Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties

This study explores the dynamic interaction between environmentally sustainable plasma enhancer and quencher agents during the incorporation of SiO2 into a TiO2 layer, with the primary objective of simultaneously augmenting protective and bioactive attributes. This enhancement is realized through th...

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Main Authors: Mosab Kaseem, Ananda Repycha Safira, Mohammad Aadil, Han-Choel Choe
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2024-10-01
Series:Nano Materials Science
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Online Access:http://www.sciencedirect.com/science/article/pii/S2589965124000035
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author Mosab Kaseem
Ananda Repycha Safira
Mohammad Aadil
Han-Choel Choe
author_facet Mosab Kaseem
Ananda Repycha Safira
Mohammad Aadil
Han-Choel Choe
author_sort Mosab Kaseem
collection DOAJ
description This study explores the dynamic interaction between environmentally sustainable plasma enhancer and quencher agents during the incorporation of SiO2 into a TiO2 layer, with the primary objective of simultaneously augmenting protective and bioactive attributes. This enhancement is realized through the synergistic utilization of Tetraethyl orthosilicate (TE) and Stevia (ST) within a plasma-assisted oxidation process. To achieve this goal, Ti–6Al–4V alloy underwent oxidation in an electrolyte solution containing acetate-glycerophosphate, with the addition of TE and ST separately and in combination. TE, as a silicon oxide (SiO2) precursor, facilitates the creation of a calcium-rich, rough, porous layer by undergoing hydrolysis to generate silanol groups (Si–OH), which subsequently condense into silicon-oxygen-silicon (Si–O–Si) bonds, resulting in SiO2 formation. In contrast, ST acts as a plasma quencher, absorbing highly reactive plasma species during the oxidation process, reducing energy levels, and diminishing sparking intensity. The combination of TE and ST results in moderate sparking, balancing Stevia's quenching effect and TE's sparking influence. As a result, this coating exhibits enhanced corrosion resistance and bioactivity compared to using either ST or TE alone. The study highlights the potential of this synergistic approach for advanced TiO2-based coatings.
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issn 2589-9651
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publishDate 2024-10-01
publisher KeAi Communications Co., Ltd.
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series Nano Materials Science
spelling doaj-art-a84aa7e8dfd04e2191e671d063c09c832025-08-20T02:06:44ZengKeAi Communications Co., Ltd.Nano Materials Science2589-96512024-10-016559661010.1016/j.nanoms.2024.01.003Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive propertiesMosab Kaseem0Ananda Repycha Safira1Mohammad Aadil2Han-Choel Choe3Corrosion and Electrochemistry Laboratory, Department of Nanotechnology and Advanced Materials Engineering, Sejong University, Seoul, 05006, South KoreaCorrosion and Electrochemistry Laboratory, Department of Nanotechnology and Advanced Materials Engineering, Sejong University, Seoul, 05006, South KoreaCorrosion and Electrochemistry Laboratory, Department of Nanotechnology and Advanced Materials Engineering, Sejong University, Seoul, 05006, South KoreaAdvanced Functional Surface and Biomaterials Research Lab, Department of Dental Materials and Research Center of Surface Control for Oral Tissue Regeneration (BRL Center of NRF), Convergence Research Center for Treatment of Oral Soft Tissue Disease (MRC), College of Dentistry, Chosun University, Gwangju, 61452, South Korea; Corresponding author.This study explores the dynamic interaction between environmentally sustainable plasma enhancer and quencher agents during the incorporation of SiO2 into a TiO2 layer, with the primary objective of simultaneously augmenting protective and bioactive attributes. This enhancement is realized through the synergistic utilization of Tetraethyl orthosilicate (TE) and Stevia (ST) within a plasma-assisted oxidation process. To achieve this goal, Ti–6Al–4V alloy underwent oxidation in an electrolyte solution containing acetate-glycerophosphate, with the addition of TE and ST separately and in combination. TE, as a silicon oxide (SiO2) precursor, facilitates the creation of a calcium-rich, rough, porous layer by undergoing hydrolysis to generate silanol groups (Si–OH), which subsequently condense into silicon-oxygen-silicon (Si–O–Si) bonds, resulting in SiO2 formation. In contrast, ST acts as a plasma quencher, absorbing highly reactive plasma species during the oxidation process, reducing energy levels, and diminishing sparking intensity. The combination of TE and ST results in moderate sparking, balancing Stevia's quenching effect and TE's sparking influence. As a result, this coating exhibits enhanced corrosion resistance and bioactivity compared to using either ST or TE alone. The study highlights the potential of this synergistic approach for advanced TiO2-based coatings.http://www.sciencedirect.com/science/article/pii/S2589965124000035Ti–6Al–4V alloyPlasma quencherHydrolysisCorrosionBioactivity
spellingShingle Mosab Kaseem
Ananda Repycha Safira
Mohammad Aadil
Han-Choel Choe
Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties
Nano Materials Science
Ti–6Al–4V alloy
Plasma quencher
Hydrolysis
Corrosion
Bioactivity
title Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties
title_full Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties
title_fullStr Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties
title_full_unstemmed Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties
title_short Chemical incorporation of SiO2 into TiO2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties
title_sort chemical incorporation of sio2 into tio2 layer by green plasma enhancer and quencher agents for synchronized improvements in the protective and bioactive properties
topic Ti–6Al–4V alloy
Plasma quencher
Hydrolysis
Corrosion
Bioactivity
url http://www.sciencedirect.com/science/article/pii/S2589965124000035
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AT anandarepychasafira chemicalincorporationofsio2intotio2layerbygreenplasmaenhancerandquencheragentsforsynchronizedimprovementsintheprotectiveandbioactiveproperties
AT mohammadaadil chemicalincorporationofsio2intotio2layerbygreenplasmaenhancerandquencheragentsforsynchronizedimprovementsintheprotectiveandbioactiveproperties
AT hanchoelchoe chemicalincorporationofsio2intotio2layerbygreenplasmaenhancerandquencheragentsforsynchronizedimprovementsintheprotectiveandbioactiveproperties