Nano Phosphorylated Pullulan-Integrated Carboxymethyl Chitosan Scaffold for Regeneration of the Pulp-Dentin Complex: An In vitro Study

Background: To optimize a novel composite scaffold comprising of nano phosphorylated pullulan incorporated carboxymethyl chitosan (nPP-CMC) and to evaluate its cell viability and proliferation in human dental pulp stem cells (hDPSCs). Methodology: Nano phosphorylated pullulan (nPP) in concentrations...

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Main Authors: M Sornamalar, C Dhanavel, G Balavaishnavi, Shahana Shajahan, Kavya Baskar, S Vijaya Raja
Format: Article
Language:English
Published: Wolters Kluwer Medknow Publications 2024-12-01
Series:Journal of Pharmacy and Bioallied Sciences
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Online Access:https://journals.lww.com/10.4103/jpbs.jpbs_1222_24
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Summary:Background: To optimize a novel composite scaffold comprising of nano phosphorylated pullulan incorporated carboxymethyl chitosan (nPP-CMC) and to evaluate its cell viability and proliferation in human dental pulp stem cells (hDPSCs). Methodology: Nano phosphorylated pullulan (nPP) in concentrations of 200 mg, 400 mg, 600 mg, 800 mg, and 1 g was vortexed in 20 mL of distilled water, followed by 30 mins of ultrasonication for even dispersion. 1 g of CMC was added to each nPP mixture, blended for 1 hour to form a hydrogel, and freeze-dried for 18 hours at -20°C to yield nPP-CMC scaffolds in ratios of 1:5, 2:5, 3:5, 4:5, and 1:1. These scaffolds were stored at room temperature. The scaffolds were characterized using SEM-EDX, FT-IR, and XRD. The optimized nPP-CMC (group 1), CMC (group 2), and osteogenic medium (group 3) were tested for cell viability with hDPSCs using the MTT assay at 0, 7, 14, and 21 days. Results: Based on the results of MTT assay, the cell viability and proliferation of nPP-CMC scaffold was comparable to that of CMC in the tested time intervals of 7 and 14 days. The 4:5 nPP-CMC revealed a favourable pore size (60–180 μm) that was suitable for cell seeding and was chosen for further experiments. Cell viability/proliferation rates of hDPSCs loaded 4:5 HAnp- CMC at 21st day was significantly greater than that at 7th day (P < .05). Conclusion: Hence, within the limitations of this in vitro study, it could be concluded that the novel experimental scaffold comprising of nPP-CMC (4:5) is an effective biomaterial that possess good bioactivity and biocompatibility properties. Thus, nPP-CMC biomaterial will have a great futuristic potential for regeneration of pulp dentin complex.
ISSN:0976-4879
0975-7406