Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown ether

Tryptophan fulfills a plethora of important functions in nature both in its free form and as a component of peptides and proteins. Selective binding of tryptophan is therefore important for diagnostic and medicinal applications. Recently, we reported a glucose naphtho crown ether which is a chemosel...

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Main Authors: Gianpaolo Gallo, Bartosz Lewandowski
Format: Article
Language:English
Published: Beilstein-Institut 2025-03-01
Series:Beilstein Journal of Organic Chemistry
Subjects:
Online Access:https://doi.org/10.3762/bjoc.21.42
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author Gianpaolo Gallo
Bartosz Lewandowski
author_facet Gianpaolo Gallo
Bartosz Lewandowski
author_sort Gianpaolo Gallo
collection DOAJ
description Tryptophan fulfills a plethora of important functions in nature both in its free form and as a component of peptides and proteins. Selective binding of tryptophan is therefore important for diagnostic and medicinal applications. Recently, we reported a glucose naphtho crown ether which is a chemoselective receptor for the esters of aromatic amino acids, in particular tryptophan, in water. Herein, we demonstrate that the same compound also binds free tryptophan selectively in aqueous media. Furthermore, it is capable of binding to tryptophan within model tripeptides. The naphthalene functionality in the glucose-derived receptor enables the study of guest binding using fluorescence spectroscopy.
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spelling doaj-art-abf9600dfdda49b1b6fa76bd4db4bfda2025-08-20T01:54:19ZengBeilstein-InstitutBeilstein Journal of Organic Chemistry1860-53972025-03-0121154154610.3762/bjoc.21.421860-5397-21-42Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown etherGianpaolo Gallo0Bartosz Lewandowski1Laboratory of Organic Chemistry, ETH Zürich, Vladimir-Prelog-Weg 3, 8093 Zürich, Switzerland Laboratory of Organic Chemistry, ETH Zürich, Vladimir-Prelog-Weg 3, 8093 Zürich, Switzerland Tryptophan fulfills a plethora of important functions in nature both in its free form and as a component of peptides and proteins. Selective binding of tryptophan is therefore important for diagnostic and medicinal applications. Recently, we reported a glucose naphtho crown ether which is a chemoselective receptor for the esters of aromatic amino acids, in particular tryptophan, in water. Herein, we demonstrate that the same compound also binds free tryptophan selectively in aqueous media. Furthermore, it is capable of binding to tryptophan within model tripeptides. The naphthalene functionality in the glucose-derived receptor enables the study of guest binding using fluorescence spectroscopy.https://doi.org/10.3762/bjoc.21.42amino acidsmacrocyclic receptorsmolecular recognitionmonosaccharidestryptophan
spellingShingle Gianpaolo Gallo
Bartosz Lewandowski
Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown ether
Beilstein Journal of Organic Chemistry
amino acids
macrocyclic receptors
molecular recognition
monosaccharides
tryptophan
title Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown ether
title_full Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown ether
title_fullStr Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown ether
title_full_unstemmed Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown ether
title_short Binding of tryptophan and tryptophan-containing peptides in water by a glucose naphtho crown ether
title_sort binding of tryptophan and tryptophan containing peptides in water by a glucose naphtho crown ether
topic amino acids
macrocyclic receptors
molecular recognition
monosaccharides
tryptophan
url https://doi.org/10.3762/bjoc.21.42
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AT bartoszlewandowski bindingoftryptophanandtryptophancontainingpeptidesinwaterbyaglucosenaphthocrownether