Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp Powder

Spray drying (SD) is widely used for fruit powder production, but hygroscopic compounds can affect flowability and cause stickiness. This study evaluated rice protein and rice starch as encapsulating agents during SD of blueberry pulp (BPP and BPS, respectively), combined with ozone aeration (BPP-O3...

Full description

Saved in:
Bibliographic Details
Main Authors: Newton C. Santos, Raphael L. J. Almeida, Anna E. S. Tomé, Fábio G. Teles, Railene H. C. R. Araújo, Juanne Q. Farias, Maria T. S. d. Fonseca, Virgínia M. d. A. Silva, Victor H. d. A. Ribeiro, Márcia R. d. S. Pedrini, Josivanda P. Gomes, Ana P. T. Rocha
Format: Article
Language:English
Published: MDPI AG 2025-04-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/14/8/1419
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850180128281198592
author Newton C. Santos
Raphael L. J. Almeida
Anna E. S. Tomé
Fábio G. Teles
Railene H. C. R. Araújo
Juanne Q. Farias
Maria T. S. d. Fonseca
Virgínia M. d. A. Silva
Victor H. d. A. Ribeiro
Márcia R. d. S. Pedrini
Josivanda P. Gomes
Ana P. T. Rocha
author_facet Newton C. Santos
Raphael L. J. Almeida
Anna E. S. Tomé
Fábio G. Teles
Railene H. C. R. Araújo
Juanne Q. Farias
Maria T. S. d. Fonseca
Virgínia M. d. A. Silva
Victor H. d. A. Ribeiro
Márcia R. d. S. Pedrini
Josivanda P. Gomes
Ana P. T. Rocha
author_sort Newton C. Santos
collection DOAJ
description Spray drying (SD) is widely used for fruit powder production, but hygroscopic compounds can affect flowability and cause stickiness. This study evaluated rice protein and rice starch as encapsulating agents during SD of blueberry pulp (BPP and BPS, respectively), combined with ozone aeration (BPP-O3 and BPS-O3), focusing on physical, morphological, structural, and bioactive properties, as well as 56-day stability. The process yield was 55.26% (BPP) and 52.5% (BPS) (<i>p</i> < 0.05). All microparticles had low moisture (<5.03%) and water activity (<0.21%). BPP had higher phenolic (308.60 mg GAE/100 g) and anthocyanin content (85.26 mg/100 g), while BPS had more flavonoids (33.84 mg CE/100 g). Ozone treatment increased solubility (89.10–91.27%) and reduced hygroscopicity (9.25–10.06%). Morphological analysis revealed that BPP produced smaller, uniform particles (11.70 µm), whereas BPS generated larger (16.67 µm) and more agglomerated particles. Ozone improved sphericity, reduced agglomeration, and enhanced flow properties. FT-IR analysis indicated no new functional groups but a reduction in absorbance bands. Ozone also enhanced the stability of bioactive compounds, reducing anthocyanin and flavonoid degradation over 56 days. Overall, BPP-O3 is a promising approach for producing functional powders with enhanced stability and physical properties, suitable for food applications.
format Article
id doaj-art-a3b69877e1364dcfa479b73f9dc30d7e
institution OA Journals
issn 2304-8158
language English
publishDate 2025-04-01
publisher MDPI AG
record_format Article
series Foods
spelling doaj-art-a3b69877e1364dcfa479b73f9dc30d7e2025-08-20T02:18:16ZengMDPI AGFoods2304-81582025-04-01148141910.3390/foods14081419Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp PowderNewton C. Santos0Raphael L. J. Almeida1Anna E. S. Tomé2Fábio G. Teles3Railene H. C. R. Araújo4Juanne Q. Farias5Maria T. S. d. Fonseca6Virgínia M. d. A. Silva7Victor H. d. A. Ribeiro8Márcia R. d. S. Pedrini9Josivanda P. Gomes10Ana P. T. Rocha11Laboratório de Processamento de Biomassa, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilLaboratório de Engenharia Bioquímica, Universidade Federal do Rio Grande do Norte, Natal 59078-970, RN, BrazilLaboratório de Processamento de Biomassa, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilLaboratório de Qualidade e Processamento de Alimentos de Origem Vegetal, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilLaboratório de Qualidade e Processamento de Alimentos de Origem Vegetal, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilLaboratório de Processamento e Armazenamento de Produtos Agrícolas, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilLaboratório de Processamento de Biomassa, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilFaculdade de Engenharia de Alimentos, Universidade Estadual de Campinas, Campinas 13083-872, SP, BrazilCentro de Ciências Humanas, Sociais e Agrárias, Universidade Federal da Paraíba, Bananeiras 58051-900, PB, BrazilLaboratório de Bioprocessos, Universidade Federal do Rio Grande do Norte, Natal 59078-970, RN, BrazilLaboratório de Processamento e Armazenamento de Produtos Agrícolas, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilLaboratório de Processamento de Biomassa, Universidade Federal de Campina Grande, Campina Grande 58429-900, PB, BrazilSpray drying (SD) is widely used for fruit powder production, but hygroscopic compounds can affect flowability and cause stickiness. This study evaluated rice protein and rice starch as encapsulating agents during SD of blueberry pulp (BPP and BPS, respectively), combined with ozone aeration (BPP-O3 and BPS-O3), focusing on physical, morphological, structural, and bioactive properties, as well as 56-day stability. The process yield was 55.26% (BPP) and 52.5% (BPS) (<i>p</i> < 0.05). All microparticles had low moisture (<5.03%) and water activity (<0.21%). BPP had higher phenolic (308.60 mg GAE/100 g) and anthocyanin content (85.26 mg/100 g), while BPS had more flavonoids (33.84 mg CE/100 g). Ozone treatment increased solubility (89.10–91.27%) and reduced hygroscopicity (9.25–10.06%). Morphological analysis revealed that BPP produced smaller, uniform particles (11.70 µm), whereas BPS generated larger (16.67 µm) and more agglomerated particles. Ozone improved sphericity, reduced agglomeration, and enhanced flow properties. FT-IR analysis indicated no new functional groups but a reduction in absorbance bands. Ozone also enhanced the stability of bioactive compounds, reducing anthocyanin and flavonoid degradation over 56 days. Overall, BPP-O3 is a promising approach for producing functional powders with enhanced stability and physical properties, suitable for food applications.https://www.mdpi.com/2304-8158/14/8/1419green technologydrying agentsrice starchrice proteinfruit pulp powder
spellingShingle Newton C. Santos
Raphael L. J. Almeida
Anna E. S. Tomé
Fábio G. Teles
Railene H. C. R. Araújo
Juanne Q. Farias
Maria T. S. d. Fonseca
Virgínia M. d. A. Silva
Victor H. d. A. Ribeiro
Márcia R. d. S. Pedrini
Josivanda P. Gomes
Ana P. T. Rocha
Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp Powder
Foods
green technology
drying agents
rice starch
rice protein
fruit pulp powder
title Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp Powder
title_full Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp Powder
title_fullStr Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp Powder
title_full_unstemmed Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp Powder
title_short Ozone Aeration Enhance Flowability, Structure, and Antioxidant Activity in Blueberry Pulp Powder
title_sort ozone aeration enhance flowability structure and antioxidant activity in blueberry pulp powder
topic green technology
drying agents
rice starch
rice protein
fruit pulp powder
url https://www.mdpi.com/2304-8158/14/8/1419
work_keys_str_mv AT newtoncsantos ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT raphaelljalmeida ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT annaestome ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT fabiogteles ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT railenehcraraujo ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT juanneqfarias ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT mariatsdfonseca ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT virginiamdasilva ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT victorhdaribeiro ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT marciardspedrini ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT josivandapgomes ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder
AT anaptrocha ozoneaerationenhanceflowabilitystructureandantioxidantactivityinblueberrypulppowder