Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic Fragmentation

Viscosimetric experiments and microscopy measurements on microdispersions of polycaprolactone (PCL) plastics showed an unexpected exponential decrease in viscosity over the first 3 months and a plateau for a further 4 months of observations. This behavior is due to the release of nanoplastics from s...

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Main Authors: Vincenzo Villani, Pier Luigi Gentili
Format: Article
Language:English
Published: MDPI AG 2025-05-01
Series:Molecules
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Online Access:https://www.mdpi.com/1420-3049/30/10/2235
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author Vincenzo Villani
Pier Luigi Gentili
author_facet Vincenzo Villani
Pier Luigi Gentili
author_sort Vincenzo Villani
collection DOAJ
description Viscosimetric experiments and microscopy measurements on microdispersions of polycaprolactone (PCL) plastics showed an unexpected exponential decrease in viscosity over the first 3 months and a plateau for a further 4 months of observations. This behavior is due to the release of nanoplastics from semicrystalline particles that reduce the viscosity of the dispersion, and leave stable and fine crystalline microplastics ranging in size from 30 to 180 μm. The development of nonlinear kinetic models for the fragmentation process from macro- to meso-, micro-, and nanoplastics reveals complex behavior that we call a cracking–leaching mechanism. The autocatalytic mechanical cracking of macroplastics larger than 5 mm is followed by a logistic-type mechanical cracking of mesoplastics between 5 and 1 mm. Therefore, microplastics smaller than 1 mm experience the leaching diffusion modeled via nonlinear coupled kinetic differential equations: semicrystalline microplastics quickly release nanoplastics from the amorphous fraction, followed by fine and stable crystalline microplastics. This proposed mechanism explains the size distribution of floating plastic debris in the oceans, with an unexpected gap of microplastics. Considering the outcome, a general reflection is made on the critical issues that currently appear unsolvable regarding plastic pollution.
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spelling doaj-art-afc06f2425dd4f70967b0d5e0e2aa1902025-08-20T01:56:35ZengMDPI AGMolecules1420-30492025-05-013010223510.3390/molecules30102235Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic FragmentationVincenzo Villani0Pier Luigi Gentili1Department of Basic and Applied Sciences, University of Basilicata, Campus Macchia Romana, 85100 Potenza, ItalyDepartment of Chemistry, Biology, and Biotechnology, University of Perugia, Via Elce di Sotto 8, 06123 Perugia, ItalyViscosimetric experiments and microscopy measurements on microdispersions of polycaprolactone (PCL) plastics showed an unexpected exponential decrease in viscosity over the first 3 months and a plateau for a further 4 months of observations. This behavior is due to the release of nanoplastics from semicrystalline particles that reduce the viscosity of the dispersion, and leave stable and fine crystalline microplastics ranging in size from 30 to 180 μm. The development of nonlinear kinetic models for the fragmentation process from macro- to meso-, micro-, and nanoplastics reveals complex behavior that we call a cracking–leaching mechanism. The autocatalytic mechanical cracking of macroplastics larger than 5 mm is followed by a logistic-type mechanical cracking of mesoplastics between 5 and 1 mm. Therefore, microplastics smaller than 1 mm experience the leaching diffusion modeled via nonlinear coupled kinetic differential equations: semicrystalline microplastics quickly release nanoplastics from the amorphous fraction, followed by fine and stable crystalline microplastics. This proposed mechanism explains the size distribution of floating plastic debris in the oceans, with an unexpected gap of microplastics. Considering the outcome, a general reflection is made on the critical issues that currently appear unsolvable regarding plastic pollution.https://www.mdpi.com/1420-3049/30/10/2235plastic pollutionkinetic models of fragmentationpolycaprolactone (PCL)viscosity of dispersionsmicroplasticsnanoplastics
spellingShingle Vincenzo Villani
Pier Luigi Gentili
Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic Fragmentation
Molecules
plastic pollution
kinetic models of fragmentation
polycaprolactone (PCL)
viscosity of dispersions
microplastics
nanoplastics
title Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic Fragmentation
title_full Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic Fragmentation
title_fullStr Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic Fragmentation
title_full_unstemmed Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic Fragmentation
title_short Viscosity of Polycaprolactone Microplastic Dispersions and Nonlinear Kinetic Models of Plastic Fragmentation
title_sort viscosity of polycaprolactone microplastic dispersions and nonlinear kinetic models of plastic fragmentation
topic plastic pollution
kinetic models of fragmentation
polycaprolactone (PCL)
viscosity of dispersions
microplastics
nanoplastics
url https://www.mdpi.com/1420-3049/30/10/2235
work_keys_str_mv AT vincenzovillani viscosityofpolycaprolactonemicroplasticdispersionsandnonlinearkineticmodelsofplasticfragmentation
AT pierluigigentili viscosityofpolycaprolactonemicroplasticdispersionsandnonlinearkineticmodelsofplasticfragmentation