Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin Film

Abstract Experimentally achieving the first‐ever electric field periodic poling of single crystal barium titanate oxide (BTO, or BaTiO3) thin film on‐insulator is reported. Owing to the outstanding optical nonlinearities of BTO, this result is a key step toward achieving quasi‐phase‐matching (QPM)....

Full description

Saved in:
Bibliographic Details
Main Authors: Pragati Aashna, Hong‐Lin Lin, Yu Cao, Yuhui Yin, Yuan Gao, Sakthi Sanjeev Mohanraj, Di Zhu, Aaron Danner
Format: Article
Language:English
Published: Wiley 2024-11-01
Series:Advanced Science
Subjects:
Online Access:https://doi.org/10.1002/advs.202406248
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850274070048800768
author Pragati Aashna
Hong‐Lin Lin
Yu Cao
Yuhui Yin
Yuan Gao
Sakthi Sanjeev Mohanraj
Di Zhu
Aaron Danner
author_facet Pragati Aashna
Hong‐Lin Lin
Yu Cao
Yuhui Yin
Yuan Gao
Sakthi Sanjeev Mohanraj
Di Zhu
Aaron Danner
author_sort Pragati Aashna
collection DOAJ
description Abstract Experimentally achieving the first‐ever electric field periodic poling of single crystal barium titanate oxide (BTO, or BaTiO3) thin film on‐insulator is reported. Owing to the outstanding optical nonlinearities of BTO, this result is a key step toward achieving quasi‐phase‐matching (QPM). First, the BTO thin film is grown on a dysprosium scandate substrate using pulsed laser deposition with a thin layer of strontium ruthenate later serving as the bottom electrode for poling. The characterization of the BTO thin film using x‐ray diffraction (XRD) and piezo‐response force microscopy to demonstrate single crystal, single domain growth of the film that enables the desired periodic poling, are presented. To investigate the poling quality, both non‐destructive piezo force response microscopy and destructive etching‐assisted scanning electron microscopy (SEM) are applied, and it is shown that high quality, uniform, and intransient poling with 50% duty cycle and periods ranging from 2 µm to 10 µm is achieved. The successful realization of periodic poling in BTO thin film unlocks the potential for highly efficient nonlinear processes under QPM that seemed far‐fetched with prior polycrystalline BTO thin films which predominantly relied on efficiency‐limited random or non‐phase matching conditions and is a key step toward integration of BTO photonic devices.
format Article
id doaj-art-ace7c59bfc2e49e09a6f066838654071
institution OA Journals
issn 2198-3844
language English
publishDate 2024-11-01
publisher Wiley
record_format Article
series Advanced Science
spelling doaj-art-ace7c59bfc2e49e09a6f0668386540712025-08-20T01:51:14ZengWileyAdvanced Science2198-38442024-11-011142n/an/a10.1002/advs.202406248Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin FilmPragati Aashna0Hong‐Lin Lin1Yu Cao2Yuhui Yin3Yuan Gao4Sakthi Sanjeev Mohanraj5Di Zhu6Aaron Danner7Department of Electrical and Computer Engineering National University of Singapore Singapore 117583 SingaporeDepartment of Electrical and Computer Engineering National University of Singapore Singapore 117583 SingaporeDepartment of Electrical and Computer Engineering National University of Singapore Singapore 117583 SingaporeDepartment of Electrical and Computer Engineering National University of Singapore Singapore 117583 SingaporeDepartment of Electrical and Computer Engineering National University of Singapore Singapore 117583 SingaporeInstitute of Materials Research and Engineering (IMRE) Agency for Science, Technology and Research (A*STAR) Singapore 138634 SingaporeDepartment of Materials Science and Engineering National University of Singapore Singapore 117575 SingaporeDepartment of Electrical and Computer Engineering National University of Singapore Singapore 117583 SingaporeAbstract Experimentally achieving the first‐ever electric field periodic poling of single crystal barium titanate oxide (BTO, or BaTiO3) thin film on‐insulator is reported. Owing to the outstanding optical nonlinearities of BTO, this result is a key step toward achieving quasi‐phase‐matching (QPM). First, the BTO thin film is grown on a dysprosium scandate substrate using pulsed laser deposition with a thin layer of strontium ruthenate later serving as the bottom electrode for poling. The characterization of the BTO thin film using x‐ray diffraction (XRD) and piezo‐response force microscopy to demonstrate single crystal, single domain growth of the film that enables the desired periodic poling, are presented. To investigate the poling quality, both non‐destructive piezo force response microscopy and destructive etching‐assisted scanning electron microscopy (SEM) are applied, and it is shown that high quality, uniform, and intransient poling with 50% duty cycle and periods ranging from 2 µm to 10 µm is achieved. The successful realization of periodic poling in BTO thin film unlocks the potential for highly efficient nonlinear processes under QPM that seemed far‐fetched with prior polycrystalline BTO thin films which predominantly relied on efficiency‐limited random or non‐phase matching conditions and is a key step toward integration of BTO photonic devices.https://doi.org/10.1002/advs.202406248barium titanate‐on‐insulatorsnonlinear frequency conversionnonlinear optical materialsoptoelectronicsperiodic polingquasi‐phase‐matching (QPM)
spellingShingle Pragati Aashna
Hong‐Lin Lin
Yu Cao
Yuhui Yin
Yuan Gao
Sakthi Sanjeev Mohanraj
Di Zhu
Aaron Danner
Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin Film
Advanced Science
barium titanate‐on‐insulators
nonlinear frequency conversion
nonlinear optical materials
optoelectronics
periodic poling
quasi‐phase‐matching (QPM)
title Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin Film
title_full Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin Film
title_fullStr Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin Film
title_full_unstemmed Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin Film
title_short Periodic Domain Inversion in Single Crystal Barium Titanate‐on‐Insulator Thin Film
title_sort periodic domain inversion in single crystal barium titanate on insulator thin film
topic barium titanate‐on‐insulators
nonlinear frequency conversion
nonlinear optical materials
optoelectronics
periodic poling
quasi‐phase‐matching (QPM)
url https://doi.org/10.1002/advs.202406248
work_keys_str_mv AT pragatiaashna periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm
AT honglinlin periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm
AT yucao periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm
AT yuhuiyin periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm
AT yuangao periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm
AT sakthisanjeevmohanraj periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm
AT dizhu periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm
AT aarondanner periodicdomaininversioninsinglecrystalbariumtitanateoninsulatorthinfilm