Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef Hams

Consumers appreciate fermented meat products due to their nutritional value and unique taste. Fermented fruit vinegar used traditionally to preserve food is characterized by a high content of nutrients and bioactive ingredients. Acid whey has antioxidant and antibacterial properties and can provide...

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Main Authors: Barbara Sionek, Anna Okoń, Anna Łepecka, Agata Antoniewska-Krzeska, Piotr Szymański, Danuta Jaworska, Jarosława Rutkowska, Danuta Kołożyn-Krajewska
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Language:English
Published: MDPI AG 2025-01-01
Series:Agriculture
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Online Access:https://www.mdpi.com/2077-0472/15/1/107
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author Barbara Sionek
Anna Okoń
Anna Łepecka
Agata Antoniewska-Krzeska
Piotr Szymański
Danuta Jaworska
Jarosława Rutkowska
Danuta Kołożyn-Krajewska
author_facet Barbara Sionek
Anna Okoń
Anna Łepecka
Agata Antoniewska-Krzeska
Piotr Szymański
Danuta Jaworska
Jarosława Rutkowska
Danuta Kołożyn-Krajewska
author_sort Barbara Sionek
collection DOAJ
description Consumers appreciate fermented meat products due to their nutritional value and unique taste. Fermented fruit vinegar used traditionally to preserve food is characterized by a high content of nutrients and bioactive ingredients. Acid whey has antioxidant and antibacterial properties and can provide probiotic lactic acid bacteria (LAB). Three variants of the fermented beef hams were produced: AW—1.5% salt and 5% acid whey, A—1.5% salt and 5% apple vinegar, and C—1.5% salt. The effect of natural marination, based on apple vinegar and acid whey on volatiles, physicochemical and microbiological parameters, and sensory quality of the raw fermented beef hams was assessed. The highest pH and the lowest oxidation–reduction potential value (ORP) was found for A hams after production and after storage (<i>p</i> < 0.05). AW hams had the highest Thiobarbituric Acid-Reactive Substances (TBARS) value after production (6.07 mg MDA/kg) and after 8 months of storage (6.12 mg MDA/kg) (<i>p</i> < 0.05). The AW and A hams showed moderate overall sensory quality after production and after storage (above 5 c.u.). Both treatments modify the formation and stability of volatile compounds, not affecting the overall quality. The number of LAB in raw fermented beef hams with acid whey and apple vinegar was high (approximately 7 log CFU/g) after 3 months, and this decreased after 8 months of storage to 6.24 and 5.83 log CFU/g, respectively, for AW and A treatment. Among sixty volatile compounds, an abundance of aldehydes, carboxylic acids, esters, and alcohols dominated, which contributed to the formation of aroma attributes of beef hams. This study demonstrates that apple vinegar and acid whey can be used for the production of microbiologically safe fermented beef hams with good sensory quality.
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spelling doaj-art-a0a4b3ec99ee4449b61122ee3c9c5ec32025-08-20T02:47:00ZengMDPI AGAgriculture2077-04722025-01-0115110710.3390/agriculture15010107Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef HamsBarbara Sionek0Anna Okoń1Anna Łepecka2Agata Antoniewska-Krzeska3Piotr Szymański4Danuta Jaworska5Jarosława Rutkowska6Danuta Kołożyn-Krajewska7Department of Food Gastronomy and Food Hygiene, Institute of Human Nutrition Sciences, Warsaw University of Life Sciences (WULS), Nowoursynowska St. 159C, 02-776 Warsaw, PolandDepartment of Meat and Fat Technology, Prof. Waclaw Dabrowski Institute of Agricultural and Food Biotechnology—State Research Institute, 02-532 Warsaw, PolandDepartment of Meat and Fat Technology, Prof. Waclaw Dabrowski Institute of Agricultural and Food Biotechnology—State Research Institute, 02-532 Warsaw, PolandDepartment of Food Gastronomy and Food Hygiene, Institute of Human Nutrition Sciences, Warsaw University of Life Sciences (WULS), Nowoursynowska St. 159C, 02-776 Warsaw, PolandDepartment of Meat and Fat Technology, Prof. Waclaw Dabrowski Institute of Agricultural and Food Biotechnology—State Research Institute, 02-532 Warsaw, PolandDepartment of Food Gastronomy and Food Hygiene, Institute of Human Nutrition Sciences, Warsaw University of Life Sciences (WULS), Nowoursynowska St. 159C, 02-776 Warsaw, PolandDepartment of Food Gastronomy and Food Hygiene, Institute of Human Nutrition Sciences, Warsaw University of Life Sciences (WULS), Nowoursynowska St. 159C, 02-776 Warsaw, PolandDepartment of Dietetics and Food Studies, Faculty of Science and Technology, Jan Dlugosz University in Czestochowa, Al. Armii Krajowej 13/15, 42-200 Czestochowa, PolandConsumers appreciate fermented meat products due to their nutritional value and unique taste. Fermented fruit vinegar used traditionally to preserve food is characterized by a high content of nutrients and bioactive ingredients. Acid whey has antioxidant and antibacterial properties and can provide probiotic lactic acid bacteria (LAB). Three variants of the fermented beef hams were produced: AW—1.5% salt and 5% acid whey, A—1.5% salt and 5% apple vinegar, and C—1.5% salt. The effect of natural marination, based on apple vinegar and acid whey on volatiles, physicochemical and microbiological parameters, and sensory quality of the raw fermented beef hams was assessed. The highest pH and the lowest oxidation–reduction potential value (ORP) was found for A hams after production and after storage (<i>p</i> < 0.05). AW hams had the highest Thiobarbituric Acid-Reactive Substances (TBARS) value after production (6.07 mg MDA/kg) and after 8 months of storage (6.12 mg MDA/kg) (<i>p</i> < 0.05). The AW and A hams showed moderate overall sensory quality after production and after storage (above 5 c.u.). Both treatments modify the formation and stability of volatile compounds, not affecting the overall quality. The number of LAB in raw fermented beef hams with acid whey and apple vinegar was high (approximately 7 log CFU/g) after 3 months, and this decreased after 8 months of storage to 6.24 and 5.83 log CFU/g, respectively, for AW and A treatment. Among sixty volatile compounds, an abundance of aldehydes, carboxylic acids, esters, and alcohols dominated, which contributed to the formation of aroma attributes of beef hams. This study demonstrates that apple vinegar and acid whey can be used for the production of microbiologically safe fermented beef hams with good sensory quality.https://www.mdpi.com/2077-0472/15/1/107vinegaracid wheylactic acid bacteriavolatilesraw fermented meat
spellingShingle Barbara Sionek
Anna Okoń
Anna Łepecka
Agata Antoniewska-Krzeska
Piotr Szymański
Danuta Jaworska
Jarosława Rutkowska
Danuta Kołożyn-Krajewska
Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef Hams
Agriculture
vinegar
acid whey
lactic acid bacteria
volatiles
raw fermented meat
title Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef Hams
title_full Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef Hams
title_fullStr Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef Hams
title_full_unstemmed Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef Hams
title_short Effect of Natural Marination Based on Apple Vinegar and Acid Whey on Volatile and Sensory Profile, Safety, and Physicochemical Properties of Raw Fermented Beef Hams
title_sort effect of natural marination based on apple vinegar and acid whey on volatile and sensory profile safety and physicochemical properties of raw fermented beef hams
topic vinegar
acid whey
lactic acid bacteria
volatiles
raw fermented meat
url https://www.mdpi.com/2077-0472/15/1/107
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