Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method
In this study,the nanoparticles of zinc oxide were readily prepared through Hydrothermal process by using zinc nitrate hexahydrate, and Sodium hydroxide as aprecursors. The surface topology, and crystalline structure of prepared ZnO nanoparticles were studied. X-ray diffraction (XRD) revealed that...
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| Format: | Article |
| Language: | English |
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Tikrit University
2019-05-01
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| Series: | Tikrit Journal of Pure Science |
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| Online Access: | https://tjpsj.org/index.php/tjps/article/view/374 |
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| author | Mohammed Ajmi Abd Khalid Hamdi Razeg Raad M.S Al-haddad |
| author_facet | Mohammed Ajmi Abd Khalid Hamdi Razeg Raad M.S Al-haddad |
| author_sort | Mohammed Ajmi Abd |
| collection | DOAJ |
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In this study,the nanoparticles of zinc oxide were readily prepared through Hydrothermal process by using zinc nitrate hexahydrate, and Sodium hydroxide as aprecursors. The surface topology, and crystalline structure of prepared ZnO nanoparticles were studied. X-ray diffraction (XRD) revealed that the prepared ZnO nano particles is highly crystalline, having (wurtzite) crystal structure. The optical analysis by UV–vis showed that these ZnO nano particles have considerable blue shift in the optical band gap energy (Eg = 4.9eV), and this may be to the quantum confinement effect of nano particles. The FT-IR results shows the existence of OH, COO, H2O groups the characteristic vibrational modes of Zn–O were identified. and AFM analysis showed that the diameters of the ZnO particles is in ananometer range of (70-74)nm
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| format | Article |
| id | doaj-art-a4c40c260c724f8d97f7c1547c6850bf |
| institution | OA Journals |
| issn | 1813-1662 2415-1726 |
| language | English |
| publishDate | 2019-05-01 |
| publisher | Tikrit University |
| record_format | Article |
| series | Tikrit Journal of Pure Science |
| spelling | doaj-art-a4c40c260c724f8d97f7c1547c6850bf2025-08-20T02:37:10ZengTikrit UniversityTikrit Journal of Pure Science1813-16622415-17262019-05-0124310.25130/tjps.v24i3.374 Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal MethodMohammed Ajmi AbdKhalid Hamdi RazegRaad M.S Al-haddad In this study,the nanoparticles of zinc oxide were readily prepared through Hydrothermal process by using zinc nitrate hexahydrate, and Sodium hydroxide as aprecursors. The surface topology, and crystalline structure of prepared ZnO nanoparticles were studied. X-ray diffraction (XRD) revealed that the prepared ZnO nano particles is highly crystalline, having (wurtzite) crystal structure. The optical analysis by UV–vis showed that these ZnO nano particles have considerable blue shift in the optical band gap energy (Eg = 4.9eV), and this may be to the quantum confinement effect of nano particles. The FT-IR results shows the existence of OH, COO, H2O groups the characteristic vibrational modes of Zn–O were identified. and AFM analysis showed that the diameters of the ZnO particles is in ananometer range of (70-74)nm https://tjpsj.org/index.php/tjps/article/view/374Hydrothermal processPrecursorZnO NanoparticleXrayAFMUV technique |
| spellingShingle | Mohammed Ajmi Abd Khalid Hamdi Razeg Raad M.S Al-haddad Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method Tikrit Journal of Pure Science Hydrothermal process Precursor ZnO Nanoparticle Xray AFM UV technique |
| title | Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method |
| title_full | Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method |
| title_fullStr | Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method |
| title_full_unstemmed | Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method |
| title_short | Preparation and Characterization of Zno Nano particles Prepared by Hydrothermal Method |
| title_sort | preparation and characterization of zno nano particles prepared by hydrothermal method |
| topic | Hydrothermal process Precursor ZnO Nanoparticle Xray AFM UV technique |
| url | https://tjpsj.org/index.php/tjps/article/view/374 |
| work_keys_str_mv | AT mohammedajmiabd preparationandcharacterizationofznonanoparticlespreparedbyhydrothermalmethod AT khalidhamdirazeg preparationandcharacterizationofznonanoparticlespreparedbyhydrothermalmethod AT raadmsalhaddad preparationandcharacterizationofznonanoparticlespreparedbyhydrothermalmethod |