In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regeneration

Introduction: Chronic periodontitis is a complex combinatory disease that eventually upsets periodontal tissues, ultimately leading to tooth loss. In vertical bone loss defects, therapy includes surgical procedures, such as flap surgery with debridement associated with scaffolds, grafts, or membrane...

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Main Authors: Supraja G., S. Balaji Ganesh, Raja Kumar, Gurumoorthy Kaarthikeyan
Format: Article
Language:English
Published: Elsevier 2025-11-01
Series:Journal of Oral Biology and Craniofacial Research
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Online Access:http://www.sciencedirect.com/science/article/pii/S2212426825001903
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author Supraja G.
S. Balaji Ganesh
Raja Kumar
Gurumoorthy Kaarthikeyan
author_facet Supraja G.
S. Balaji Ganesh
Raja Kumar
Gurumoorthy Kaarthikeyan
author_sort Supraja G.
collection DOAJ
description Introduction: Chronic periodontitis is a complex combinatory disease that eventually upsets periodontal tissues, ultimately leading to tooth loss. In vertical bone loss defects, therapy includes surgical procedures, such as flap surgery with debridement associated with scaffolds, grafts, or membranes. The aim of the study is to fabricate a novel carrageenan, Calcium Magnesium Silicate (CaMgSiO), and ovine extracellular matrix (ECM)-based scaffold for periodontal bone regeneration. Materials and methods: To a 2 % carrageenan solution, 1 mg/mL of CaMgSiO and ECM was added. This homogenous solution was immersed in 0.15 M CaCl2 solution. The divalent cations (Ca+ 2 ions) were diffused into the gel and crosslinked to form a scaffold. The cross-linked scaffold (kappa carrageenan-CaMgSiO-ECM) was washed twice, underwent lyophilization and stored at 4 °C for further use. Scaffold characterization was done by means of X-ray diffraction (XRD), Raman spectrum, and scanning electron microscope (SEM), and energy dispersive spectroscopy (EDS). Then hemocompatibility assay, swelling analysis, and differentiation test were done to assess the biocompatibility of the scaffold. Result: Calcium was observed with a weight percentage of 16.7 %, silicate with 27.6 wt%, and magnesium with 2.8 wt% via EDS spectra. Kappa carrageenan, CaMgSiO + ECM scaffold has good agreement with red blood cells with a minimal lysis of 2 % at the concentration of 10 mg/mL, and the differentiation test showed maximum proliferation of cells. Conclusion: The novel CaMgSiO ECM scaffold significantly enhances cell proliferation; it is highly hemocompatible and has enhanced mineralization properties. Hence, incorporation of bioactive bioceramics induces stability as well as enhances the regeneration properties of the tendon-derived ECM.
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spelling doaj-art-a8f080419c2543dd96b65408acb14d212025-08-20T04:01:57ZengElsevierJournal of Oral Biology and Craniofacial Research2212-42682025-11-011561260126510.1016/j.jobcr.2025.08.011In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regenerationSupraja G.0S. Balaji Ganesh1Raja Kumar2Gurumoorthy Kaarthikeyan3Corresponding author.; Department of Periodontics, Saveetha Dental College and Hospitals, Saveetha Institute of Medical and Technical Sciences (SIMATS), Saveetha University, Chennai, 600077, Tamil Nadu, IndiaCorresponding author.; Department of Periodontics, Saveetha Dental College and Hospitals, Saveetha Institute of Medical and Technical Sciences (SIMATS), Saveetha University, Chennai, 600077, Tamil Nadu, IndiaDepartment of Periodontics, Saveetha Dental College and Hospitals, Saveetha Institute of Medical and Technical Sciences (SIMATS), Saveetha University, Chennai, 600077, Tamil Nadu, IndiaDepartment of Periodontics, Saveetha Dental College and Hospitals, Saveetha Institute of Medical and Technical Sciences (SIMATS), Saveetha University, Chennai, 600077, Tamil Nadu, IndiaIntroduction: Chronic periodontitis is a complex combinatory disease that eventually upsets periodontal tissues, ultimately leading to tooth loss. In vertical bone loss defects, therapy includes surgical procedures, such as flap surgery with debridement associated with scaffolds, grafts, or membranes. The aim of the study is to fabricate a novel carrageenan, Calcium Magnesium Silicate (CaMgSiO), and ovine extracellular matrix (ECM)-based scaffold for periodontal bone regeneration. Materials and methods: To a 2 % carrageenan solution, 1 mg/mL of CaMgSiO and ECM was added. This homogenous solution was immersed in 0.15 M CaCl2 solution. The divalent cations (Ca+ 2 ions) were diffused into the gel and crosslinked to form a scaffold. The cross-linked scaffold (kappa carrageenan-CaMgSiO-ECM) was washed twice, underwent lyophilization and stored at 4 °C for further use. Scaffold characterization was done by means of X-ray diffraction (XRD), Raman spectrum, and scanning electron microscope (SEM), and energy dispersive spectroscopy (EDS). Then hemocompatibility assay, swelling analysis, and differentiation test were done to assess the biocompatibility of the scaffold. Result: Calcium was observed with a weight percentage of 16.7 %, silicate with 27.6 wt%, and magnesium with 2.8 wt% via EDS spectra. Kappa carrageenan, CaMgSiO + ECM scaffold has good agreement with red blood cells with a minimal lysis of 2 % at the concentration of 10 mg/mL, and the differentiation test showed maximum proliferation of cells. Conclusion: The novel CaMgSiO ECM scaffold significantly enhances cell proliferation; it is highly hemocompatible and has enhanced mineralization properties. Hence, incorporation of bioactive bioceramics induces stability as well as enhances the regeneration properties of the tendon-derived ECM.http://www.sciencedirect.com/science/article/pii/S2212426825001903Tissue engineeringExtracellular matrixCarrageenanScaffoldPeriodontal regenerationDental
spellingShingle Supraja G.
S. Balaji Ganesh
Raja Kumar
Gurumoorthy Kaarthikeyan
In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regeneration
Journal of Oral Biology and Craniofacial Research
Tissue engineering
Extracellular matrix
Carrageenan
Scaffold
Periodontal regeneration
Dental
title In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regeneration
title_full In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regeneration
title_fullStr In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regeneration
title_full_unstemmed In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regeneration
title_short In-vitro evaluation of multicomponent scaffold with kappa carrageenan, tendon extracellular matrix and calcium-magnesium silicate for periodontal bone regeneration
title_sort in vitro evaluation of multicomponent scaffold with kappa carrageenan tendon extracellular matrix and calcium magnesium silicate for periodontal bone regeneration
topic Tissue engineering
Extracellular matrix
Carrageenan
Scaffold
Periodontal regeneration
Dental
url http://www.sciencedirect.com/science/article/pii/S2212426825001903
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AT rajakumar invitroevaluationofmulticomponentscaffoldwithkappacarrageenantendonextracellularmatrixandcalciummagnesiumsilicateforperiodontalboneregeneration
AT gurumoorthykaarthikeyan invitroevaluationofmulticomponentscaffoldwithkappacarrageenantendonextracellularmatrixandcalciummagnesiumsilicateforperiodontalboneregeneration