A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline Hydrochloride

The harmful effects of antibiotics on aquatic environments have become a growing concern of modern society. Developing high-performance photocatalysts capable of degrading antibiotics under solar light is, therefore, crucial. In this study, TiO<sub>2</sub>-cuttlebone composites are prepa...

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Main Authors: Qing Li, Penghui Liu, Huizhen Lin, Hun Xue, Jingyun Mao
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:Inorganics
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Online Access:https://www.mdpi.com/2304-6740/12/12/319
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author Qing Li
Penghui Liu
Huizhen Lin
Hun Xue
Jingyun Mao
author_facet Qing Li
Penghui Liu
Huizhen Lin
Hun Xue
Jingyun Mao
author_sort Qing Li
collection DOAJ
description The harmful effects of antibiotics on aquatic environments have become a growing concern of modern society. Developing high-performance photocatalysts capable of degrading antibiotics under solar light is, therefore, crucial. In this study, TiO<sub>2</sub>-cuttlebone composites are prepared via the sol–gel method, to produce carbonate radicals (•CO<sub>3</sub><sup>−</sup>) under solar light irradiation. The •CO<sub>3</sub><sup>−</sup> radicals exhibit high selectivity for the degradation of tetracycline hydrochloride (TC). Compared to TiO<sub>2</sub> alone, the TiO<sub>2</sub>-cuttlebone composite demonstrates excellent solar-driven photocatalytic activity for TC degradation in both freshwater and seawater. The reaction pathways of TC degradation in seawater are elucidated using HPLC-MS/MS analysis. Moreover, a TiO<sub>2</sub>-cuttlebone self-suspending photocatalyst device is fabricated using 3D printing technology and low-temperature deposition methods, with aluminum–plastic (AP) as a substrate. This innovative device is easily recyclable from photocatalytic solutions while maintaining high stability, making it highly desirable for practical applications.
format Article
id doaj-art-a70d7cfd94f04241a1795f3544962c6f
institution DOAJ
issn 2304-6740
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publishDate 2024-12-01
publisher MDPI AG
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series Inorganics
spelling doaj-art-a70d7cfd94f04241a1795f3544962c6f2025-08-20T02:57:08ZengMDPI AGInorganics2304-67402024-12-01121231910.3390/inorganics12120319A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline HydrochlorideQing Li0Penghui Liu1Huizhen Lin2Hun Xue3Jingyun Mao4College of Environmental and Resource Sciences, College of Carbon Neutral Modern Industry, Fujian Normal University, Fuzhou 350007, ChinaCollege of Environmental and Resource Sciences, College of Carbon Neutral Modern Industry, Fujian Normal University, Fuzhou 350007, ChinaCollege of Environmental and Resource Sciences, College of Carbon Neutral Modern Industry, Fujian Normal University, Fuzhou 350007, ChinaCollege of Environmental and Resource Sciences, College of Carbon Neutral Modern Industry, Fujian Normal University, Fuzhou 350007, ChinaCollege of Environmental and Resource Sciences, College of Carbon Neutral Modern Industry, Fujian Normal University, Fuzhou 350007, ChinaThe harmful effects of antibiotics on aquatic environments have become a growing concern of modern society. Developing high-performance photocatalysts capable of degrading antibiotics under solar light is, therefore, crucial. In this study, TiO<sub>2</sub>-cuttlebone composites are prepared via the sol–gel method, to produce carbonate radicals (•CO<sub>3</sub><sup>−</sup>) under solar light irradiation. The •CO<sub>3</sub><sup>−</sup> radicals exhibit high selectivity for the degradation of tetracycline hydrochloride (TC). Compared to TiO<sub>2</sub> alone, the TiO<sub>2</sub>-cuttlebone composite demonstrates excellent solar-driven photocatalytic activity for TC degradation in both freshwater and seawater. The reaction pathways of TC degradation in seawater are elucidated using HPLC-MS/MS analysis. Moreover, a TiO<sub>2</sub>-cuttlebone self-suspending photocatalyst device is fabricated using 3D printing technology and low-temperature deposition methods, with aluminum–plastic (AP) as a substrate. This innovative device is easily recyclable from photocatalytic solutions while maintaining high stability, making it highly desirable for practical applications.https://www.mdpi.com/2304-6740/12/12/319TiO<sub>2</sub>-cuttlebonecarbonate radicalphotocatalysistetracycline hydrochlorideseawaterself-suspending
spellingShingle Qing Li
Penghui Liu
Huizhen Lin
Hun Xue
Jingyun Mao
A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline Hydrochloride
Inorganics
TiO<sub>2</sub>-cuttlebone
carbonate radical
photocatalysis
tetracycline hydrochloride
seawater
self-suspending
title A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline Hydrochloride
title_full A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline Hydrochloride
title_fullStr A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline Hydrochloride
title_full_unstemmed A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline Hydrochloride
title_short A Novel TiO<sub>2</sub>-Cuttlebone Photocatalyst for Highly Efficient Catalytic Degradation of Tetracycline Hydrochloride
title_sort novel tio sub 2 sub cuttlebone photocatalyst for highly efficient catalytic degradation of tetracycline hydrochloride
topic TiO<sub>2</sub>-cuttlebone
carbonate radical
photocatalysis
tetracycline hydrochloride
seawater
self-suspending
url https://www.mdpi.com/2304-6740/12/12/319
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