Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer Coating

Per- and polyfluoroalkyl substances (PFASs), used since the 1940s, are persistent and carcinogenic pollutants. Water is a major exposure route; effective removal is essential. While nanofiltration (NF) and reverse osmosis (RO) are effective but costly, ultrafiltration (UF) membranes offer advantages...

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Main Authors: Oruc Kaan Turk, Mehmet Cakmakci, Ismail Hakki Zengin, Dogan Karadag, Ebubekir Yuksel
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Membranes
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Online Access:https://www.mdpi.com/2077-0375/15/6/172
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author Oruc Kaan Turk
Mehmet Cakmakci
Ismail Hakki Zengin
Dogan Karadag
Ebubekir Yuksel
author_facet Oruc Kaan Turk
Mehmet Cakmakci
Ismail Hakki Zengin
Dogan Karadag
Ebubekir Yuksel
author_sort Oruc Kaan Turk
collection DOAJ
description Per- and polyfluoroalkyl substances (PFASs), used since the 1940s, are persistent and carcinogenic pollutants. Water is a major exposure route; effective removal is essential. While nanofiltration (NF) and reverse osmosis (RO) are effective but costly, ultrafiltration (UF) membranes offer advantages such as lower cost and higher flux, but their relatively large pore size makes them ineffective for PFAS compounds like perfluorooctane sulfonic acid (PFOS) and perfluorooctanoic acid (PFOA). Since PFAS removal depends on both pore size and surface properties, this study investigates the effect of polyelectrolyte multilayer coatings using poly(allylamine hydrochloride) (PAH) and poly(acrylic acid) (PAA) on the zeta potential of UF membranes. Pristine UF membranes showed limited performance (UP150: ~2% for both PFOS and PFOA; UP020: 34.4% PFOS, 24.1% PFOA), while coating significantly enhanced removal (coated UP150: 45.3% PFOS, 43.4% PFOA; coated UP020: 77.8% PFOS, 73.3% PFOA). The modified UF membranes achieved PFAS removal efficiencies significantly closer to NF membranes, though still below those of RO (e.g., BW30XLE: up to 91.0% PFOS, 88.3% PFOA; NP030: up to 81.0% PFOS, 79.3% PFOA). Findings emphasize the importance of membrane surface charge and suggest that modified UF membranes offer a promising, low-cost alternative for PFAS removal under low-pressure conditions.
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spelling doaj-art-9b4f83633dcb433c84c1d2624d2e9e712025-08-20T02:21:04ZengMDPI AGMembranes2077-03752025-06-0115617210.3390/membranes15060172Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer CoatingOruc Kaan Turk0Mehmet Cakmakci1Ismail Hakki Zengin2Dogan Karadag3Ebubekir Yuksel4Department of Environmental Engineering, Faculty of Civil Engineering, Yıldız Technical University, İstanbul 34220, TürkiyeDepartment of Environmental Engineering, Faculty of Civil Engineering, Yıldız Technical University, İstanbul 34220, TürkiyeDepartment of Environmental Engineering, Faculty of Civil Engineering, Yıldız Technical University, İstanbul 34220, TürkiyeDepartment of Environmental Engineering, Faculty of Civil Engineering, Yıldız Technical University, İstanbul 34220, TürkiyeDepartment of Environmental Engineering, Faculty of Engineering, Gebze Technical University, Kocaeli 41400, TürkiyePer- and polyfluoroalkyl substances (PFASs), used since the 1940s, are persistent and carcinogenic pollutants. Water is a major exposure route; effective removal is essential. While nanofiltration (NF) and reverse osmosis (RO) are effective but costly, ultrafiltration (UF) membranes offer advantages such as lower cost and higher flux, but their relatively large pore size makes them ineffective for PFAS compounds like perfluorooctane sulfonic acid (PFOS) and perfluorooctanoic acid (PFOA). Since PFAS removal depends on both pore size and surface properties, this study investigates the effect of polyelectrolyte multilayer coatings using poly(allylamine hydrochloride) (PAH) and poly(acrylic acid) (PAA) on the zeta potential of UF membranes. Pristine UF membranes showed limited performance (UP150: ~2% for both PFOS and PFOA; UP020: 34.4% PFOS, 24.1% PFOA), while coating significantly enhanced removal (coated UP150: 45.3% PFOS, 43.4% PFOA; coated UP020: 77.8% PFOS, 73.3% PFOA). The modified UF membranes achieved PFAS removal efficiencies significantly closer to NF membranes, though still below those of RO (e.g., BW30XLE: up to 91.0% PFOS, 88.3% PFOA; NP030: up to 81.0% PFOS, 79.3% PFOA). Findings emphasize the importance of membrane surface charge and suggest that modified UF membranes offer a promising, low-cost alternative for PFAS removal under low-pressure conditions.https://www.mdpi.com/2077-0375/15/6/172PFOAPFOSPFASmembrane technologyzeta potential
spellingShingle Oruc Kaan Turk
Mehmet Cakmakci
Ismail Hakki Zengin
Dogan Karadag
Ebubekir Yuksel
Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer Coating
Membranes
PFOA
PFOS
PFAS
membrane technology
zeta potential
title Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer Coating
title_full Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer Coating
title_fullStr Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer Coating
title_full_unstemmed Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer Coating
title_short Improving PFAS Rejection by Ultrafiltration Membranes via Polyelectrolyte Multilayer Coating
title_sort improving pfas rejection by ultrafiltration membranes via polyelectrolyte multilayer coating
topic PFOA
PFOS
PFAS
membrane technology
zeta potential
url https://www.mdpi.com/2077-0375/15/6/172
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