The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical Determination

A sensing system of bisphenol A (BPA) based on the electrochemical detection utilizing molecularly imprinted polymer (MIP) as a receptor of BPA was investigated. MIP for BPA was polymerized thermally from 4-vinylpyridine as a functional monomer and ethylene dimethacrylate (EDMA) as a cross-linker an...

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Main Authors: Izumi Kubo, Nobuyuki Yokota, Yuko Nakane, Yusuke Fuchiwaki
Format: Article
Language:English
Published: Wiley 2011-01-01
Series:International Journal of Electrochemistry
Online Access:http://dx.doi.org/10.4061/2011/534936
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author Izumi Kubo
Nobuyuki Yokota
Yuko Nakane
Yusuke Fuchiwaki
author_facet Izumi Kubo
Nobuyuki Yokota
Yuko Nakane
Yusuke Fuchiwaki
author_sort Izumi Kubo
collection DOAJ
description A sensing system of bisphenol A (BPA) based on the electrochemical detection utilizing molecularly imprinted polymer (MIP) as a receptor of BPA was investigated. MIP for BPA was polymerized thermally from 4-vinylpyridine as a functional monomer and ethylene dimethacrylate (EDMA) as a cross-linker and served to prepare an MIP packed column. BPA in an aqueous solution was adsorbed to an MIP packed column and eluted by acetonitrile/phosphate buffer (60/40, v/v). From aqueous solution, BPA was adsorbed to the column and eluted completely in the eluent. The eluted BPA was electrochemically detected by cyclic voltammetry. Optimum pH and scan rate were 7.0 and 0.1 V/s in phosphate buffer. Electrochemical detection of BPA in acetonitrile/phosphate buffer was performed, and linear relationship between BPA and anodic peak current was observed at the range of 10–100 μM. In the eluent, anodic peak current of BPA was observed around 650 mV.
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issn 2090-3537
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publishDate 2011-01-01
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series International Journal of Electrochemistry
spelling doaj-art-aae1e5b7eb8540b58a66618cf6db7bdb2025-08-20T02:20:12ZengWileyInternational Journal of Electrochemistry2090-35372011-01-01201110.4061/2011/534936534936The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical DeterminationIzumi Kubo0Nobuyuki Yokota1Yuko Nakane2Yusuke Fuchiwaki3Department of Bioinformatics, Graduate School of Engineering, Soka University, 1-236, Tangi-cho, Hachioji, Tokyo 192-8577, JapanDepartment of Bioinformatics, Graduate School of Engineering, Soka University, 1-236, Tangi-cho, Hachioji, Tokyo 192-8577, JapanDepartment of Bioinformatics, Graduate School of Engineering, Soka University, 1-236, Tangi-cho, Hachioji, Tokyo 192-8577, JapanDepartment of Bioinformatics, Graduate School of Engineering, Soka University, 1-236, Tangi-cho, Hachioji, Tokyo 192-8577, JapanA sensing system of bisphenol A (BPA) based on the electrochemical detection utilizing molecularly imprinted polymer (MIP) as a receptor of BPA was investigated. MIP for BPA was polymerized thermally from 4-vinylpyridine as a functional monomer and ethylene dimethacrylate (EDMA) as a cross-linker and served to prepare an MIP packed column. BPA in an aqueous solution was adsorbed to an MIP packed column and eluted by acetonitrile/phosphate buffer (60/40, v/v). From aqueous solution, BPA was adsorbed to the column and eluted completely in the eluent. The eluted BPA was electrochemically detected by cyclic voltammetry. Optimum pH and scan rate were 7.0 and 0.1 V/s in phosphate buffer. Electrochemical detection of BPA in acetonitrile/phosphate buffer was performed, and linear relationship between BPA and anodic peak current was observed at the range of 10–100 μM. In the eluent, anodic peak current of BPA was observed around 650 mV.http://dx.doi.org/10.4061/2011/534936
spellingShingle Izumi Kubo
Nobuyuki Yokota
Yuko Nakane
Yusuke Fuchiwaki
The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical Determination
International Journal of Electrochemistry
title The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical Determination
title_full The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical Determination
title_fullStr The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical Determination
title_full_unstemmed The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical Determination
title_short The Establishment of Bisphenol A Sensing System Utilizing Molecularly Imprinted Polymer Receptor and Electrochemical Determination
title_sort establishment of bisphenol a sensing system utilizing molecularly imprinted polymer receptor and electrochemical determination
url http://dx.doi.org/10.4061/2011/534936
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