Thermal Behavior of a Natural Sepiolite from Northeastern Iran

Sepiolite deposits have been recently discovered in northeastern Iran. However, there is still little information about its physicochemical and mineralogical characteristics. Therefore, the collapse of the sepiolite (with sizes of < 63 μm) structure induced by temperature elevation in an electric...

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Main Authors: S. Hojati, H. Khademi
Format: Article
Language:English
Published: University of Tehran 2013-06-01
Series:Journal of Sciences, Islamic Republic of Iran
Subjects:
Online Access:https://jsciences.ut.ac.ir/article_32079_cd5d5e8f5495ae3b3801827a36d7e309.pdf
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author S. Hojati
H. Khademi
author_facet S. Hojati
H. Khademi
author_sort S. Hojati
collection DOAJ
description Sepiolite deposits have been recently discovered in northeastern Iran. However, there is still little information about its physicochemical and mineralogical characteristics. Therefore, the collapse of the sepiolite (with sizes of < 63 μm) structure induced by temperature elevation in an electric furnace at 350, 550, and 850 °C for 4 hours was studied using X-ray diffraction (XRD) in combination with Thermogravimetric analysis (TGA) and infrared spectroscopic analysis. Results showed that the main mineral constituent of the samples is a well crystallized sepiolite. However, dolomite and quartz were also present in minor amounts. Results also revealed that with temperature different phases including ‘sepiolite dihydrite’, ‘sepiolite anhydrite’ and ‘enstatite’ were formed, as magnesium coordinated water and octahedrically coordinated hydroxyl groups, were eliminated and the dehydroxylated phase was recrystallized to enstatite, a stable form of magnesium silicate (MgSiO3).
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spelling doaj-art-a596dc1b130c40018891e455e5f3b7da2025-08-20T02:25:53ZengUniversity of TehranJournal of Sciences, Islamic Republic of Iran1016-11042345-69142013-06-0124212913432079Thermal Behavior of a Natural Sepiolite from Northeastern IranS. Hojati0H. Khademi1Department of Soil Science, College of Agriculture, Shahid Chamran University, Ahvaz 6135783151, Khuzestan, Islamic Republic of IranDepartment of Soil Science, College of Agriculture, Isfahan University of Technology, Isfahan 8415683111, Isfahan, Islamic Republic of IranSepiolite deposits have been recently discovered in northeastern Iran. However, there is still little information about its physicochemical and mineralogical characteristics. Therefore, the collapse of the sepiolite (with sizes of < 63 μm) structure induced by temperature elevation in an electric furnace at 350, 550, and 850 °C for 4 hours was studied using X-ray diffraction (XRD) in combination with Thermogravimetric analysis (TGA) and infrared spectroscopic analysis. Results showed that the main mineral constituent of the samples is a well crystallized sepiolite. However, dolomite and quartz were also present in minor amounts. Results also revealed that with temperature different phases including ‘sepiolite dihydrite’, ‘sepiolite anhydrite’ and ‘enstatite’ were formed, as magnesium coordinated water and octahedrically coordinated hydroxyl groups, were eliminated and the dehydroxylated phase was recrystallized to enstatite, a stable form of magnesium silicate (MgSiO3).https://jsciences.ut.ac.ir/article_32079_cd5d5e8f5495ae3b3801827a36d7e309.pdfsepioliteenstatitezeolitic waterinfrared spectroscopy
spellingShingle S. Hojati
H. Khademi
Thermal Behavior of a Natural Sepiolite from Northeastern Iran
Journal of Sciences, Islamic Republic of Iran
sepiolite
enstatite
zeolitic water
infrared spectroscopy
title Thermal Behavior of a Natural Sepiolite from Northeastern Iran
title_full Thermal Behavior of a Natural Sepiolite from Northeastern Iran
title_fullStr Thermal Behavior of a Natural Sepiolite from Northeastern Iran
title_full_unstemmed Thermal Behavior of a Natural Sepiolite from Northeastern Iran
title_short Thermal Behavior of a Natural Sepiolite from Northeastern Iran
title_sort thermal behavior of a natural sepiolite from northeastern iran
topic sepiolite
enstatite
zeolitic water
infrared spectroscopy
url https://jsciences.ut.ac.ir/article_32079_cd5d5e8f5495ae3b3801827a36d7e309.pdf
work_keys_str_mv AT shojati thermalbehaviorofanaturalsepiolitefromnortheasterniran
AT hkhademi thermalbehaviorofanaturalsepiolitefromnortheasterniran