Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayers

Abstract Mitigating ethanol inhibition in chemiresistors is essential for accurately detecting target gases in various fields. Conventional approaches to reducing ethanol interference frequently result in a significant deterioration of sensing capabilities, including decreased target gas response, a...

Full description

Saved in:
Bibliographic Details
Main Authors: Ki Beom Kim, Myung Sung Sohn, In-Sung Hwang, Do Joon Yoo, Seong-Yong Jeong, Yun Chan Kang, Young Kook Moon
Format: Article
Language:English
Published: Nature Portfolio 2025-06-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-025-60500-2
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849725071274278912
author Ki Beom Kim
Myung Sung Sohn
In-Sung Hwang
Do Joon Yoo
Seong-Yong Jeong
Yun Chan Kang
Young Kook Moon
author_facet Ki Beom Kim
Myung Sung Sohn
In-Sung Hwang
Do Joon Yoo
Seong-Yong Jeong
Yun Chan Kang
Young Kook Moon
author_sort Ki Beom Kim
collection DOAJ
description Abstract Mitigating ethanol inhibition in chemiresistors is essential for accurately detecting target gases in various fields. Conventional approaches to reducing ethanol interference frequently result in a significant deterioration of sensing capabilities, including decreased target gas response, altered selectivity, and sluggish response kinetics. In this study, a coating of acidic proton form ZSM-5 (HZSM-5) overlayer is proposed as a facile and universal strategy for eliminating ethanol inhibition without compromising intrinsic sensing properties. An HZSM-5 overlayer deposited on the oxide sensors exhibits exceptional formaldehyde (HCHO), which poses harmful health impacts to humans even at trace levels, detection properties by effectively eliminating ethanol interference without altering the HCHO response or response time. The exceptional performance of the bilayer sensor is systematically explained by the dehydration of ethanol to less reactive ethylene by the acidic HZSM-5 overlayer. Analysis using NH3 temperature-programmed desorption (NH3–TPD), proton transfer reaction quadrupole mass spectrometry (PTR–QMS) as well as in-situ diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) are performed to verify the above proposals. Additionally, sensor arrays are employed to enable pattern recognition capable of shielding HCHO, benzene, toluene, and p-xylene from ethanol interferents, thereby facilitating the electronic noses for monitoring indoor air pollutants.
format Article
id doaj-art-a1e2b4923071417595780aa5a0ae33c6
institution DOAJ
issn 2041-1723
language English
publishDate 2025-06-01
publisher Nature Portfolio
record_format Article
series Nature Communications
spelling doaj-art-a1e2b4923071417595780aa5a0ae33c62025-08-20T03:10:34ZengNature PortfolioNature Communications2041-17232025-06-0116111210.1038/s41467-025-60500-2Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayersKi Beom Kim0Myung Sung Sohn1In-Sung Hwang2Do Joon Yoo3Seong-Yong Jeong4Yun Chan Kang5Young Kook Moon6Department of Materials Science and Engineering, Korea UniversityDepartment of Materials Science and Engineering, Korea UniversitySentech GMI Co. LtdSentech GMI Co. LtdDivision of Advanced Materials engineering, Kongju National UniversityDepartment of Materials Science and Engineering, Korea UniversityNanomaterials Research Division, Korea Institute of Materials Science (KIMS)Abstract Mitigating ethanol inhibition in chemiresistors is essential for accurately detecting target gases in various fields. Conventional approaches to reducing ethanol interference frequently result in a significant deterioration of sensing capabilities, including decreased target gas response, altered selectivity, and sluggish response kinetics. In this study, a coating of acidic proton form ZSM-5 (HZSM-5) overlayer is proposed as a facile and universal strategy for eliminating ethanol inhibition without compromising intrinsic sensing properties. An HZSM-5 overlayer deposited on the oxide sensors exhibits exceptional formaldehyde (HCHO), which poses harmful health impacts to humans even at trace levels, detection properties by effectively eliminating ethanol interference without altering the HCHO response or response time. The exceptional performance of the bilayer sensor is systematically explained by the dehydration of ethanol to less reactive ethylene by the acidic HZSM-5 overlayer. Analysis using NH3 temperature-programmed desorption (NH3–TPD), proton transfer reaction quadrupole mass spectrometry (PTR–QMS) as well as in-situ diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) are performed to verify the above proposals. Additionally, sensor arrays are employed to enable pattern recognition capable of shielding HCHO, benzene, toluene, and p-xylene from ethanol interferents, thereby facilitating the electronic noses for monitoring indoor air pollutants.https://doi.org/10.1038/s41467-025-60500-2
spellingShingle Ki Beom Kim
Myung Sung Sohn
In-Sung Hwang
Do Joon Yoo
Seong-Yong Jeong
Yun Chan Kang
Young Kook Moon
Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayers
Nature Communications
title Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayers
title_full Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayers
title_fullStr Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayers
title_full_unstemmed Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayers
title_short Mitigating alcohol inhibition of oxide chemiresistors: bilayer sensors with HZSM-5 zeolite overlayers
title_sort mitigating alcohol inhibition of oxide chemiresistors bilayer sensors with hzsm 5 zeolite overlayers
url https://doi.org/10.1038/s41467-025-60500-2
work_keys_str_mv AT kibeomkim mitigatingalcoholinhibitionofoxidechemiresistorsbilayersensorswithhzsm5zeoliteoverlayers
AT myungsungsohn mitigatingalcoholinhibitionofoxidechemiresistorsbilayersensorswithhzsm5zeoliteoverlayers
AT insunghwang mitigatingalcoholinhibitionofoxidechemiresistorsbilayersensorswithhzsm5zeoliteoverlayers
AT dojoonyoo mitigatingalcoholinhibitionofoxidechemiresistorsbilayersensorswithhzsm5zeoliteoverlayers
AT seongyongjeong mitigatingalcoholinhibitionofoxidechemiresistorsbilayersensorswithhzsm5zeoliteoverlayers
AT yunchankang mitigatingalcoholinhibitionofoxidechemiresistorsbilayersensorswithhzsm5zeoliteoverlayers
AT youngkookmoon mitigatingalcoholinhibitionofoxidechemiresistorsbilayersensorswithhzsm5zeoliteoverlayers