Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen Production

ABSTRACT Efficient photocatalytic water splitting can be significantly enhanced through the careful design of S‐scheme heterostructures, which play a pivotal role in optimizing performance. Herein, we report the construction of ZnIn2S4/CdS S‐scheme heterojunctions under ambient conditions, based on...

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Main Authors: Dongdong Zhang, Zhiyi Gao, Dongjiang Yang, Lin Wang, Xiangdong Yang, Kai Tang, Hongli Yang, Xiaoqiang Zhan, Zhengjun Wang, Weiyou Yang
Format: Article
Language:English
Published: Wiley 2025-06-01
Series:Carbon Energy
Subjects:
Online Access:https://doi.org/10.1002/cey2.707
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author Dongdong Zhang
Zhiyi Gao
Dongjiang Yang
Lin Wang
Xiangdong Yang
Kai Tang
Hongli Yang
Xiaoqiang Zhan
Zhengjun Wang
Weiyou Yang
author_facet Dongdong Zhang
Zhiyi Gao
Dongjiang Yang
Lin Wang
Xiangdong Yang
Kai Tang
Hongli Yang
Xiaoqiang Zhan
Zhengjun Wang
Weiyou Yang
author_sort Dongdong Zhang
collection DOAJ
description ABSTRACT Efficient photocatalytic water splitting can be significantly enhanced through the careful design of S‐scheme heterostructures, which play a pivotal role in optimizing performance. Herein, we report the construction of ZnIn2S4/CdS S‐scheme heterojunctions under ambient conditions, based on a sonochemical strategy. This structure is facilitated by the well‐matched interface between the (007) plane of layered ZnIn2S4 and the (101) plane of CdS, leading to a threshold optical response of 2.12 eV, which optimally aligns with visible light absorption. As a proof of concept, the resulting ZnIn₂S₄/CdS catalysts demonstrate a remarkable improvement in photocatalytic H₂ evolution, achieving a rate of 5678.2 μmol h−1g−1 under visible light irradiation (λ > 400 nm). This rate is approximately 10 times higher than that of pristine ZnIn₂S₄ nanosheets (NSs) and about 4.6 times higher than that of CdS nanoparticles (NPs), surpassing the performance of most ZnIn₂S₄‐based photocatalysts reported to date. Moreover, they deliver a robust photocatalytic performance during long‐term operation of up to 60 h, showing their potential for use in practical applications. Based on the theoretical calculation and experimental results, it is verified that the movements of electrons and holes in the opposite direction could be induced by the disparity in the work function and the internal electric field within the interfaces, thus facilitating the construction of S‐scheme heterojunctions, which fundamentally suppresses carrier recombination while minimizing photocorrosion of ZnIn2S4 toward enhanced photocatalytic behaviors.
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spelling doaj-art-a0b1d4f8e1cd4b489b2364ea175ad6002025-08-20T03:14:50ZengWileyCarbon Energy2637-93682025-06-0176n/an/a10.1002/cey2.707Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen ProductionDongdong Zhang0Zhiyi Gao1Dongjiang Yang2Lin Wang3Xiangdong Yang4Kai Tang5Hongli Yang6Xiaoqiang Zhan7Zhengjun Wang8Weiyou Yang9Institute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaCAS Key Laboratory of Magnetic Materials and Devices Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences Ningbo ChinaInstitute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaInstitute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaInstitute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaInstitute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaInstitute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaInstitute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaCollege of Chemistry and Materials Engineering, Wenzhou University Wenzhou ChinaInstitute of Micro/Nano Materials and Devices Ningbo University of Technology Ningbo Zhejiang ChinaABSTRACT Efficient photocatalytic water splitting can be significantly enhanced through the careful design of S‐scheme heterostructures, which play a pivotal role in optimizing performance. Herein, we report the construction of ZnIn2S4/CdS S‐scheme heterojunctions under ambient conditions, based on a sonochemical strategy. This structure is facilitated by the well‐matched interface between the (007) plane of layered ZnIn2S4 and the (101) plane of CdS, leading to a threshold optical response of 2.12 eV, which optimally aligns with visible light absorption. As a proof of concept, the resulting ZnIn₂S₄/CdS catalysts demonstrate a remarkable improvement in photocatalytic H₂ evolution, achieving a rate of 5678.2 μmol h−1g−1 under visible light irradiation (λ > 400 nm). This rate is approximately 10 times higher than that of pristine ZnIn₂S₄ nanosheets (NSs) and about 4.6 times higher than that of CdS nanoparticles (NPs), surpassing the performance of most ZnIn₂S₄‐based photocatalysts reported to date. Moreover, they deliver a robust photocatalytic performance during long‐term operation of up to 60 h, showing their potential for use in practical applications. Based on the theoretical calculation and experimental results, it is verified that the movements of electrons and holes in the opposite direction could be induced by the disparity in the work function and the internal electric field within the interfaces, thus facilitating the construction of S‐scheme heterojunctions, which fundamentally suppresses carrier recombination while minimizing photocorrosion of ZnIn2S4 toward enhanced photocatalytic behaviors.https://doi.org/10.1002/cey2.707CdSheterojunctionsinterfacephotocatalytic hydrogen productionZnIn2S4
spellingShingle Dongdong Zhang
Zhiyi Gao
Dongjiang Yang
Lin Wang
Xiangdong Yang
Kai Tang
Hongli Yang
Xiaoqiang Zhan
Zhengjun Wang
Weiyou Yang
Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen Production
Carbon Energy
CdS
heterojunctions
interface
photocatalytic hydrogen production
ZnIn2S4
title Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen Production
title_full Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen Production
title_fullStr Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen Production
title_full_unstemmed Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen Production
title_short Crystal‐Interface‐Mediated Self‐Assembly of ZnIn2S4/CdS S‐scheme Heterojunctions Toward Efficient Photocatalytic Hydrogen Production
title_sort crystal interface mediated self assembly of znin2s4 cds s scheme heterojunctions toward efficient photocatalytic hydrogen production
topic CdS
heterojunctions
interface
photocatalytic hydrogen production
ZnIn2S4
url https://doi.org/10.1002/cey2.707
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