Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdust

This study investigates the production and thermal characterization of biochar derived from two biomass sources: rapeseed meal and sawdust of Fraxinus excelsior. Biochars were produced through slow pyrolysis at 350 °C, and their chemical composition, thermal stability, and carbon structure were anal...

Full description

Saved in:
Bibliographic Details
Main Authors: Mohammad Meysami, Amin Rabie, Reza Amini Najafabadi, Amirhossein Meysami, Taghi Isfahani
Format: Article
Language:English
Published: Elsevier 2025-09-01
Series:Results in Engineering
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2590123025024673
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849731251817152512
author Mohammad Meysami
Amin Rabie
Reza Amini Najafabadi
Amirhossein Meysami
Taghi Isfahani
author_facet Mohammad Meysami
Amin Rabie
Reza Amini Najafabadi
Amirhossein Meysami
Taghi Isfahani
author_sort Mohammad Meysami
collection DOAJ
description This study investigates the production and thermal characterization of biochar derived from two biomass sources: rapeseed meal and sawdust of Fraxinus excelsior. Biochars were produced through slow pyrolysis at 350 °C, and their chemical composition, thermal stability, and carbon structure were analyzed using FTIR, Raman spectroscopy, CHNS analysis, TGA/DTG, and DSC. The results showed high fixed carbon contents of 59.3 % for rapeseed meal and 57.6 % for wood-based biochars, with sulfur contents below 0.1 %. FTIR and Raman analyses confirmed the formation of stable carbonaceous structures with characteristic functional groups. TGA revealed strong thermal stability, with residual masses of 42 % and 47 % at 1000 °C for rapeseed and wood biochars, respectively. DSC analysis demonstrated that wood-derived biochar retained more energy, while rapeseed biochar exhibited higher carbon content. A statistical comparison using bootstrap, effect size, and Bayesian estimation confirmed these trends. Overall, both biochars demonstrate strong potential as sustainable, carbon-rich alternatives for high-temperature industrial applications.
format Article
id doaj-art-a1b91dd1cc9d4115ac4f7cdfffc44162
institution DOAJ
issn 2590-1230
language English
publishDate 2025-09-01
publisher Elsevier
record_format Article
series Results in Engineering
spelling doaj-art-a1b91dd1cc9d4115ac4f7cdfffc441622025-08-20T03:08:36ZengElsevierResults in Engineering2590-12302025-09-012710639710.1016/j.rineng.2025.106397Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdustMohammad Meysami0Amin Rabie1Reza Amini Najafabadi2Amirhossein Meysami3Taghi Isfahani4Department of Mathematics, Clarkson University, Potsdam, NY, USA; Corresponding author.Golpayegan College of Engineering, Isfahan University of Technology, Golpayegan, IranGolpayegan College of Engineering, Isfahan University of Technology, Golpayegan, IranGolpayegan College of Engineering, Isfahan University of Technology, Golpayegan, IranGolpayegan College of Engineering, Isfahan University of Technology, Golpayegan, IranThis study investigates the production and thermal characterization of biochar derived from two biomass sources: rapeseed meal and sawdust of Fraxinus excelsior. Biochars were produced through slow pyrolysis at 350 °C, and their chemical composition, thermal stability, and carbon structure were analyzed using FTIR, Raman spectroscopy, CHNS analysis, TGA/DTG, and DSC. The results showed high fixed carbon contents of 59.3 % for rapeseed meal and 57.6 % for wood-based biochars, with sulfur contents below 0.1 %. FTIR and Raman analyses confirmed the formation of stable carbonaceous structures with characteristic functional groups. TGA revealed strong thermal stability, with residual masses of 42 % and 47 % at 1000 °C for rapeseed and wood biochars, respectively. DSC analysis demonstrated that wood-derived biochar retained more energy, while rapeseed biochar exhibited higher carbon content. A statistical comparison using bootstrap, effect size, and Bayesian estimation confirmed these trends. Overall, both biochars demonstrate strong potential as sustainable, carbon-rich alternatives for high-temperature industrial applications.http://www.sciencedirect.com/science/article/pii/S2590123025024673BiomassBiocharRapeseed mealWood wasteFossil carbon
spellingShingle Mohammad Meysami
Amin Rabie
Reza Amini Najafabadi
Amirhossein Meysami
Taghi Isfahani
Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdust
Results in Engineering
Biomass
Biochar
Rapeseed meal
Wood waste
Fossil carbon
title Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdust
title_full Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdust
title_fullStr Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdust
title_full_unstemmed Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdust
title_short Comparative thermal and structural analysis of biochar from rapeseed meal and Fraxinus excelsior sawdust
title_sort comparative thermal and structural analysis of biochar from rapeseed meal and fraxinus excelsior sawdust
topic Biomass
Biochar
Rapeseed meal
Wood waste
Fossil carbon
url http://www.sciencedirect.com/science/article/pii/S2590123025024673
work_keys_str_mv AT mohammadmeysami comparativethermalandstructuralanalysisofbiocharfromrapeseedmealandfraxinusexcelsiorsawdust
AT aminrabie comparativethermalandstructuralanalysisofbiocharfromrapeseedmealandfraxinusexcelsiorsawdust
AT rezaamininajafabadi comparativethermalandstructuralanalysisofbiocharfromrapeseedmealandfraxinusexcelsiorsawdust
AT amirhosseinmeysami comparativethermalandstructuralanalysisofbiocharfromrapeseedmealandfraxinusexcelsiorsawdust
AT taghiisfahani comparativethermalandstructuralanalysisofbiocharfromrapeseedmealandfraxinusexcelsiorsawdust