The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)

The red palm weevil (RPW; Coleoptera: Curculionidae) is a destructive pest affecting palms worldwide, capable of causing significant economic losses and ecological damage in managed palm ecosystems. Current management heavily relies on synthetic insecticides, but their overuse fosters resistance. &l...

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Main Authors: Camilo Ayra-Pardo, Victor Ramaré, Ana Couto, Mariana Almeida, Ricardo Martins, José Américo Sousa, Maria João Santos
Format: Article
Language:English
Published: MDPI AG 2025-02-01
Series:Toxins
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Online Access:https://www.mdpi.com/2072-6651/17/2/84
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author Camilo Ayra-Pardo
Victor Ramaré
Ana Couto
Mariana Almeida
Ricardo Martins
José Américo Sousa
Maria João Santos
author_facet Camilo Ayra-Pardo
Victor Ramaré
Ana Couto
Mariana Almeida
Ricardo Martins
José Américo Sousa
Maria João Santos
author_sort Camilo Ayra-Pardo
collection DOAJ
description The red palm weevil (RPW; Coleoptera: Curculionidae) is a destructive pest affecting palms worldwide, capable of causing significant economic losses and ecological damage in managed palm ecosystems. Current management heavily relies on synthetic insecticides, but their overuse fosters resistance. <i>Bacillus thuringiensis</i> (Bt) offers a promising alternative, producing toxins selective against various insect orders, including Coleoptera. However, no specific Bt toxin has yet been identified for RPW. This study investigates the toxicity against RPW larvae of the Bt Cry1Ia protoxin, known for its dual activity against Lepidoptera and Coleoptera. A laboratory RPW colony was reared for two generations, ensuring a reliable insect source for bioassays. Cry1Ia was expressed as a 6xHis-tagged fusion protein in <i>Escherichia coli</i> and purified using nickel affinity. Incubation with RPW larval gut proteases for 24 h produced a stable core of ~65 kDa. Diet-incorporation bioassays revealed high Cry1Ia toxicity in neonate larvae. In contrast, the lepidopteran-active Cry1Ac protoxin, used as a robust negative control, was completely degraded after 24 h of in vitro proteolysis and showed no toxicity in bioassays. Cry1Ia-fed larvae exhibited significant midgut cell damage, characteristic of Bt intoxication. These findings highlight Cry1Ia’s strong potential for integration into RPW management programs.
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spelling doaj-art-9ea03032fe00407291b090f93f254ec02025-08-20T03:12:19ZengMDPI AGToxins2072-66512025-02-011728410.3390/toxins17020084The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)Camilo Ayra-Pardo0Victor Ramaré1Ana Couto2Mariana Almeida3Ricardo Martins4José Américo Sousa5Maria João Santos6CIIMAR/CIMAR LA, Interdisciplinary Centre of Marine and Environmental Research, University of Porto, Terminal de Cruzeiros do Porto de Leixões, Avda. General Norton de Matos s/n, 4450-208 Matosinhos, PortugalDepartment of Biology, Polytech Clermont, Campus Universitaire des Cézeaux 2 Avenue Blaise Pascal TSA 60206, 63178 Aubière Cedex, FranceCIIMAR/CIMAR LA, Interdisciplinary Centre of Marine and Environmental Research, University of Porto, Terminal de Cruzeiros do Porto de Leixões, Avda. General Norton de Matos s/n, 4450-208 Matosinhos, PortugalCIIMAR–Biology Department, Faculty of Sciences, University of Porto, 4169-007 Porto, PortugalCIIMAR–Biology Department, Faculty of Sciences, University of Porto, 4169-007 Porto, PortugalCIIMAR/CIMAR LA, Interdisciplinary Centre of Marine and Environmental Research, University of Porto, Terminal de Cruzeiros do Porto de Leixões, Avda. General Norton de Matos s/n, 4450-208 Matosinhos, PortugalCIIMAR/CIMAR LA, Interdisciplinary Centre of Marine and Environmental Research, University of Porto, Terminal de Cruzeiros do Porto de Leixões, Avda. General Norton de Matos s/n, 4450-208 Matosinhos, PortugalThe red palm weevil (RPW; Coleoptera: Curculionidae) is a destructive pest affecting palms worldwide, capable of causing significant economic losses and ecological damage in managed palm ecosystems. Current management heavily relies on synthetic insecticides, but their overuse fosters resistance. <i>Bacillus thuringiensis</i> (Bt) offers a promising alternative, producing toxins selective against various insect orders, including Coleoptera. However, no specific Bt toxin has yet been identified for RPW. This study investigates the toxicity against RPW larvae of the Bt Cry1Ia protoxin, known for its dual activity against Lepidoptera and Coleoptera. A laboratory RPW colony was reared for two generations, ensuring a reliable insect source for bioassays. Cry1Ia was expressed as a 6xHis-tagged fusion protein in <i>Escherichia coli</i> and purified using nickel affinity. Incubation with RPW larval gut proteases for 24 h produced a stable core of ~65 kDa. Diet-incorporation bioassays revealed high Cry1Ia toxicity in neonate larvae. In contrast, the lepidopteran-active Cry1Ac protoxin, used as a robust negative control, was completely degraded after 24 h of in vitro proteolysis and showed no toxicity in bioassays. Cry1Ia-fed larvae exhibited significant midgut cell damage, characteristic of Bt intoxication. These findings highlight Cry1Ia’s strong potential for integration into RPW management programs.https://www.mdpi.com/2072-6651/17/2/84biological controlpalm pestinsect pathogeninsecticidal crystal proteinsinsect bioassaysparaffin histology
spellingShingle Camilo Ayra-Pardo
Victor Ramaré
Ana Couto
Mariana Almeida
Ricardo Martins
José Américo Sousa
Maria João Santos
The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)
Toxins
biological control
palm pest
insect pathogen
insecticidal crystal proteins
insect bioassays
paraffin histology
title The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)
title_full The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)
title_fullStr The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)
title_full_unstemmed The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)
title_short The Proteolytic Activation, Toxic Effects, and Midgut Histopathology of the <i>Bacillus thuringiensis</i> Cry1Ia Protoxin in <i>Rhynchophorus ferrugineus</i> (Coleoptera: Curculionidae)
title_sort proteolytic activation toxic effects and midgut histopathology of the i bacillus thuringiensis i cry1ia protoxin in i rhynchophorus ferrugineus i coleoptera curculionidae
topic biological control
palm pest
insect pathogen
insecticidal crystal proteins
insect bioassays
paraffin histology
url https://www.mdpi.com/2072-6651/17/2/84
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