Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocomposites
Novel Ag2S/PbSO4 nanocomposites have been successfully synthesized by solvothermal process in propylene glycol as solvent. In this study, sodium dodecyl sulfate (SDS) was applied not only as a surfactant, but also as a sulfur source to produce Ag2S/PbSO4. The products were characterized by X-ray dif...
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| Language: | English |
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Springer
2017-02-01
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| Series: | Journal of Saudi Chemical Society |
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| Online Access: | http://www.sciencedirect.com/science/article/pii/S131961031500054X |
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| author | Mohammad Ali Karimi Mehdi Ranjbar Ashraf Salmanipour |
| author_facet | Mohammad Ali Karimi Mehdi Ranjbar Ashraf Salmanipour |
| author_sort | Mohammad Ali Karimi |
| collection | DOAJ |
| description | Novel Ag2S/PbSO4 nanocomposites have been successfully synthesized by solvothermal process in propylene glycol as solvent. In this study, sodium dodecyl sulfate (SDS) was applied not only as a surfactant, but also as a sulfur source to produce Ag2S/PbSO4. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), photoluminescence (PL) spectroscopy and energy dispersive spectroscopy (EDS). The absorption and photoluminescence study of the Ag2S/PbSO4 nanocomposite showed quantum confinement behavior with band gap of 3.1 eV. Moreover, effects of reaction time on the morphology and particle sizes of the final products have been investigated by SEM images. |
| format | Article |
| id | doaj-art-af387afd328143629f0b8c9dd6ec8b2c |
| institution | Kabale University |
| issn | 1319-6103 |
| language | English |
| publishDate | 2017-02-01 |
| publisher | Springer |
| record_format | Article |
| series | Journal of Saudi Chemical Society |
| spelling | doaj-art-af387afd328143629f0b8c9dd6ec8b2c2025-08-20T03:52:03ZengSpringerJournal of Saudi Chemical Society1319-61032017-02-0121219319710.1016/j.jscs.2015.04.006Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocompositesMohammad Ali Karimi0Mehdi Ranjbar1Ashraf Salmanipour2Department of Chemistry, Payame Noor University, P.O. Box 19395-3697, Tehran, IranYoung Researchers and Elite Club, Kerman Branch, Islamic Azad University, Kerman, IranDepartment of Chemistry, Shahid Bahonar University of Kerman, P.O. Box 76175-133, Kerman, IranNovel Ag2S/PbSO4 nanocomposites have been successfully synthesized by solvothermal process in propylene glycol as solvent. In this study, sodium dodecyl sulfate (SDS) was applied not only as a surfactant, but also as a sulfur source to produce Ag2S/PbSO4. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), photoluminescence (PL) spectroscopy and energy dispersive spectroscopy (EDS). The absorption and photoluminescence study of the Ag2S/PbSO4 nanocomposite showed quantum confinement behavior with band gap of 3.1 eV. Moreover, effects of reaction time on the morphology and particle sizes of the final products have been investigated by SEM images.http://www.sciencedirect.com/science/article/pii/S131961031500054XSynthesisNanocompositesSolvothermalScanning electron microscopyX-ray diffraction |
| spellingShingle | Mohammad Ali Karimi Mehdi Ranjbar Ashraf Salmanipour Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocomposites Journal of Saudi Chemical Society Synthesis Nanocomposites Solvothermal Scanning electron microscopy X-ray diffraction |
| title | Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocomposites |
| title_full | Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocomposites |
| title_fullStr | Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocomposites |
| title_full_unstemmed | Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocomposites |
| title_short | Novel solvothermal synthesis and characterization of Ag2S/PbSO4 nanocomposites |
| title_sort | novel solvothermal synthesis and characterization of ag2s pbso4 nanocomposites |
| topic | Synthesis Nanocomposites Solvothermal Scanning electron microscopy X-ray diffraction |
| url | http://www.sciencedirect.com/science/article/pii/S131961031500054X |
| work_keys_str_mv | AT mohammadalikarimi novelsolvothermalsynthesisandcharacterizationofag2spbso4nanocomposites AT mehdiranjbar novelsolvothermalsynthesisandcharacterizationofag2spbso4nanocomposites AT ashrafsalmanipour novelsolvothermalsynthesisandcharacterizationofag2spbso4nanocomposites |