Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives

Abstract The 4-anilinoquinazoline sulfonamide derivatives in medicinal chemistry are well-known antitumor backbones via different mechanisms. Herein, we reported the synthesis of five new 2,4-disubstituted-6-iodoquinazoline derivatives coded compounds 3a–e. The respective compounds were examined for...

Full description

Saved in:
Bibliographic Details
Main Authors: Khaled M. Aboshanab, Amr S. Bishr, Siti Azma Jusoh, Mohammad Y. Alshahrani, Khondaker Miraz Rahman, Ahmed M. Alafeefy
Format: Article
Language:English
Published: SpringerOpen 2025-06-01
Series:AMB Express
Subjects:
Online Access:https://doi.org/10.1186/s13568-025-01899-1
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850207441261690880
author Khaled M. Aboshanab
Amr S. Bishr
Siti Azma Jusoh
Mohammad Y. Alshahrani
Khondaker Miraz Rahman
Ahmed M. Alafeefy
author_facet Khaled M. Aboshanab
Amr S. Bishr
Siti Azma Jusoh
Mohammad Y. Alshahrani
Khondaker Miraz Rahman
Ahmed M. Alafeefy
author_sort Khaled M. Aboshanab
collection DOAJ
description Abstract The 4-anilinoquinazoline sulfonamide derivatives in medicinal chemistry are well-known antitumor backbones via different mechanisms. Herein, we reported the synthesis of five new 2,4-disubstituted-6-iodoquinazoline derivatives coded compounds 3a–e. The respective compounds were examined for their antiproliferative, antimicrobial, and carbonic anhydrase XII (CAXII) inhibitory activity against four cancerous cell lines. Compound 3c was proven to be the most effective as an anticancer. It stopped the growth of the four used tumor cell lines at concentrations ranging from 4.0 to 8.0 µM as compared to the reference doxorubicin (2.3–3.25 µM). Compound 3b, was able to stop the proliferation of the tumor cell lines with IC50 between 6.0 and 9.0 µM. The five compounds exhibited both broad-spectrum and antifungal action; however, their antibacterial activities against Gram-positive bacteria were superior to those of Gram-negative. Compound 3c showed the strongest antibacterial and antifungal activities, followed by compound 3b. In conclusion, the 4-substituted-anilino derivatives equipped with sulfonamide at position 4 of the quinazoline nucleus are suitable antitumor lead compounds. Moreover, the 4-methoxyphenyl substituent at position-2 has a better impact on activity than unsubstituted or even other substituents. The lab results are aligned with molecular docking analysis of the respective compounds against the potential targets, including CAXII, human thymidylate synthase (hTS), and human thymidine kinase (hTK), for the anticancer activities and DHFR of E. coli and S. aureus for the antibacterial properties. Compounds 3c and 3b are highly recommended for preclinical and clinical evaluation as anticancer and/or antibacterial agents for potential use in humans.
format Article
id doaj-art-9a78db2c5f7041f7beb2c7f149dd6d64
institution OA Journals
issn 2191-0855
language English
publishDate 2025-06-01
publisher SpringerOpen
record_format Article
series AMB Express
spelling doaj-art-9a78db2c5f7041f7beb2c7f149dd6d642025-08-20T02:10:31ZengSpringerOpenAMB Express2191-08552025-06-0115111510.1186/s13568-025-01899-1Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivativesKhaled M. Aboshanab0Amr S. Bishr1Siti Azma Jusoh2Mohammad Y. Alshahrani3Khondaker Miraz Rahman4Ahmed M. Alafeefy5Department of Microbiology and Immunology, Faculty of Pharmacy, Ain Shams UniversityDepartment of Microbiology and Immunology, Faculty of Pharmacy, Ain Shams UniversityDepartment of Pharmacology and Life Sciences, Faculty of Pharmacy, Universiti Teknologi MARA (UiTM), Puncak Alam CampusCentral Labs, King Khalid UniversitySchool of Cancer and Pharmaceutical Science, King’s College LondonDepartment of Pharmaceutical Chemistry, Faculty of Pharmacy, Universiti Teknologi MARA (UiTM), Puncak Alam CampusAbstract The 4-anilinoquinazoline sulfonamide derivatives in medicinal chemistry are well-known antitumor backbones via different mechanisms. Herein, we reported the synthesis of five new 2,4-disubstituted-6-iodoquinazoline derivatives coded compounds 3a–e. The respective compounds were examined for their antiproliferative, antimicrobial, and carbonic anhydrase XII (CAXII) inhibitory activity against four cancerous cell lines. Compound 3c was proven to be the most effective as an anticancer. It stopped the growth of the four used tumor cell lines at concentrations ranging from 4.0 to 8.0 µM as compared to the reference doxorubicin (2.3–3.25 µM). Compound 3b, was able to stop the proliferation of the tumor cell lines with IC50 between 6.0 and 9.0 µM. The five compounds exhibited both broad-spectrum and antifungal action; however, their antibacterial activities against Gram-positive bacteria were superior to those of Gram-negative. Compound 3c showed the strongest antibacterial and antifungal activities, followed by compound 3b. In conclusion, the 4-substituted-anilino derivatives equipped with sulfonamide at position 4 of the quinazoline nucleus are suitable antitumor lead compounds. Moreover, the 4-methoxyphenyl substituent at position-2 has a better impact on activity than unsubstituted or even other substituents. The lab results are aligned with molecular docking analysis of the respective compounds against the potential targets, including CAXII, human thymidylate synthase (hTS), and human thymidine kinase (hTK), for the anticancer activities and DHFR of E. coli and S. aureus for the antibacterial properties. Compounds 3c and 3b are highly recommended for preclinical and clinical evaluation as anticancer and/or antibacterial agents for potential use in humans.https://doi.org/10.1186/s13568-025-01899-1QuinazolineSulfonamideCarbonic anhydraseCancerAntimicrobialMolecular docking
spellingShingle Khaled M. Aboshanab
Amr S. Bishr
Siti Azma Jusoh
Mohammad Y. Alshahrani
Khondaker Miraz Rahman
Ahmed M. Alafeefy
Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives
AMB Express
Quinazoline
Sulfonamide
Carbonic anhydrase
Cancer
Antimicrobial
Molecular docking
title Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives
title_full Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives
title_fullStr Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives
title_full_unstemmed Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives
title_short Anticancer, antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives
title_sort anticancer antimicrobial and molecular docking analysis of newly synthesized iodoquinazoline derivatives
topic Quinazoline
Sulfonamide
Carbonic anhydrase
Cancer
Antimicrobial
Molecular docking
url https://doi.org/10.1186/s13568-025-01899-1
work_keys_str_mv AT khaledmaboshanab anticancerantimicrobialandmoleculardockinganalysisofnewlysynthesizediodoquinazolinederivatives
AT amrsbishr anticancerantimicrobialandmoleculardockinganalysisofnewlysynthesizediodoquinazolinederivatives
AT sitiazmajusoh anticancerantimicrobialandmoleculardockinganalysisofnewlysynthesizediodoquinazolinederivatives
AT mohammadyalshahrani anticancerantimicrobialandmoleculardockinganalysisofnewlysynthesizediodoquinazolinederivatives
AT khondakermirazrahman anticancerantimicrobialandmoleculardockinganalysisofnewlysynthesizediodoquinazolinederivatives
AT ahmedmalafeefy anticancerantimicrobialandmoleculardockinganalysisofnewlysynthesizediodoquinazolinederivatives