Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVD

The inherent brittleness of tungsten severely limits its application as plasma-facing materials (PFMs). Tungsten fiber (Wf) reinforced tungsten (W) composites (Wf/W) offer a promising toughening approach for tungsten. However, this toughening method faces significant challenges, such as how to optim...

Full description

Saved in:
Bibliographic Details
Main Authors: Chuan Wu, Youping Lu, Juan Du, Pan Wen, Jun Tang, Tianyu Zhao, Jiming Chen, Pinghuai Wang, Xiang Liu
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Nuclear Materials and Energy
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2352179125000948
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850123624887877632
author Chuan Wu
Youping Lu
Juan Du
Pan Wen
Jun Tang
Tianyu Zhao
Jiming Chen
Pinghuai Wang
Xiang Liu
author_facet Chuan Wu
Youping Lu
Juan Du
Pan Wen
Jun Tang
Tianyu Zhao
Jiming Chen
Pinghuai Wang
Xiang Liu
author_sort Chuan Wu
collection DOAJ
description The inherent brittleness of tungsten severely limits its application as plasma-facing materials (PFMs). Tungsten fiber (Wf) reinforced tungsten (W) composites (Wf/W) offer a promising toughening approach for tungsten. However, this toughening method faces significant challenges, such as how to optimize the interface strength and preventing damage to the fiber-reinforced structure. In this study, four types of interfaces (Y, Cr, Y2O3, and YSZ) were prepared using magnetron sputtering technology, followed by the fabrication of single Wf-reinforced W composites via chemical vapor deposition (CVD). The fracture behavior of the Wf/W composite before and after the annealing process was investigated through three-point bending tests. The results indicate that the interfaces including yttrium (Y), yttrium oxide (Y2O3), and yttria-stabilized zirconia (YSZ) all exhibit weak binding strength, leading to interface debonding during the three-point bending test and resulting in ductile fracture behavior for the composite. In contrast, the chromium (Cr) interface displays a high binding strength and lead to brittle fracture behavior for the composite. After annealing at 1000 °C, the binding strength of Y2O3 and YSZ interfaces increases, which causes the brittle fracture behavior of the composite. After annealing at 1600 °C, the Cr interface diffused into the Wf and caused the recrystallization of the Wf. The Y interface underwent melting and solidification, leading to a decrease of the binding strength. The interface strength ranks as follows: Cr > YSZ > Y2O3 > Y.
format Article
id doaj-art-99d28ef303da40e798d502c8e42c90ec
institution OA Journals
issn 2352-1791
language English
publishDate 2025-06-01
publisher Elsevier
record_format Article
series Nuclear Materials and Energy
spelling doaj-art-99d28ef303da40e798d502c8e42c90ec2025-08-20T02:34:33ZengElsevierNuclear Materials and Energy2352-17912025-06-014310195210.1016/j.nme.2025.101952Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVDChuan Wu0Youping Lu1Juan Du2Pan Wen3Jun Tang4Tianyu Zhao5Jiming Chen6Pinghuai Wang7Xiang Liu8Fusion Science Center, Southwestern Institute of Physics, Chengdu 610225. China; Key Laboratory of Radiation Physics and Technology of Ministry of Education, Institute of Nuclear Science and Technology, Sichuan University, Chengdu 610064, ChinaFusion Science Center, Southwestern Institute of Physics, Chengdu 610225. ChinaFusion Science Center, Southwestern Institute of Physics, Chengdu 610225. China; Corresponding author.Fusion Science Center, Southwestern Institute of Physics, Chengdu 610225. ChinaKey Laboratory of Radiation Physics and Technology of Ministry of Education, Institute of Nuclear Science and Technology, Sichuan University, Chengdu 610064, ChinaFusion Science Center, Southwestern Institute of Physics, Chengdu 610225. China; Key Laboratory of Radiation Physics and Technology of Ministry of Education, Institute of Nuclear Science and Technology, Sichuan University, Chengdu 610064, ChinaFusion Science Center, Southwestern Institute of Physics, Chengdu 610225. ChinaFusion Science Center, Southwestern Institute of Physics, Chengdu 610225. ChinaFusion Science Center, Southwestern Institute of Physics, Chengdu 610225. ChinaThe inherent brittleness of tungsten severely limits its application as plasma-facing materials (PFMs). Tungsten fiber (Wf) reinforced tungsten (W) composites (Wf/W) offer a promising toughening approach for tungsten. However, this toughening method faces significant challenges, such as how to optimize the interface strength and preventing damage to the fiber-reinforced structure. In this study, four types of interfaces (Y, Cr, Y2O3, and YSZ) were prepared using magnetron sputtering technology, followed by the fabrication of single Wf-reinforced W composites via chemical vapor deposition (CVD). The fracture behavior of the Wf/W composite before and after the annealing process was investigated through three-point bending tests. The results indicate that the interfaces including yttrium (Y), yttrium oxide (Y2O3), and yttria-stabilized zirconia (YSZ) all exhibit weak binding strength, leading to interface debonding during the three-point bending test and resulting in ductile fracture behavior for the composite. In contrast, the chromium (Cr) interface displays a high binding strength and lead to brittle fracture behavior for the composite. After annealing at 1000 °C, the binding strength of Y2O3 and YSZ interfaces increases, which causes the brittle fracture behavior of the composite. After annealing at 1600 °C, the Cr interface diffused into the Wf and caused the recrystallization of the Wf. The Y interface underwent melting and solidification, leading to a decrease of the binding strength. The interface strength ranks as follows: Cr > YSZ > Y2O3 > Y.http://www.sciencedirect.com/science/article/pii/S2352179125000948Fiber reinforcedTungsten fiberInterfaceThree-point bendingPseudo toughening
spellingShingle Chuan Wu
Youping Lu
Juan Du
Pan Wen
Jun Tang
Tianyu Zhao
Jiming Chen
Pinghuai Wang
Xiang Liu
Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVD
Nuclear Materials and Energy
Fiber reinforced
Tungsten fiber
Interface
Three-point bending
Pseudo toughening
title Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVD
title_full Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVD
title_fullStr Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVD
title_full_unstemmed Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVD
title_short Study on the annealing and three-point bending fracture behavior of single W fiber-reinforced W composites with multiple interfaces prepared by CVD
title_sort study on the annealing and three point bending fracture behavior of single w fiber reinforced w composites with multiple interfaces prepared by cvd
topic Fiber reinforced
Tungsten fiber
Interface
Three-point bending
Pseudo toughening
url http://www.sciencedirect.com/science/article/pii/S2352179125000948
work_keys_str_mv AT chuanwu studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT youpinglu studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT juandu studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT panwen studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT juntang studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT tianyuzhao studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT jimingchen studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT pinghuaiwang studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd
AT xiangliu studyontheannealingandthreepointbendingfracturebehaviorofsinglewfiberreinforcedwcompositeswithmultipleinterfacespreparedbycvd