Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its Mechanism

The dried root of <i>Sanguisorba officinalis</i> L. (commonly known as Diyu) has been studied for its various pharmacological effects, including its antibacterial, antitumor, antioxidant, and anti-inflammatory activities. In the present study, primary cultured vascular endothelial cells...

Full description

Saved in:
Bibliographic Details
Main Authors: Hangyu Jin, Jiaze Li, Shuyuan Wang, Enyi Jin, Jun Zhe Min, Gao Li, Yun Jung Lee, Lihua Cao
Format: Article
Language:English
Published: MDPI AG 2025-04-01
Series:Plants
Subjects:
Online Access:https://www.mdpi.com/2223-7747/14/7/1095
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849730394198376448
author Hangyu Jin
Jiaze Li
Shuyuan Wang
Enyi Jin
Jun Zhe Min
Gao Li
Yun Jung Lee
Lihua Cao
author_facet Hangyu Jin
Jiaze Li
Shuyuan Wang
Enyi Jin
Jun Zhe Min
Gao Li
Yun Jung Lee
Lihua Cao
author_sort Hangyu Jin
collection DOAJ
description The dried root of <i>Sanguisorba officinalis</i> L. (commonly known as Diyu) has been studied for its various pharmacological effects, including its antibacterial, antitumor, antioxidant, and anti-inflammatory activities. In the present study, primary cultured vascular endothelial cells (HUVECs) and isolated phenylephrine-precontracted rat thoracic aortic rings were examined to investigate the possible mechanism of a butanol extract of Diyu (BSO) in its vascular relaxant effect. HUVECs treated with BSO produced a significantly higher amount of nitric oxide (NO) compared to the control. However, its production was inhibited by pretreatment with N<sup>G</sup>-nitro-L-arginine methylester (L-NAME) or wortmannin. BSO also increased the phosphorylation levels of endothelial nitric oxide synthase (eNOS) and Akt. In the aortic ring, BSO relaxed PE-precontracted rat thoracic aortic rings in a concentration-dependent manner. The absence of the vascular endothelium significantly attenuated BSO-induced vasorelaxation. The non-selective NOS inhibitor, L-NAME, and the selective inhibitor of soluble guanylyl cyclase (sGC), 1H-[1,2,4]-oxadiazolo-[4,3-α]-quinoxalin-1-one (ODQ), dramatically inhibited the BSO-induced relaxation effect of the endothelium-intact aortic ring. Ca<sup>2+</sup>-free buffer and intracellular Ca<sup>2+</sup> homeostasis regulators (TG, Gd<sup>3+</sup>, and 2–APB) inhibited BSO-induced vasorelaxation. In Ca<sup>2+</sup>-free Krebs solution, BSO markedly reduced PE-induced contraction. Vasodilation induced by BSO was significantly inhibited by wortmannin, an inhibitor of Akt. Pretreatment with the non-selective inhibitor of Ca<sup>2+</sup>-activated K<sup>+</sup> channels (K<sub>Ca</sub>), tetraethylammonium (TEA), significantly attenuated the BSO-induced vasorelaxant effect. Furthermore, BSO decreased the systolic blood pressure and heart rate in a concentration-dependent manner in rats. In conclusion, BSO induces vasorelaxation via endothelium-dependent signaling, primarily through the activation of the PI3K-Akt-eNOS-NO signaling pathway in endothelial cells, and the activation of the NO-sGC-cGMP-K⁺ channels pathway in vascular smooth muscle cells. Additionally, store-operated Ca<sup>2+</sup> entry (SOCE)-eNOS pathways and the inhibition of Ca<sup>2</sup>⁺ mobilization from intracellular stores contribute to BSO-induced vasorelaxation.
format Article
id doaj-art-9e7531b63dbf4bec9a0f374b039a9ced
institution DOAJ
issn 2223-7747
language English
publishDate 2025-04-01
publisher MDPI AG
record_format Article
series Plants
spelling doaj-art-9e7531b63dbf4bec9a0f374b039a9ced2025-08-20T03:08:53ZengMDPI AGPlants2223-77472025-04-01147109510.3390/plants14071095Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its MechanismHangyu Jin0Jiaze Li1Shuyuan Wang2Enyi Jin3Jun Zhe Min4Gao Li5Yun Jung Lee6Lihua Cao7Clinical Medicine, College of Medicine, Yanbian University, Yanji 133002, ChinaKey Laboratory of Natural Medicines of the Changbai Mountain, Ministry of Education, Medical Pharmacy, Yanbian University, Yanji 133002, ChinaCenter of Morphological Experiment, College of Medicine, Yanbian University, Yanji 133002, ChinaKey Laboratory of Natural Medicines of the Changbai Mountain, Ministry of Education, Medical Pharmacy, Yanbian University, Yanji 133002, ChinaKey Laboratory of Natural Medicines of the Changbai Mountain, Ministry of Education, Medical Pharmacy, Yanbian University, Yanji 133002, ChinaKey Laboratory of Natural Medicines of the Changbai Mountain, Ministry of Education, Medical Pharmacy, Yanbian University, Yanji 133002, ChinaWonkwang-Oriental Medicines Research Institute, Wonkwang University, Iksan 54538, Republic of KoreaKey Laboratory of Natural Medicines of the Changbai Mountain, Ministry of Education, Medical Pharmacy, Yanbian University, Yanji 133002, ChinaThe dried root of <i>Sanguisorba officinalis</i> L. (commonly known as Diyu) has been studied for its various pharmacological effects, including its antibacterial, antitumor, antioxidant, and anti-inflammatory activities. In the present study, primary cultured vascular endothelial cells (HUVECs) and isolated phenylephrine-precontracted rat thoracic aortic rings were examined to investigate the possible mechanism of a butanol extract of Diyu (BSO) in its vascular relaxant effect. HUVECs treated with BSO produced a significantly higher amount of nitric oxide (NO) compared to the control. However, its production was inhibited by pretreatment with N<sup>G</sup>-nitro-L-arginine methylester (L-NAME) or wortmannin. BSO also increased the phosphorylation levels of endothelial nitric oxide synthase (eNOS) and Akt. In the aortic ring, BSO relaxed PE-precontracted rat thoracic aortic rings in a concentration-dependent manner. The absence of the vascular endothelium significantly attenuated BSO-induced vasorelaxation. The non-selective NOS inhibitor, L-NAME, and the selective inhibitor of soluble guanylyl cyclase (sGC), 1H-[1,2,4]-oxadiazolo-[4,3-α]-quinoxalin-1-one (ODQ), dramatically inhibited the BSO-induced relaxation effect of the endothelium-intact aortic ring. Ca<sup>2+</sup>-free buffer and intracellular Ca<sup>2+</sup> homeostasis regulators (TG, Gd<sup>3+</sup>, and 2–APB) inhibited BSO-induced vasorelaxation. In Ca<sup>2+</sup>-free Krebs solution, BSO markedly reduced PE-induced contraction. Vasodilation induced by BSO was significantly inhibited by wortmannin, an inhibitor of Akt. Pretreatment with the non-selective inhibitor of Ca<sup>2+</sup>-activated K<sup>+</sup> channels (K<sub>Ca</sub>), tetraethylammonium (TEA), significantly attenuated the BSO-induced vasorelaxant effect. Furthermore, BSO decreased the systolic blood pressure and heart rate in a concentration-dependent manner in rats. In conclusion, BSO induces vasorelaxation via endothelium-dependent signaling, primarily through the activation of the PI3K-Akt-eNOS-NO signaling pathway in endothelial cells, and the activation of the NO-sGC-cGMP-K⁺ channels pathway in vascular smooth muscle cells. Additionally, store-operated Ca<sup>2+</sup> entry (SOCE)-eNOS pathways and the inhibition of Ca<sup>2</sup>⁺ mobilization from intracellular stores contribute to BSO-induced vasorelaxation.https://www.mdpi.com/2223-7747/14/7/1095<i>Sanguisorba officinalis</i>DiyuvasorelaxationNO-cGMPK<sup>+</sup> channelsPI3K-Akt
spellingShingle Hangyu Jin
Jiaze Li
Shuyuan Wang
Enyi Jin
Jun Zhe Min
Gao Li
Yun Jung Lee
Lihua Cao
Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its Mechanism
Plants
<i>Sanguisorba officinalis</i>
Diyu
vasorelaxation
NO-cGMP
K<sup>+</sup> channels
PI3K-Akt
title Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its Mechanism
title_full Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its Mechanism
title_fullStr Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its Mechanism
title_full_unstemmed Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its Mechanism
title_short Vasodilatory Effect of <i>n</i>-Butanol Extract from <i>Sanguisorba officinalis</i> L. and Its Mechanism
title_sort vasodilatory effect of i n i butanol extract from i sanguisorba officinalis i l and its mechanism
topic <i>Sanguisorba officinalis</i>
Diyu
vasorelaxation
NO-cGMP
K<sup>+</sup> channels
PI3K-Akt
url https://www.mdpi.com/2223-7747/14/7/1095
work_keys_str_mv AT hangyujin vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism
AT jiazeli vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism
AT shuyuanwang vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism
AT enyijin vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism
AT junzhemin vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism
AT gaoli vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism
AT yunjunglee vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism
AT lihuacao vasodilatoryeffectofinibutanolextractfromisanguisorbaofficinalisilanditsmechanism