Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy

Summary: Metal halide perovskite (MHP) solar cells are promising aerospace power sources given their potential as inexpensive, lightweight, and resilient solar electricity generators. Herein, the intrinsic radiation tolerance of unencapsulated methylammonium lead iodide/chloride (CH3NH3PbI3-xClx) fi...

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Main Authors: Samuel Erickson, Calista Lum, Katie Stephens, Mritunjaya Parashar, Darshpreet Kaur Saini, Bibhudutta Rout, Cheol Park, Timothy J. Peshek, Lyndsey McMillon-Brown, Sayantani Ghosh
Format: Article
Language:English
Published: Elsevier 2025-01-01
Series:iScience
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Online Access:http://www.sciencedirect.com/science/article/pii/S258900422402813X
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author Samuel Erickson
Calista Lum
Katie Stephens
Mritunjaya Parashar
Darshpreet Kaur Saini
Bibhudutta Rout
Cheol Park
Timothy J. Peshek
Lyndsey McMillon-Brown
Sayantani Ghosh
author_facet Samuel Erickson
Calista Lum
Katie Stephens
Mritunjaya Parashar
Darshpreet Kaur Saini
Bibhudutta Rout
Cheol Park
Timothy J. Peshek
Lyndsey McMillon-Brown
Sayantani Ghosh
author_sort Samuel Erickson
collection DOAJ
description Summary: Metal halide perovskite (MHP) solar cells are promising aerospace power sources given their potential as inexpensive, lightweight, and resilient solar electricity generators. Herein, the intrinsic radiation tolerance of unencapsulated methylammonium lead iodide/chloride (CH3NH3PbI3-xClx) films was isolated. Spatially resolved photoluminescence (PL) spectroscopy and confocal microscopy revealed the fundamental defect physics through optical changes as films were irradiated with 4.5 MeV neutrons and 20 keV protons at fluences between 5×1010 and 1×1016 p+/cm2. As proton radiation increased beyond 1×1013 p+/cm2, defects formed in the film, causing both a decrease in photoluminescence intensity and a 30% increase in surface darkening. All proton irradiated films additionally exhibited continuous increase of energy bandgaps and decreasing charge recombination lifetimes with increasing proton fluences. These optical changes in the absorber layer precede performance declines detectable in standard current-voltage measurements of complete solar cell devices and therefore have the potential of serving as early indicators of radiation tolerance.
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spelling doaj-art-a8a4561212f64b95be2afa77700f7c002025-08-20T02:39:48ZengElsevieriScience2589-00422025-01-0128111158610.1016/j.isci.2024.111586Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopySamuel Erickson0Calista Lum1Katie Stephens2Mritunjaya Parashar3Darshpreet Kaur Saini4Bibhudutta Rout5Cheol Park6Timothy J. Peshek7Lyndsey McMillon-Brown8Sayantani Ghosh9Department of Physics, University of California, Merced, Merced, CA, USADepartment of Physics, University of California, Merced, Merced, CA, USAMaterials and Biomaterials Science and Engineering, University of California, Merced, Merced, CA, USADepartment of Physics, University of North Texas, Denton, TX, USADepartment of Physics, University of North Texas, Denton, TX, USADepartment of Physics, University of North Texas, Denton, TX, USAAdvanced Materials and Processing Branch, NASA Langley Research Center, Hampton, VA 23681, USAPhotovoltaic and Electrochemical Systems Branch, John H. Glenn Research Center, National Aeronautics and Space Administration, Cleveland, OH, USAPhotovoltaic and Electrochemical Systems Branch, John H. Glenn Research Center, National Aeronautics and Space Administration, Cleveland, OH, USADepartment of Physics, University of California, Merced, Merced, CA, USA; Corresponding authorSummary: Metal halide perovskite (MHP) solar cells are promising aerospace power sources given their potential as inexpensive, lightweight, and resilient solar electricity generators. Herein, the intrinsic radiation tolerance of unencapsulated methylammonium lead iodide/chloride (CH3NH3PbI3-xClx) films was isolated. Spatially resolved photoluminescence (PL) spectroscopy and confocal microscopy revealed the fundamental defect physics through optical changes as films were irradiated with 4.5 MeV neutrons and 20 keV protons at fluences between 5×1010 and 1×1016 p+/cm2. As proton radiation increased beyond 1×1013 p+/cm2, defects formed in the film, causing both a decrease in photoluminescence intensity and a 30% increase in surface darkening. All proton irradiated films additionally exhibited continuous increase of energy bandgaps and decreasing charge recombination lifetimes with increasing proton fluences. These optical changes in the absorber layer precede performance declines detectable in standard current-voltage measurements of complete solar cell devices and therefore have the potential of serving as early indicators of radiation tolerance.http://www.sciencedirect.com/science/article/pii/S258900422402813XPhysicsMaterials scienceEnergy materials
spellingShingle Samuel Erickson
Calista Lum
Katie Stephens
Mritunjaya Parashar
Darshpreet Kaur Saini
Bibhudutta Rout
Cheol Park
Timothy J. Peshek
Lyndsey McMillon-Brown
Sayantani Ghosh
Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy
iScience
Physics
Materials science
Energy materials
title Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy
title_full Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy
title_fullStr Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy
title_full_unstemmed Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy
title_short Elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy
title_sort elucidating early proton irradiation effects in metal halide perovskites via photoluminescence spectroscopy
topic Physics
Materials science
Energy materials
url http://www.sciencedirect.com/science/article/pii/S258900422402813X
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