Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels

The ability to control process parameters over time and build space in electron beam powder bed fusion (PBF-EB) opens up unprecedented opportunities to tailor the process and use materials of a different nature in the same build. The present investigation explored the various methods used to adapt t...

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Main Authors: Carlos Botero, William Sjöström, Emilio Jimenez-Pique, Andrey Koptyug, Lars-Erik Rännar
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:Journal of Manufacturing and Materials Processing
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Online Access:https://www.mdpi.com/2504-4494/9/1/7
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author Carlos Botero
William Sjöström
Emilio Jimenez-Pique
Andrey Koptyug
Lars-Erik Rännar
author_facet Carlos Botero
William Sjöström
Emilio Jimenez-Pique
Andrey Koptyug
Lars-Erik Rännar
author_sort Carlos Botero
collection DOAJ
description The ability to control process parameters over time and build space in electron beam powder bed fusion (PBF-EB) opens up unprecedented opportunities to tailor the process and use materials of a different nature in the same build. The present investigation explored the various methods used to adapt the PBF-EB process for the production of functionally graded materials (FGMs). In this way, two pre-alloyed powders—a stainless steel (SS) powder and a highly alloyed cold work tool steel (TS) powder—were combined during processing in an S20 Arcam machine. Feasibility experiments were first carried out in a downscaled build setup, in which a single powder container was installed on top of the rake system. In the container, one powder was placed on top of the other (SS/TS) so that the gradient materials were produced as the powders were spread and intermixed during the build. The process was later scaled up to an industrial machine setup, where a similar approach was implemented using two configurations of powder disposal: SS/SS + TS/TS and TS/TS + SS/SS. Each configuration had an intermediate layer of powder blend. The FGMs obtained were characterized in terms of their microstructure and local and macromechanical properties. For the microstructural analysis, optical microscopy, scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDX) were performed on the polished cross-sections. This provided evidence of gradual microstructural and compositional transitions in the samples, with a shift from SS to TS and vice versa. Nanoindentation experiments confirmed that there was a consequent gradient in the hardness, stiffness, and wear ratio from the softer and ductile SS to the harder and stiff TS. Scratch experiments revealed gradual evolution in the sliding wear behavior of the printed materials. A “progressive spring” and a “hardness-tailored punching tool” were fabricated as demonstrators. The results obtained demonstrate the great potential to gradually tailor the composition, microstructure, mechanical properties, and wear resistance by combining different powders, and they suggest that any PBF-EB system can be repurposed to build gradient materials without hardware modification. Potential applications include the tooling industry, where hard and wear-resistant materials are needed for the surfaces of tools, with tougher and more ductile materials used in the cores of tools.
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spelling doaj-art-9f58b1a106804c2b93fe659a30c569342025-01-24T13:36:25ZengMDPI AGJournal of Manufacturing and Materials Processing2504-44942024-12-0191710.3390/jmmp9010007Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded SteelsCarlos Botero0William Sjöström1Emilio Jimenez-Pique2Andrey Koptyug3Lars-Erik Rännar4Sports Tech Research Centre, Mid Sweden University, Akademigatan 1, SE-83140 Östersund, SwedenSports Tech Research Centre, Mid Sweden University, Akademigatan 1, SE-83140 Östersund, SwedenBarcelona Research Center in Multiscale Science and Engineering, Universitat Politècnica de Catalunya, Campus Diagonal Besòs—EEBE, 08019 Barcelona, SpainSports Tech Research Centre, Mid Sweden University, Akademigatan 1, SE-83140 Östersund, SwedenSports Tech Research Centre, Mid Sweden University, Akademigatan 1, SE-83140 Östersund, SwedenThe ability to control process parameters over time and build space in electron beam powder bed fusion (PBF-EB) opens up unprecedented opportunities to tailor the process and use materials of a different nature in the same build. The present investigation explored the various methods used to adapt the PBF-EB process for the production of functionally graded materials (FGMs). In this way, two pre-alloyed powders—a stainless steel (SS) powder and a highly alloyed cold work tool steel (TS) powder—were combined during processing in an S20 Arcam machine. Feasibility experiments were first carried out in a downscaled build setup, in which a single powder container was installed on top of the rake system. In the container, one powder was placed on top of the other (SS/TS) so that the gradient materials were produced as the powders were spread and intermixed during the build. The process was later scaled up to an industrial machine setup, where a similar approach was implemented using two configurations of powder disposal: SS/SS + TS/TS and TS/TS + SS/SS. Each configuration had an intermediate layer of powder blend. The FGMs obtained were characterized in terms of their microstructure and local and macromechanical properties. For the microstructural analysis, optical microscopy, scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDX) were performed on the polished cross-sections. This provided evidence of gradual microstructural and compositional transitions in the samples, with a shift from SS to TS and vice versa. Nanoindentation experiments confirmed that there was a consequent gradient in the hardness, stiffness, and wear ratio from the softer and ductile SS to the harder and stiff TS. Scratch experiments revealed gradual evolution in the sliding wear behavior of the printed materials. A “progressive spring” and a “hardness-tailored punching tool” were fabricated as demonstrators. The results obtained demonstrate the great potential to gradually tailor the composition, microstructure, mechanical properties, and wear resistance by combining different powders, and they suggest that any PBF-EB system can be repurposed to build gradient materials without hardware modification. Potential applications include the tooling industry, where hard and wear-resistant materials are needed for the surfaces of tools, with tougher and more ductile materials used in the cores of tools.https://www.mdpi.com/2504-4494/9/1/7electron beam powder bed fusionmulti-materialstool steelstainless steel
spellingShingle Carlos Botero
William Sjöström
Emilio Jimenez-Pique
Andrey Koptyug
Lars-Erik Rännar
Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels
Journal of Manufacturing and Materials Processing
electron beam powder bed fusion
multi-materials
tool steel
stainless steel
title Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels
title_full Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels
title_fullStr Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels
title_full_unstemmed Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels
title_short Small- to Large-Scale Electron Beam Powder Bed Fusion of Functionally Graded Steels
title_sort small to large scale electron beam powder bed fusion of functionally graded steels
topic electron beam powder bed fusion
multi-materials
tool steel
stainless steel
url https://www.mdpi.com/2504-4494/9/1/7
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AT emiliojimenezpique smalltolargescaleelectronbeampowderbedfusionoffunctionallygradedsteels
AT andreykoptyug smalltolargescaleelectronbeampowderbedfusionoffunctionallygradedsteels
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