Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processing

Fire-resistant steels are engineered to retain high strength at elevated temperatures, typically maintaining a yield strength (YS) ratio (600 °C/RT) above 0.67 to prevent sudden structural collapse during fire exposure. Although achieving such strength retention is critical, ensuring sufficient frac...

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Main Authors: Hyungkwon Park, Hyo-Haeng Jo, Chiwon Kim, Seong Hoon Kim, Kyeong-Won Kim, Joonoh Moon, Hyun-Uk Hong, Jun-Ho Chung, Bong-Ho Lee, Chang-Hoon Lee
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425016928
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author Hyungkwon Park
Hyo-Haeng Jo
Chiwon Kim
Seong Hoon Kim
Kyeong-Won Kim
Joonoh Moon
Hyun-Uk Hong
Jun-Ho Chung
Bong-Ho Lee
Chang-Hoon Lee
author_facet Hyungkwon Park
Hyo-Haeng Jo
Chiwon Kim
Seong Hoon Kim
Kyeong-Won Kim
Joonoh Moon
Hyun-Uk Hong
Jun-Ho Chung
Bong-Ho Lee
Chang-Hoon Lee
author_sort Hyungkwon Park
collection DOAJ
description Fire-resistant steels are engineered to retain high strength at elevated temperatures, typically maintaining a yield strength (YS) ratio (600 °C/RT) above 0.67 to prevent sudden structural collapse during fire exposure. Although achieving such strength retention is critical, ensuring sufficient fracture toughness is equally essential for structural reliability. However, toughness behavior in fire-resistant steels has been largely overlooked, particularly in relation to thermomechanical processing. In this study, the influence of thermomechanical controlled processing (TMCP) on the microstructure and mechanical behavior of fire-resistant steel was investigated, with an emphasis on the strength-toughness trade-off. With increasing TMCP conducted below the non-recrystallization temperature (Tnr), the bainite fraction decreased markedly from 79 % to 27 %, whereas the ferrite fraction increased. The prior austenite grain size of the bainite was significantly refined, whereas the ferrite grain size remained nearly unchanged. This microstructural evolution led to a gradual reduction in yield strength (YS) at both room and elevated temperatures, decreasing the YS ratio (600 °C/RT) from 0.717 to 0.501. Meanwhile, the Charpy impact energy increased from 32.9 to 169.5 J, thereby demonstrating a clear trade-off between strength and toughness. Notably, the bainite fraction exhibited a strong linear correlation with the strength and YS ratio, whereas ferrite played a dominant role in enhancing toughness, with a complementary contribution from bainitic grain refinement. These findings demonstrate that the mechanical performance of fire-resistant steels can be effectively tuned through process optimization alone, thereby providing a practical strategy for designing steels with balanced strength and toughness.
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spelling doaj-art-9f7374e1308f4e5cba469d26a405307e2025-08-20T03:16:56ZengElsevierJournal of Materials Research and Technology2238-78542025-07-01373729373810.1016/j.jmrt.2025.07.034Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processingHyungkwon Park0Hyo-Haeng Jo1Chiwon Kim2Seong Hoon Kim3Kyeong-Won Kim4Joonoh Moon5Hyun-Uk Hong6Jun-Ho Chung7Bong-Ho Lee8Chang-Hoon Lee9Extreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of KoreaDepartment of Materials Science and Engineering, Changwon National University, Republic of KoreaDepartment of Materials Science and Engineering, Changwon National University, Republic of KoreaResearch & Development (R&D) Center, Hyundai Steel Company, Incheon, 22525, Republic of KoreaCenter for Core Research Facilities, Daegu Gyeongbuk Institute of Science and Technology, Republic of KoreaExtreme Materials Research Institute, Korea Institute of Materials Science, Changwon, Republic of Korea; Corresponding author.Fire-resistant steels are engineered to retain high strength at elevated temperatures, typically maintaining a yield strength (YS) ratio (600 °C/RT) above 0.67 to prevent sudden structural collapse during fire exposure. Although achieving such strength retention is critical, ensuring sufficient fracture toughness is equally essential for structural reliability. However, toughness behavior in fire-resistant steels has been largely overlooked, particularly in relation to thermomechanical processing. In this study, the influence of thermomechanical controlled processing (TMCP) on the microstructure and mechanical behavior of fire-resistant steel was investigated, with an emphasis on the strength-toughness trade-off. With increasing TMCP conducted below the non-recrystallization temperature (Tnr), the bainite fraction decreased markedly from 79 % to 27 %, whereas the ferrite fraction increased. The prior austenite grain size of the bainite was significantly refined, whereas the ferrite grain size remained nearly unchanged. This microstructural evolution led to a gradual reduction in yield strength (YS) at both room and elevated temperatures, decreasing the YS ratio (600 °C/RT) from 0.717 to 0.501. Meanwhile, the Charpy impact energy increased from 32.9 to 169.5 J, thereby demonstrating a clear trade-off between strength and toughness. Notably, the bainite fraction exhibited a strong linear correlation with the strength and YS ratio, whereas ferrite played a dominant role in enhancing toughness, with a complementary contribution from bainitic grain refinement. These findings demonstrate that the mechanical performance of fire-resistant steels can be effectively tuned through process optimization alone, thereby providing a practical strategy for designing steels with balanced strength and toughness.http://www.sciencedirect.com/science/article/pii/S2238785425016928Fire-resistant steelThermomechanical controlled processing (TMCP)BainiteYield strengthImpact toughness
spellingShingle Hyungkwon Park
Hyo-Haeng Jo
Chiwon Kim
Seong Hoon Kim
Kyeong-Won Kim
Joonoh Moon
Hyun-Uk Hong
Jun-Ho Chung
Bong-Ho Lee
Chang-Hoon Lee
Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processing
Journal of Materials Research and Technology
Fire-resistant steel
Thermomechanical controlled processing (TMCP)
Bainite
Yield strength
Impact toughness
title Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processing
title_full Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processing
title_fullStr Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processing
title_full_unstemmed Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processing
title_short Microstructural evolution and strength-toughness behavior of fire-resistant steel under thermo-mechanical controlled processing
title_sort microstructural evolution and strength toughness behavior of fire resistant steel under thermo mechanical controlled processing
topic Fire-resistant steel
Thermomechanical controlled processing (TMCP)
Bainite
Yield strength
Impact toughness
url http://www.sciencedirect.com/science/article/pii/S2238785425016928
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