Impact of solvent on the solution-processed hole transport layer deposition in organic solar cells

Recently, the solution-processed copper[I] iodide (CuI) thin film deposition has been identified as an important hole transport layer (HTL) in excitonic solar cells. Further, we explored the potential of CuI as an efficient HTL and introduced a range of solvents compatible with CuI for the preparati...

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Main Authors: Neeraj Chaudhary, Rashi Kedia, Manisha Khatak, Manisha Balkhandia, Asit Patra
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Next Materials
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Online Access:http://www.sciencedirect.com/science/article/pii/S2949822825001558
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author Neeraj Chaudhary
Rashi Kedia
Manisha Khatak
Manisha Balkhandia
Asit Patra
author_facet Neeraj Chaudhary
Rashi Kedia
Manisha Khatak
Manisha Balkhandia
Asit Patra
author_sort Neeraj Chaudhary
collection DOAJ
description Recently, the solution-processed copper[I] iodide (CuI) thin film deposition has been identified as an important hole transport layer (HTL) in excitonic solar cells. Further, we explored the potential of CuI as an efficient HTL and introduced a range of solvents compatible with CuI for the preparation of organic solar cells. This work investigates the impact of various solvent on physical properties of CuI. Eight solvents namely; cyclohexane, carbon tetrachloride (CCl4), benzene, tetrahydrofuran, dichloromethane, acetonitrile, dimethoxy sulfoxide (DMSO) and water (H2O) were selected for density functional calculations and for that purpose we used the basis set B3LYP/3-21 g to access the impact of solvents on energy levels, charge distribution and atomic distance within CuI. Based on the computational results, hydrophilic organic solvents DMSO along with N,N-dimethylformamide (DMF), and diisopropyl sulphide (DPS) were chosen to dissolve CuI for the solution-processed HTL. The HTL formed from these three solvents were analysed using UV–vis–NIR spectroscopy, cyclic voltammetry, X-ray diffraction and scanning electron microscope (SEM) to get the better understanding of their electrical, optical and morphological behaviour. To evaluate the effectiveness of this HTL material employing different solvents, two active layers PTB7:PC71BM and PCDTBT:PC71BM were tested with the device configuration ITO/CuI/active layer/Al. Our results indicate that the choice of solvent for the HTL deposition significantly influence the photovoltaic performance with DMSO as a solvent achieving the highest power conversion efficiency (PCE) of ̴ 4.28 % in this particular case for CuI which is due to the more crystalline film yielded with DMSO under ambient conditions.
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spelling doaj-art-a3eb38199dda4a54ab874e25b5d44b972025-08-20T02:11:54ZengElsevierNext Materials2949-82282025-07-01810063710.1016/j.nxmate.2025.100637Impact of solvent on the solution-processed hole transport layer deposition in organic solar cellsNeeraj Chaudhary0Rashi Kedia1Manisha Khatak2Manisha Balkhandia3Asit Patra4Photovoltaic Metrology Section, Advanced Material and Device Metrology Division, CSR-National Physical Laboratory, Dr K. S. Krishnan Marg, New Delhi 110012, IndiaPhotovoltaic Metrology Section, Advanced Material and Device Metrology Division, CSR-National Physical Laboratory, Dr K. S. Krishnan Marg, New Delhi 110012, IndiaPhotovoltaic Metrology Section, Advanced Material and Device Metrology Division, CSR-National Physical Laboratory, Dr K. S. Krishnan Marg, New Delhi 110012, IndiaPhotovoltaic Metrology Section, Advanced Material and Device Metrology Division, CSR-National Physical Laboratory, Dr K. S. Krishnan Marg, New Delhi 110012, IndiaCorresponding author.; Photovoltaic Metrology Section, Advanced Material and Device Metrology Division, CSR-National Physical Laboratory, Dr K. S. Krishnan Marg, New Delhi 110012, IndiaRecently, the solution-processed copper[I] iodide (CuI) thin film deposition has been identified as an important hole transport layer (HTL) in excitonic solar cells. Further, we explored the potential of CuI as an efficient HTL and introduced a range of solvents compatible with CuI for the preparation of organic solar cells. This work investigates the impact of various solvent on physical properties of CuI. Eight solvents namely; cyclohexane, carbon tetrachloride (CCl4), benzene, tetrahydrofuran, dichloromethane, acetonitrile, dimethoxy sulfoxide (DMSO) and water (H2O) were selected for density functional calculations and for that purpose we used the basis set B3LYP/3-21 g to access the impact of solvents on energy levels, charge distribution and atomic distance within CuI. Based on the computational results, hydrophilic organic solvents DMSO along with N,N-dimethylformamide (DMF), and diisopropyl sulphide (DPS) were chosen to dissolve CuI for the solution-processed HTL. The HTL formed from these three solvents were analysed using UV–vis–NIR spectroscopy, cyclic voltammetry, X-ray diffraction and scanning electron microscope (SEM) to get the better understanding of their electrical, optical and morphological behaviour. To evaluate the effectiveness of this HTL material employing different solvents, two active layers PTB7:PC71BM and PCDTBT:PC71BM were tested with the device configuration ITO/CuI/active layer/Al. Our results indicate that the choice of solvent for the HTL deposition significantly influence the photovoltaic performance with DMSO as a solvent achieving the highest power conversion efficiency (PCE) of ̴ 4.28 % in this particular case for CuI which is due to the more crystalline film yielded with DMSO under ambient conditions.http://www.sciencedirect.com/science/article/pii/S2949822825001558CuIComputational studiesSolution-processableHole transport materialThin film depositionSolvent effect
spellingShingle Neeraj Chaudhary
Rashi Kedia
Manisha Khatak
Manisha Balkhandia
Asit Patra
Impact of solvent on the solution-processed hole transport layer deposition in organic solar cells
Next Materials
CuI
Computational studies
Solution-processable
Hole transport material
Thin film deposition
Solvent effect
title Impact of solvent on the solution-processed hole transport layer deposition in organic solar cells
title_full Impact of solvent on the solution-processed hole transport layer deposition in organic solar cells
title_fullStr Impact of solvent on the solution-processed hole transport layer deposition in organic solar cells
title_full_unstemmed Impact of solvent on the solution-processed hole transport layer deposition in organic solar cells
title_short Impact of solvent on the solution-processed hole transport layer deposition in organic solar cells
title_sort impact of solvent on the solution processed hole transport layer deposition in organic solar cells
topic CuI
Computational studies
Solution-processable
Hole transport material
Thin film deposition
Solvent effect
url http://www.sciencedirect.com/science/article/pii/S2949822825001558
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AT manishakhatak impactofsolventonthesolutionprocessedholetransportlayerdepositioninorganicsolarcells
AT manishabalkhandia impactofsolventonthesolutionprocessedholetransportlayerdepositioninorganicsolarcells
AT asitpatra impactofsolventonthesolutionprocessedholetransportlayerdepositioninorganicsolarcells