Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal Fires

In order to overcome the deficiency of the existing fire control technology and control coal spontaneous combustion by sealing air leakages in coal mines, inorganic solidified foam (ISF) with high closed porosity was developed. The effect of sodium dodecyl sulfate (SDS) concentration on the porosity...

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Main Authors: Yi Lu, Botao Qin
Format: Article
Language:English
Published: Wiley 2015-01-01
Series:Advances in Materials Science and Engineering
Online Access:http://dx.doi.org/10.1155/2015/724548
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author Yi Lu
Botao Qin
author_facet Yi Lu
Botao Qin
author_sort Yi Lu
collection DOAJ
description In order to overcome the deficiency of the existing fire control technology and control coal spontaneous combustion by sealing air leakages in coal mines, inorganic solidified foam (ISF) with high closed porosity was developed. The effect of sodium dodecyl sulfate (SDS) concentration on the porosity of the foams was investigated. The results showed that the optimized closed porosity of the solidified foam was 38.65 wt.% for an SDS concentration of approximately 7.4×10-3 mol/L. Based on observations of the microstructure of the pore walls after solidification, it was inferred that an equilibrium between the hydration process and the drainage process existed. Therefore, the ISF was improved using three different systems. Gelatin can increase the viscosity of the continuous phase to form a viscoelastic film around the air cells, and the SDS + gelatin system can create a mixed surfactant layer at gas/liquid interfaces. The accelerator (AC) accelerates the hydration process and coagulation of the pore walls before the end of drainage. The mixed SDS + gelatin + AC systems produced an ISF with a total porosity of 79.89% and a closed porosity of 66.89%, which verified the proposed stabilization mechanism.
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spelling doaj-art-996c02e95d7e40c5b8b943d28964242e2025-08-20T03:37:02ZengWileyAdvances in Materials Science and Engineering1687-84341687-84422015-01-01201510.1155/2015/724548724548Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal FiresYi Lu0Botao Qin1State Key Laboratory of Coal Resources and Mine Safety, China University of Mining and Technology, Xuzhou, Jiangsu 221008, ChinaState Key Laboratory of Coal Resources and Mine Safety, China University of Mining and Technology, Xuzhou, Jiangsu 221008, ChinaIn order to overcome the deficiency of the existing fire control technology and control coal spontaneous combustion by sealing air leakages in coal mines, inorganic solidified foam (ISF) with high closed porosity was developed. The effect of sodium dodecyl sulfate (SDS) concentration on the porosity of the foams was investigated. The results showed that the optimized closed porosity of the solidified foam was 38.65 wt.% for an SDS concentration of approximately 7.4×10-3 mol/L. Based on observations of the microstructure of the pore walls after solidification, it was inferred that an equilibrium between the hydration process and the drainage process existed. Therefore, the ISF was improved using three different systems. Gelatin can increase the viscosity of the continuous phase to form a viscoelastic film around the air cells, and the SDS + gelatin system can create a mixed surfactant layer at gas/liquid interfaces. The accelerator (AC) accelerates the hydration process and coagulation of the pore walls before the end of drainage. The mixed SDS + gelatin + AC systems produced an ISF with a total porosity of 79.89% and a closed porosity of 66.89%, which verified the proposed stabilization mechanism.http://dx.doi.org/10.1155/2015/724548
spellingShingle Yi Lu
Botao Qin
Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal Fires
Advances in Materials Science and Engineering
title Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal Fires
title_full Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal Fires
title_fullStr Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal Fires
title_full_unstemmed Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal Fires
title_short Experimental Investigation of Closed Porosity of Inorganic Solidified Foam Designed to Prevent Coal Fires
title_sort experimental investigation of closed porosity of inorganic solidified foam designed to prevent coal fires
url http://dx.doi.org/10.1155/2015/724548
work_keys_str_mv AT yilu experimentalinvestigationofclosedporosityofinorganicsolidifiedfoamdesignedtopreventcoalfires
AT botaoqin experimentalinvestigationofclosedporosityofinorganicsolidifiedfoamdesignedtopreventcoalfires