DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosis

Abstract Solid bubbles have expanded the SERS assay toolbox, but their detection performance in biofluids is still hampered by the irrational design of the plasmonic sensing interface. A plasmonic bubble aggregate‐driven DNA‐encoded SERS assay is reported here that enables simultaneous, ultrasensiti...

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Main Authors: Yu Yang, Hao Lu, Dan Fang, Yuyuan Zhang, Yuteng Tang, Songsong Zhao, Jun Yan, Xiaojie Qin, Jianlei Shen, Fan Yang
Format: Article
Language:English
Published: Wiley 2024-12-01
Series:Aggregate
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Online Access:https://doi.org/10.1002/agt2.636
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author Yu Yang
Hao Lu
Dan Fang
Yuyuan Zhang
Yuteng Tang
Songsong Zhao
Jun Yan
Xiaojie Qin
Jianlei Shen
Fan Yang
author_facet Yu Yang
Hao Lu
Dan Fang
Yuyuan Zhang
Yuteng Tang
Songsong Zhao
Jun Yan
Xiaojie Qin
Jianlei Shen
Fan Yang
author_sort Yu Yang
collection DOAJ
description Abstract Solid bubbles have expanded the SERS assay toolbox, but their detection performance in biofluids is still hampered by the irrational design of the plasmonic sensing interface. A plasmonic bubble aggregate‐driven DNA‐encoded SERS assay is reported here that enables simultaneous, ultrasensitive, and specific detection of multiple miRNAs in blood samples for accurate cancer diagnosis. In this assay, the buoyancy of plasmonic bubbles allows them to self‐aggregate at a droplet apex for SERS reconfiguration, form single‐layer bubble aggregates with plasmonic nanogaps, and prevent the coffee ring effect during evaporation assembly. Furthermore, DNA‐encoded plasmonic bubbles seamlessly couple with dual‐color catalytic hybridization assembly to amplify the specific miRNA‐responsive Raman signal, and function as both an analyte concentrator and a Raman signal aggregator without external forces. Using these merits, this magnet‐free, portable assay achieves femtomolar dual‐miRNA quantitation with single‐base resolution, simultaneous miRNA detection across four cell lines, and accurate cancer diagnosis (AUC = 1) via analyzing 40 blood samples with machine learning, thus providing a promising tool for clinical diagnosis.
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institution DOAJ
issn 2692-4560
language English
publishDate 2024-12-01
publisher Wiley
record_format Article
series Aggregate
spelling doaj-art-ad4f7af39a7d4d7b9d2c2761097de25e2025-08-20T02:49:08ZengWileyAggregate2692-45602024-12-0156n/an/a10.1002/agt2.636DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosisYu Yang0Hao Lu1Dan Fang2Yuyuan Zhang3Yuteng Tang4Songsong Zhao5Jun Yan6Xiaojie Qin7Jianlei Shen8Fan Yang9Guangxi Key Laboratory of Pharmaceutical Precision Detection and Screening Key Laboratory of Micro‐Nanoscale Bioanalysis and Drug Screening of Guangxi Education Department State Key Laboratory of Targeting Oncology Pharmaceutical College Guangxi Medical University Nanning ChinaGuangxi Key Laboratory of Pharmaceutical Precision Detection and Screening Key Laboratory of Micro‐Nanoscale Bioanalysis and Drug Screening of Guangxi Education Department State Key Laboratory of Targeting Oncology Pharmaceutical College Guangxi Medical University Nanning ChinaGuangxi Key Laboratory of Pharmaceutical Precision Detection and Screening Key Laboratory of Micro‐Nanoscale Bioanalysis and Drug Screening of Guangxi Education Department State Key Laboratory of Targeting Oncology Pharmaceutical College Guangxi Medical University Nanning ChinaGuangxi Key Laboratory of Pharmaceutical Precision Detection and Screening Key Laboratory of Micro‐Nanoscale Bioanalysis and Drug Screening of Guangxi Education Department State Key Laboratory of Targeting Oncology Pharmaceutical College Guangxi Medical University Nanning ChinaGuangxi Key Laboratory of Pharmaceutical Precision Detection and Screening Key Laboratory of Micro‐Nanoscale Bioanalysis and Drug Screening of Guangxi Education Department State Key Laboratory of Targeting Oncology Pharmaceutical College Guangxi Medical University Nanning ChinaGuangxi Key Laboratory of Chemistry and Engineering of Forest Products Guangxi Collaborative Innovation Center for Chemistry and Engineering of Forest Products College of Chemistry and Chemical Engineering Guangxi Minzu University Nanning ChinaGuangxi Key Laboratory of Chemistry and Engineering of Forest Products Guangxi Collaborative Innovation Center for Chemistry and Engineering of Forest Products College of Chemistry and Chemical Engineering Guangxi Minzu University Nanning ChinaGuangxi Key Laboratory of Pharmaceutical Precision Detection and Screening Key Laboratory of Micro‐Nanoscale Bioanalysis and Drug Screening of Guangxi Education Department State Key Laboratory of Targeting Oncology Pharmaceutical College Guangxi Medical University Nanning ChinaSchool of Chemistry and Chemical Engineering Shanghai Jiao Tong University Shanghai ChinaGuangxi Key Laboratory of Pharmaceutical Precision Detection and Screening Key Laboratory of Micro‐Nanoscale Bioanalysis and Drug Screening of Guangxi Education Department State Key Laboratory of Targeting Oncology Pharmaceutical College Guangxi Medical University Nanning ChinaAbstract Solid bubbles have expanded the SERS assay toolbox, but their detection performance in biofluids is still hampered by the irrational design of the plasmonic sensing interface. A plasmonic bubble aggregate‐driven DNA‐encoded SERS assay is reported here that enables simultaneous, ultrasensitive, and specific detection of multiple miRNAs in blood samples for accurate cancer diagnosis. In this assay, the buoyancy of plasmonic bubbles allows them to self‐aggregate at a droplet apex for SERS reconfiguration, form single‐layer bubble aggregates with plasmonic nanogaps, and prevent the coffee ring effect during evaporation assembly. Furthermore, DNA‐encoded plasmonic bubbles seamlessly couple with dual‐color catalytic hybridization assembly to amplify the specific miRNA‐responsive Raman signal, and function as both an analyte concentrator and a Raman signal aggregator without external forces. Using these merits, this magnet‐free, portable assay achieves femtomolar dual‐miRNA quantitation with single‐base resolution, simultaneous miRNA detection across four cell lines, and accurate cancer diagnosis (AUC = 1) via analyzing 40 blood samples with machine learning, thus providing a promising tool for clinical diagnosis.https://doi.org/10.1002/agt2.636DNA assemblyDNA‐encoded SERS nanosensorsmicroRNAplasmonic bubbleself‐aggregation nanogap
spellingShingle Yu Yang
Hao Lu
Dan Fang
Yuyuan Zhang
Yuteng Tang
Songsong Zhao
Jun Yan
Xiaojie Qin
Jianlei Shen
Fan Yang
DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosis
Aggregate
DNA assembly
DNA‐encoded SERS nanosensors
microRNA
plasmonic bubble
self‐aggregation nanogap
title DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosis
title_full DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosis
title_fullStr DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosis
title_full_unstemmed DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosis
title_short DNA‐encoded plasmonic bubbles aggregating dual‐microRNA SERS signals for cancer diagnosis
title_sort dna encoded plasmonic bubbles aggregating dual microrna sers signals for cancer diagnosis
topic DNA assembly
DNA‐encoded SERS nanosensors
microRNA
plasmonic bubble
self‐aggregation nanogap
url https://doi.org/10.1002/agt2.636
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