent tagging
plastic recycling
url https://www.mdpi.com/1420-3049/29/24/5940
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AT rubinatroiano fluorescentlytaggedpolymethylmethacrylates
AT donatellafiore fluorescentlytaggedpolymethylmethacrylates
AT patriziagazzerro fluorescentlytaggedpolymethylmethacrylates
AT mariateresalettieri fluorescentlytaggedpolymethylmethacrylates
AT vincenzovenditto fluorescentlytaggedpolymethylmethacrylates
AT stefaniapragliola fluorescentlytaggedpolymethylmethacrylates