Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technology

The paper presents the fabrication of chessboard-structured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings by electrospray mask in-situ forming technique. The influence of the coating's structure and components on microstructure, film-substrate adhesion strength, and reciprocating we...

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Main Authors: Zhihui Zhang, Jianxin Deng, Lingxuan Fan, Junyan Wang
Format: Article
Language:English
Published: Elsevier 2025-03-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425003904
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author Zhihui Zhang
Jianxin Deng
Lingxuan Fan
Junyan Wang
author_facet Zhihui Zhang
Jianxin Deng
Lingxuan Fan
Junyan Wang
author_sort Zhihui Zhang
collection DOAJ
description The paper presents the fabrication of chessboard-structured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings by electrospray mask in-situ forming technique. The influence of the coating's structure and components on microstructure, film-substrate adhesion strength, and reciprocating wear performance were studied. The results showed that the chessboard structure of the hard coating had a high surface energy of 83.45 mJ/m2, which enhanced the adhesion of the lubricant coating. The addition of graphite (C) improved the uniformity, thermal stability, and lubrication of the (CFx)n/CaF2 lubricant coating. Within the 25–600 °C temperature range, the chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coating all exhibited low friction coefficients, which attributed to the synergistic effect between chessboard structure and coating material.
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institution OA Journals
issn 2238-7854
language English
publishDate 2025-03-01
publisher Elsevier
record_format Article
series Journal of Materials Research and Technology
spelling doaj-art-9b563d3dd048468997da5022e4b3bae52025-08-20T02:14:31ZengElsevierJournal of Materials Research and Technology2238-78542025-03-01354438445610.1016/j.jmrt.2025.02.143Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technologyZhihui Zhang0Jianxin Deng1Lingxuan Fan2Junyan Wang3Key Laboratory of High Efficiency and Clean Mechanical Manufacture of MOE, School of Mechanical Engineering, Shandong University, Jinan 250061, ChinaCorresponding author.; Key Laboratory of High Efficiency and Clean Mechanical Manufacture of MOE, School of Mechanical Engineering, Shandong University, Jinan 250061, ChinaKey Laboratory of High Efficiency and Clean Mechanical Manufacture of MOE, School of Mechanical Engineering, Shandong University, Jinan 250061, ChinaKey Laboratory of High Efficiency and Clean Mechanical Manufacture of MOE, School of Mechanical Engineering, Shandong University, Jinan 250061, ChinaThe paper presents the fabrication of chessboard-structured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings by electrospray mask in-situ forming technique. The influence of the coating's structure and components on microstructure, film-substrate adhesion strength, and reciprocating wear performance were studied. The results showed that the chessboard structure of the hard coating had a high surface energy of 83.45 mJ/m2, which enhanced the adhesion of the lubricant coating. The addition of graphite (C) improved the uniformity, thermal stability, and lubrication of the (CFx)n/CaF2 lubricant coating. Within the 25–600 °C temperature range, the chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coating all exhibited low friction coefficients, which attributed to the synergistic effect between chessboard structure and coating material.http://www.sciencedirect.com/science/article/pii/S2238785425003904Electrospray mask in-situ formationComposite coatingReciprocating wearWide temperature range
spellingShingle Zhihui Zhang
Jianxin Deng
Lingxuan Fan
Junyan Wang
Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technology
Journal of Materials Research and Technology
Electrospray mask in-situ formation
Composite coating
Reciprocating wear
Wide temperature range
title Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technology
title_full Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technology
title_fullStr Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technology
title_full_unstemmed Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technology
title_short Microstructure and high-temperature tribological properties of chessboard-textured (CFx)n/CaF2/C–ZrO2/TiO2 lubricant-hard alternate coatings fabricated by electrospray mask in-situ forming technology
title_sort microstructure and high temperature tribological properties of chessboard textured cfx n caf2 c zro2 tio2 lubricant hard alternate coatings fabricated by electrospray mask in situ forming technology
topic Electrospray mask in-situ formation
Composite coating
Reciprocating wear
Wide temperature range
url http://www.sciencedirect.com/science/article/pii/S2238785425003904
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AT jianxindeng microstructureandhightemperaturetribologicalpropertiesofchessboardtexturedcfxncaf2czro2tio2lubricanthardalternatecoatingsfabricatedbyelectrospraymaskinsituformingtechnology
AT lingxuanfan microstructureandhightemperaturetribologicalpropertiesofchessboardtexturedcfxncaf2czro2tio2lubricanthardalternatecoatingsfabricatedbyelectrospraymaskinsituformingtechnology
AT junyanwang microstructureandhightemperaturetribologicalpropertiesofchessboardtexturedcfxncaf2czro2tio2lubricanthardalternatecoatingsfabricatedbyelectrospraymaskinsituformingtechnology