Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate

Objective: To evaluate the biaxial flexural strength (BFS) of lithium disilicate (L), cemented on different substrates (epoxy resin - E and metal - M) with dual-cure resin cement (Rc) and zinc phosphate cement (Zc), not aged, thermally aged (TC) or thermo-mechanical aged (TC/MC). Material and Metho...

Full description

Saved in:
Bibliographic Details
Main Authors: Leonardo Custódio de Lima, Jean Soares Miranda, Ronaldo Luís Almeida de Carvalho, Aline Serrado de Pinho Barcellos, Marina Amaral, Estevão Tomomitsu Kimpara
Format: Article
Language:English
Published: Universidade Estadual Paulista 2023-10-01
Series:Brazilian Dental Science
Online Access:https://ojs.ict.unesp.br/index.php/cob/article/view/3923
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849228812585271296
author Leonardo Custódio de Lima
Jean Soares Miranda
Ronaldo Luís Almeida de Carvalho
Aline Serrado de Pinho Barcellos
Marina Amaral
Estevão Tomomitsu Kimpara
author_facet Leonardo Custódio de Lima
Jean Soares Miranda
Ronaldo Luís Almeida de Carvalho
Aline Serrado de Pinho Barcellos
Marina Amaral
Estevão Tomomitsu Kimpara
author_sort Leonardo Custódio de Lima
collection DOAJ
description Objective: To evaluate the biaxial flexural strength (BFS) of lithium disilicate (L), cemented on different substrates (epoxy resin - E and metal - M) with dual-cure resin cement (Rc) and zinc phosphate cement (Zc), not aged, thermally aged (TC) or thermo-mechanical aged (TC/MC). Material and Methods: Disks of L, E, and M were fabricated, and the cementation was performed according to the following groups: ERc (L+E+Rc); MRc (L+M+Rc); MZc (L+M+Zc); EZc (L+E+Zc). Ten samples from each described group were tested in BFS, ten more samples were subjected to TC (1×104 cycles between 5 ºC and 55 ºC water), and the last 10 samples were subjected to TC/MC (MC: 1.2×106 cycles, 50 N, 3.8 Hz). The BFS test was performed and scanning electron microscopy (SEM) was performed to evaluate the failure mode. The effect of the cementation strategy (cement/substrate) was compared in each aging method and the effect of the aging method was evaluated for each cementation strategy by one-way ANOVA and Tukey post-hoc test (a=0.05). Results: The strength values were highest to M (237.8 ~ 463.9 MPa), in comparison to the E (41.03 ~ 66.76 MPa), despite aging and luting agent. Flexural strength data decreased after TC and TC/MC in groups cemented with Zc, but was stable when cemented with Rc. SEM analysis indicated that failure origins were located at the tensile surface of the L. Conclusion: Lithium disilicate discs cemented to the metallic substrate presented the highest biaxial flexural strength. The cementation with dual-cure resin cement did not decrease BFS after aging. KEYWORDS Aging; Cementation; Ceramics; Flexural strength; Lithium disilicate.
format Article
id doaj-art-9bfb72bceeb948928eb74cb3b2b61810
institution Kabale University
issn 2178-6011
language English
publishDate 2023-10-01
publisher Universidade Estadual Paulista
record_format Article
series Brazilian Dental Science
spelling doaj-art-9bfb72bceeb948928eb74cb3b2b618102025-08-22T14:53:10ZengUniversidade Estadual PaulistaBrazilian Dental Science2178-60112023-10-0126410.4322/bds.2023.e3923Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicateLeonardo Custódio de Lima 0https://orcid.org/0000-0002-8016-9636Jean Soares Miranda1https://orcid.org/0000-0001-5379-0155Ronaldo Luís Almeida de Carvalho2https://orcid.org/0000-0002-5383-7758Aline Serrado de Pinho Barcellos3https://orcid.org/0000-0001-9638-7147Marina Amaral4https://orcid.org/0000-0002-4301-2760Estevão Tomomitsu Kimpara5https://orcid.org/0000-0003-0586-4644Departamento de Odontologia Restauradora, Faculdade de Odontologia, Universidade de São Paulo, SP, Brazil.Departamento de Odontologia, Universidade Federal de Juiz de Fora, Governador Valadares, MG, Brazil.Departamento de Odontologia, Universidade Braz Cubas, Mogi das Cruzes, SP, Brazil.Departamento de Materiais e Dentários e Prótese, Instituto de Ciência e Tecnologia, Unesp, São José dos Campos, SP, Brazil.Departamento de Odontologia, Universidade de Taubaté, Taubaté, SP, Brazil.Departamento de Materiais e Dentários e Prótese, Instituto de Ciência e Tecnologia, Unesp, São José dos Campos, SP, Brazil. Objective: To evaluate the biaxial flexural strength (BFS) of lithium disilicate (L), cemented on different substrates (epoxy resin - E and metal - M) with dual-cure resin cement (Rc) and zinc phosphate cement (Zc), not aged, thermally aged (TC) or thermo-mechanical aged (TC/MC). Material and Methods: Disks of L, E, and M were fabricated, and the cementation was performed according to the following groups: ERc (L+E+Rc); MRc (L+M+Rc); MZc (L+M+Zc); EZc (L+E+Zc). Ten samples from each described group were tested in BFS, ten more samples were subjected to TC (1×104 cycles between 5 ºC and 55 ºC water), and the last 10 samples were subjected to TC/MC (MC: 1.2×106 cycles, 50 N, 3.8 Hz). The BFS test was performed and scanning electron microscopy (SEM) was performed to evaluate the failure mode. The effect of the cementation strategy (cement/substrate) was compared in each aging method and the effect of the aging method was evaluated for each cementation strategy by one-way ANOVA and Tukey post-hoc test (a=0.05). Results: The strength values were highest to M (237.8 ~ 463.9 MPa), in comparison to the E (41.03 ~ 66.76 MPa), despite aging and luting agent. Flexural strength data decreased after TC and TC/MC in groups cemented with Zc, but was stable when cemented with Rc. SEM analysis indicated that failure origins were located at the tensile surface of the L. Conclusion: Lithium disilicate discs cemented to the metallic substrate presented the highest biaxial flexural strength. The cementation with dual-cure resin cement did not decrease BFS after aging. KEYWORDS Aging; Cementation; Ceramics; Flexural strength; Lithium disilicate. https://ojs.ict.unesp.br/index.php/cob/article/view/3923
spellingShingle Leonardo Custódio de Lima
Jean Soares Miranda
Ronaldo Luís Almeida de Carvalho
Aline Serrado de Pinho Barcellos
Marina Amaral
Estevão Tomomitsu Kimpara
Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
Brazilian Dental Science
title Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_full Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_fullStr Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_full_unstemmed Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_short Influence of substrate, cement and aging on the biaxial flexural strength of lithium disilicate
title_sort influence of substrate cement and aging on the biaxial flexural strength of lithium disilicate
url https://ojs.ict.unesp.br/index.php/cob/article/view/3923
work_keys_str_mv AT leonardocustodiodelima influenceofsubstratecementandagingonthebiaxialflexuralstrengthoflithiumdisilicate
AT jeansoaresmiranda influenceofsubstratecementandagingonthebiaxialflexuralstrengthoflithiumdisilicate
AT ronaldoluisalmeidadecarvalho influenceofsubstratecementandagingonthebiaxialflexuralstrengthoflithiumdisilicate
AT alineserradodepinhobarcellos influenceofsubstratecementandagingonthebiaxialflexuralstrengthoflithiumdisilicate
AT marinaamaral influenceofsubstratecementandagingonthebiaxialflexuralstrengthoflithiumdisilicate
AT estevaotomomitsukimpara influenceofsubstratecementandagingonthebiaxialflexuralstrengthoflithiumdisilicate