Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial Activity

Application of solid support, solvent free reaction condition and a dynamic microwave power system in the chemical synthesis of some novel 1, 3-diaryl-propenones has been described. A series of chalcones (3a-h) were synthesized by the condensation of 4-hydroxy-3,5-dinitroacetophenone with various su...

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Main Authors: K. L. Ameta, Biresh Kumar, Nitu S. Rathore
Format: Article
Language:English
Published: Wiley 2011-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2011/165047
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author K. L. Ameta
Biresh Kumar
Nitu S. Rathore
author_facet K. L. Ameta
Biresh Kumar
Nitu S. Rathore
author_sort K. L. Ameta
collection DOAJ
description Application of solid support, solvent free reaction condition and a dynamic microwave power system in the chemical synthesis of some novel 1, 3-diaryl-propenones has been described. A series of chalcones (3a-h) were synthesized by the condensation of 4-hydroxy-3,5-dinitroacetophenone with various substituted aromatic aldehydes in presence of montmorrilonite K10 as a catalyst and solid support media under microwave irradiation. The protocol offers several advantages such as simple procedure, fast reaction rate, mild reaction condition, eco-friendly and improved yield as compared to conventional methods. These compounds have been screened for their antibacterial and antifungal activities against different microorganisms. The structures of novel synthesized compounds have been established on the basis of elemental analysis, 1H NMR, 13C NMR and IR spectral data.
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spelling doaj-art-aa648e1e1c514d0dadbbbae0c7bcfed42025-08-20T02:20:54ZengWileyE-Journal of Chemistry0973-49452090-98102011-01-018266567010.1155/2011/165047Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial ActivityK. L. Ameta0Biresh Kumar1Nitu S. Rathore2Department of Chemistry, FASC Mody Institute of Technology & Science, (Deemed University) Lakshmangarh-332311, Rajasthan, IndiaDepartment of Chemistry, FASC Mody Institute of Technology & Science, (Deemed University) Lakshmangarh-332311, Rajasthan, IndiaDepartment of Chemistry, FASC Mody Institute of Technology & Science, (Deemed University) Lakshmangarh-332311, Rajasthan, IndiaApplication of solid support, solvent free reaction condition and a dynamic microwave power system in the chemical synthesis of some novel 1, 3-diaryl-propenones has been described. A series of chalcones (3a-h) were synthesized by the condensation of 4-hydroxy-3,5-dinitroacetophenone with various substituted aromatic aldehydes in presence of montmorrilonite K10 as a catalyst and solid support media under microwave irradiation. The protocol offers several advantages such as simple procedure, fast reaction rate, mild reaction condition, eco-friendly and improved yield as compared to conventional methods. These compounds have been screened for their antibacterial and antifungal activities against different microorganisms. The structures of novel synthesized compounds have been established on the basis of elemental analysis, 1H NMR, 13C NMR and IR spectral data.http://dx.doi.org/10.1155/2011/165047
spellingShingle K. L. Ameta
Biresh Kumar
Nitu S. Rathore
Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial Activity
E-Journal of Chemistry
title Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial Activity
title_full Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial Activity
title_fullStr Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial Activity
title_full_unstemmed Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial Activity
title_short Microwave Induced Improved Synthesis of Some Novel Substituted 1, 3-Diarylpropenones and their Antimicrobial Activity
title_sort microwave induced improved synthesis of some novel substituted 1 3 diarylpropenones and their antimicrobial activity
url http://dx.doi.org/10.1155/2011/165047
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