New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>

Nine chaetoglobosins (<b>1</b>–<b>9</b>) including five previously undescribed ones (<b>1</b>–<b>5</b>) were obtained from the culture broth of an endophytic fungus (<i>Chaetomium</i> sp. UJN-EF006) isolated from the leaves of <i>Vacc...

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Main Authors: Luo-Jing Wang, Zong-Yan Ma, Xin-Ling Wang, Kai-Le Wang, Tong Zhang, Rui-Ying Han, Jun-Jiang Li, Jie Bao, Yin-Yin Wang, Hua Zhang
Format: Article
Language:English
Published: MDPI AG 2025-07-01
Series:Journal of Fungi
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Online Access:https://www.mdpi.com/2309-608X/11/7/511
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author Luo-Jing Wang
Zong-Yan Ma
Xin-Ling Wang
Kai-Le Wang
Tong Zhang
Rui-Ying Han
Jun-Jiang Li
Jie Bao
Yin-Yin Wang
Hua Zhang
author_facet Luo-Jing Wang
Zong-Yan Ma
Xin-Ling Wang
Kai-Le Wang
Tong Zhang
Rui-Ying Han
Jun-Jiang Li
Jie Bao
Yin-Yin Wang
Hua Zhang
author_sort Luo-Jing Wang
collection DOAJ
description Nine chaetoglobosins (<b>1</b>–<b>9</b>) including five previously undescribed ones (<b>1</b>–<b>5</b>) were obtained from the culture broth of an endophytic fungus (<i>Chaetomium</i> sp. UJN-EF006) isolated from the leaves of <i>Vaccinium bracteatum</i>. The structures of these fungal metabolites were elucidated by spectroscopic methods including mass spectroscopy, nuclear magnetic resonance, single crystal X-ray crystallography, and electronic circular dichroism. To accelerate the development of novel fungicides, all of the isolated chaetoglobosins were evaluated for their antifungal activity against two crop pathogens, <i>Botrytis cinerea</i> and <i>Sclerotinia sclerotiorum</i>. The assay results revealed that chaetoglobosins <b>2</b>, <b>6</b>, <b>7</b>, and <b>9</b> possessed a significant fungicidal effect against <i>B. cinerea</i>, with EC<sub>50</sub> values all below 10 μg/mL. Particularly, the most potent compound, <b>7</b>, was 175- and 96-fold as active as the commercially available fungicides carbendazim (EC<sub>50</sub> 70.11 μg/mL) and azoxystrobin (EC<sub>50</sub> 39.02 μg/mL), respectively. A further observation under scanning electron microscope indicated that compound <b>2</b> could markedly impair the fungal hyphae of <i>B. cinerea</i>. The study demonstrates that the chaetoglobosins had excellent in vitro antifungal activities against <i>B. cinerea</i>.
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issn 2309-608X
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publisher MDPI AG
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series Journal of Fungi
spelling doaj-art-a05806c587c74bf7bf5b701fca756c052025-08-20T03:35:28ZengMDPI AGJournal of Fungi2309-608X2025-07-0111751110.3390/jof11070511New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>Luo-Jing Wang0Zong-Yan Ma1Xin-Ling Wang2Kai-Le Wang3Tong Zhang4Rui-Ying Han5Jun-Jiang Li6Jie Bao7Yin-Yin Wang8Hua Zhang9School of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaSchool of Biological Science and Technology, University of Jinan, Jinan 250022, ChinaNine chaetoglobosins (<b>1</b>–<b>9</b>) including five previously undescribed ones (<b>1</b>–<b>5</b>) were obtained from the culture broth of an endophytic fungus (<i>Chaetomium</i> sp. UJN-EF006) isolated from the leaves of <i>Vaccinium bracteatum</i>. The structures of these fungal metabolites were elucidated by spectroscopic methods including mass spectroscopy, nuclear magnetic resonance, single crystal X-ray crystallography, and electronic circular dichroism. To accelerate the development of novel fungicides, all of the isolated chaetoglobosins were evaluated for their antifungal activity against two crop pathogens, <i>Botrytis cinerea</i> and <i>Sclerotinia sclerotiorum</i>. The assay results revealed that chaetoglobosins <b>2</b>, <b>6</b>, <b>7</b>, and <b>9</b> possessed a significant fungicidal effect against <i>B. cinerea</i>, with EC<sub>50</sub> values all below 10 μg/mL. Particularly, the most potent compound, <b>7</b>, was 175- and 96-fold as active as the commercially available fungicides carbendazim (EC<sub>50</sub> 70.11 μg/mL) and azoxystrobin (EC<sub>50</sub> 39.02 μg/mL), respectively. A further observation under scanning electron microscope indicated that compound <b>2</b> could markedly impair the fungal hyphae of <i>B. cinerea</i>. The study demonstrates that the chaetoglobosins had excellent in vitro antifungal activities against <i>B. cinerea</i>.https://www.mdpi.com/2309-608X/11/7/511<i>Chaetomium</i> sp.chaetoglobosinphytopathogenfungicide<i>Botrytis cinerea</i><i>Sclerotinia sclerotiorum</i>
spellingShingle Luo-Jing Wang
Zong-Yan Ma
Xin-Ling Wang
Kai-Le Wang
Tong Zhang
Rui-Ying Han
Jun-Jiang Li
Jie Bao
Yin-Yin Wang
Hua Zhang
New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>
Journal of Fungi
<i>Chaetomium</i> sp.
chaetoglobosin
phytopathogen
fungicide
<i>Botrytis cinerea</i>
<i>Sclerotinia sclerotiorum</i>
title New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>
title_full New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>
title_fullStr New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>
title_full_unstemmed New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>
title_short New Chaetoglobosins with Fungicidal Activity from <i>Chaetomium</i> sp. UJN-EF006 Endophytic in <i>Vaccinium bracteatum</i>
title_sort new chaetoglobosins with fungicidal activity from i chaetomium i sp ujn ef006 endophytic in i vaccinium bracteatum i
topic <i>Chaetomium</i> sp.
chaetoglobosin
phytopathogen
fungicide
<i>Botrytis cinerea</i>
<i>Sclerotinia sclerotiorum</i>
url https://www.mdpi.com/2309-608X/11/7/511
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