NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIES

On allowing NH3CH2CH2NH3(PhCO2)2 in slightly hydrated methanol to react with SnPh2Cl2, NH3CH2CH2NH3PhCO2SnPhCl3OH is obtained as a white precipitate. The IR and Mössbauer studies allow to suggest a moiety obtained by addition of OH- and PhCO2- to SnPhCl3, the environment around the tin being octahed...

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Main Authors: Libasse Diop, Kochikpa Y.A. Okio
Format: Article
Language:English
Published: Alma Mater Publishing House "Vasile Alecsandri" University of Bacau 2010-07-01
Series:Scientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry
Subjects:
Online Access:http://pubs.ub.ro/dwnl.php?id=CSCC6201011V02S01A0005
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author Libasse Diop
Kochikpa Y.A. Okio
author_facet Libasse Diop
Kochikpa Y.A. Okio
author_sort Libasse Diop
collection DOAJ
description On allowing NH3CH2CH2NH3(PhCO2)2 in slightly hydrated methanol to react with SnPh2Cl2, NH3CH2CH2NH3PhCO2SnPhCl3OH is obtained as a white precipitate. The IR and Mössbauer studies allow to suggest a moiety obtained by addition of OH- and PhCO2- to SnPhCl3, the environment around the tin being octahedral, PhCO2- behaving as a monocoordinating ligand.
format Article
id doaj-art-b0fc406507ed49bbbfbe134bb4765f9d
institution OA Journals
issn 1582-540X
language English
publishDate 2010-07-01
publisher Alma Mater Publishing House "Vasile Alecsandri" University of Bacau
record_format Article
series Scientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry
spelling doaj-art-b0fc406507ed49bbbfbe134bb4765f9d2025-08-20T02:00:37ZengAlma Mater Publishing House "Vasile Alecsandri" University of BacauScientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry1582-540X2010-07-01112299302NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIESLibasse DiopKochikpa Y.A. OkioOn allowing NH3CH2CH2NH3(PhCO2)2 in slightly hydrated methanol to react with SnPh2Cl2, NH3CH2CH2NH3PhCO2SnPhCl3OH is obtained as a white precipitate. The IR and Mössbauer studies allow to suggest a moiety obtained by addition of OH- and PhCO2- to SnPhCl3, the environment around the tin being octahedral, PhCO2- behaving as a monocoordinating ligand.http://pubs.ub.ro/dwnl.php?id=CSCC6201011V02S01A0005phenyl tin compoundbenzoateinfrared spectrumMössbauer spectrumpolymeric structure
spellingShingle Libasse Diop
Kochikpa Y.A. Okio
NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIES
Scientific Study & Research: Chemistry & Chemical Engineering, Biotechnology, Food Industry
phenyl tin compound
benzoate
infrared spectrum
Mössbauer spectrum
polymeric structure
title NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIES
title_full NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIES
title_fullStr NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIES
title_full_unstemmed NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIES
title_short NH3CH2CH2NH3PhCO2SnPhCl3OH, AN UNEXPECTED ADDUCT: SYNTHESIS AND SPECTROSCOPIC STUDIES
title_sort nh3ch2ch2nh3phco2snphcl3oh an unexpected adduct synthesis and spectroscopic studies
topic phenyl tin compound
benzoate
infrared spectrum
Mössbauer spectrum
polymeric structure
url http://pubs.ub.ro/dwnl.php?id=CSCC6201011V02S01A0005
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AT kochikpayaokio nh3ch2ch2nh3phco2snphcl3ohanunexpectedadductsynthesisandspectroscopicstudies