Operando phase mapping in multi-material laser powder bed fusion

Layer-wise laser-based additive manufacturing techniques offer immense versatility and flexibility in fabricating metallic composites with complex shapes. Interest in producing new multi-materials with advanced characteristics outpaces the available methods that provide insights into the bulk materi...

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Main Authors: Shieren Sumarli, Florencia Malamud, Steven Van Petegem, Steve Gaudez, Antonios Baganis, Matteo Busi, Efthymios Polatidis, Christian Leinenbach, Roland E. Logé, Markus Strobl
Format: Article
Language:English
Published: Taylor & Francis Group 2024-12-01
Series:Virtual and Physical Prototyping
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Online Access:https://www.tandfonline.com/doi/10.1080/17452759.2024.2429132
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author Shieren Sumarli
Florencia Malamud
Steven Van Petegem
Steve Gaudez
Antonios Baganis
Matteo Busi
Efthymios Polatidis
Christian Leinenbach
Roland E. Logé
Markus Strobl
author_facet Shieren Sumarli
Florencia Malamud
Steven Van Petegem
Steve Gaudez
Antonios Baganis
Matteo Busi
Efthymios Polatidis
Christian Leinenbach
Roland E. Logé
Markus Strobl
author_sort Shieren Sumarli
collection DOAJ
description Layer-wise laser-based additive manufacturing techniques offer immense versatility and flexibility in fabricating metallic composites with complex shapes. Interest in producing new multi-materials with advanced characteristics outpaces the available methods that provide insights into the bulk material formation, which in turn enables process and material optimisation. While some advanced operando studies enable highly local observations in the established metallic layers, the effect of intrinsic heat treatment inherent in the process in the bulk of the material is generally beyond reach of operando characterisation. Here, we approach the regime through advanced operando neutron imaging utilising a custom-designed laser powder bed fusion device on a neutron beamline. Operando polarisation contrast neutron imaging experiments were carried out during building centimetre-sized specimens with different powder premixture compositions of 316L and CuCrZr. The results of these full-field spatially resolved measurements reveal the quantitative evolution of ferromagnetic phases and temperature throughout the specimens and processing time.
format Article
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institution Kabale University
issn 1745-2759
1745-2767
language English
publishDate 2024-12-01
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record_format Article
series Virtual and Physical Prototyping
spelling doaj-art-a1672805d8364bc0af6fa47095c7e7bf2025-01-08T19:51:37ZengTaylor & Francis GroupVirtual and Physical Prototyping1745-27591745-27672024-12-0119110.1080/17452759.2024.2429132Operando phase mapping in multi-material laser powder bed fusionShieren Sumarli0Florencia Malamud1Steven Van Petegem2Steve Gaudez3Antonios Baganis4Matteo Busi5Efthymios Polatidis6Christian Leinenbach7Roland E. Logé8Markus Strobl9PSI Center for Neutron and Muon Sciences, Paul Scherrer Institute, Villigen, SwitzerlandPSI Center for Neutron and Muon Sciences, Paul Scherrer Institute, Villigen, SwitzerlandPSI Center for Photon Science, Paul Scherrer Institute, Villigen, SwitzerlandPSI Center for Photon Science, Paul Scherrer Institute, Villigen, SwitzerlandLaboratory for Advanced Materials Processing, Swiss Federal Laboratories for Materials Science and Technology (Empa), Dübendorf, SwitzerlandPSI Center for Neutron and Muon Sciences, Paul Scherrer Institute, Villigen, SwitzerlandLaboratory of Technology and Strength of Materials, University of Patras, Patras, GreeceLaboratory for Advanced Materials Processing, Swiss Federal Laboratories for Materials Science and Technology (Empa), Dübendorf, SwitzerlandThermomechanical Metallurgy Laboratory – PX Group Chair, École Polytechnique Fédérale de Lausanne (EPFL), Lausanne, SwitzerlandPSI Center for Neutron and Muon Sciences, Paul Scherrer Institute, Villigen, SwitzerlandLayer-wise laser-based additive manufacturing techniques offer immense versatility and flexibility in fabricating metallic composites with complex shapes. Interest in producing new multi-materials with advanced characteristics outpaces the available methods that provide insights into the bulk material formation, which in turn enables process and material optimisation. While some advanced operando studies enable highly local observations in the established metallic layers, the effect of intrinsic heat treatment inherent in the process in the bulk of the material is generally beyond reach of operando characterisation. Here, we approach the regime through advanced operando neutron imaging utilising a custom-designed laser powder bed fusion device on a neutron beamline. Operando polarisation contrast neutron imaging experiments were carried out during building centimetre-sized specimens with different powder premixture compositions of 316L and CuCrZr. The results of these full-field spatially resolved measurements reveal the quantitative evolution of ferromagnetic phases and temperature throughout the specimens and processing time.https://www.tandfonline.com/doi/10.1080/17452759.2024.2429132Operando polarisation contrast neutron imagingoperando neutron temperature mappinglaser powder bed fusionmulti-material processingferromagnetic phase quantification
spellingShingle Shieren Sumarli
Florencia Malamud
Steven Van Petegem
Steve Gaudez
Antonios Baganis
Matteo Busi
Efthymios Polatidis
Christian Leinenbach
Roland E. Logé
Markus Strobl
Operando phase mapping in multi-material laser powder bed fusion
Virtual and Physical Prototyping
Operando polarisation contrast neutron imaging
operando neutron temperature mapping
laser powder bed fusion
multi-material processing
ferromagnetic phase quantification
title Operando phase mapping in multi-material laser powder bed fusion
title_full Operando phase mapping in multi-material laser powder bed fusion
title_fullStr Operando phase mapping in multi-material laser powder bed fusion
title_full_unstemmed Operando phase mapping in multi-material laser powder bed fusion
title_short Operando phase mapping in multi-material laser powder bed fusion
title_sort operando phase mapping in multi material laser powder bed fusion
topic Operando polarisation contrast neutron imaging
operando neutron temperature mapping
laser powder bed fusion
multi-material processing
ferromagnetic phase quantification
url https://www.tandfonline.com/doi/10.1080/17452759.2024.2429132
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