Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological Approach

In this work, we synthesized the Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>3+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) nan...

Full description

Saved in:
Bibliographic Details
Main Authors: Liza Saher, Adel Benali, Saoussen Haddad, Essebti Dhahri, Manuel P. F. Graça, Benilde F. O. Costa, Luisa A. Helguero, Artur M. S. Silva
Format: Article
Language:English
Published: MDPI AG 2025-05-01
Series:Crystals
Subjects:
Online Access:https://www.mdpi.com/2073-4352/15/5/482
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849327559294058496
author Liza Saher
Adel Benali
Saoussen Haddad
Essebti Dhahri
Manuel P. F. Graça
Benilde F. O. Costa
Luisa A. Helguero
Artur M. S. Silva
author_facet Liza Saher
Adel Benali
Saoussen Haddad
Essebti Dhahri
Manuel P. F. Graça
Benilde F. O. Costa
Luisa A. Helguero
Artur M. S. Silva
author_sort Liza Saher
collection DOAJ
description In this work, we synthesized the Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>3+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) nanoparticles via the auto-combustion method. The cell viability against two breast cancer cells (MDA-MB-231 and T-47D cells) and the PC3 prostate cancer cells were carefully analyzed and correlated with the structural parameters and particle size values as well as the chemical composition. The produced compounds’ morphological and structural characteristics were performed using scanning transmission microscopy (TEM) and X-ray Diffraction (XRD). For all compounds, the analyses of the XRD experimental data revealed a structurally reversed cubic spinel with space group Fd-3m. All of the compounds had crystallites smaller than 45 nm which concorded well with the particle size values deduced from TEM images. Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>Ho<sub>0.1</sub>O<sub>4</sub> nanoparticles induced a high mortality of breast and prostate cancer cells (MDA-MB-231, T-47D, and PC3) while the Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>Sm<sub>0.1</sub>O<sub>4</sub> compound (higher particle size) reduced almost 35% of MDA-MB-231 cancer cells. With very low cytotoxicity against normal human cells, the Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>Ho<sub>0.1</sub>O<sub>4</sub> nanoparticles play a significant role in the elimination of cancer cells.
format Article
id doaj-art-994f4ec602c64210bb8b77996591ff7d
institution Kabale University
issn 2073-4352
language English
publishDate 2025-05-01
publisher MDPI AG
record_format Article
series Crystals
spelling doaj-art-994f4ec602c64210bb8b77996591ff7d2025-08-20T03:47:49ZengMDPI AGCrystals2073-43522025-05-0115548210.3390/cryst15050482Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological ApproachLiza Saher0Adel Benali1Saoussen Haddad2Essebti Dhahri3Manuel P. F. Graça4Benilde F. O. Costa5Luisa A. Helguero6Artur M. S. Silva7LAQV-REQUIMTE, Department of Chemistry, University of Aveiro, 3810-193 Aveiro, PortugalI3N, Physics Department, Campus de Santiago, University of Aveiro, 3810-193 Aveiro, PortugalDepartment of Chemistry, Faculty of Science, Northern Border University, Arar 91431, Saudi ArabiaLaboratoire de Physique Appliquée, Faculté des Sciences, Université de Sfax, B.P. 1171, Sfax 3000, TunisiaI3N, Physics Department, Campus de Santiago, University of Aveiro, 3810-193 Aveiro, PortugalUniversity of Coimbra, CFisUC, Physics Department, 3400-516 Coimbra, PortugalInstitute of Biomedicine (iBiMED), Department of Medical Sciences, University of Aveiro, 3810-193 Aveiro, PortugalInstitute of Biomedicine (iBiMED), Department of Medical Sciences, University of Aveiro, 3810-193 Aveiro, PortugalIn this work, we synthesized the Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>3+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) nanoparticles via the auto-combustion method. The cell viability against two breast cancer cells (MDA-MB-231 and T-47D cells) and the PC3 prostate cancer cells were carefully analyzed and correlated with the structural parameters and particle size values as well as the chemical composition. The produced compounds’ morphological and structural characteristics were performed using scanning transmission microscopy (TEM) and X-ray Diffraction (XRD). For all compounds, the analyses of the XRD experimental data revealed a structurally reversed cubic spinel with space group Fd-3m. All of the compounds had crystallites smaller than 45 nm which concorded well with the particle size values deduced from TEM images. Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>Ho<sub>0.1</sub>O<sub>4</sub> nanoparticles induced a high mortality of breast and prostate cancer cells (MDA-MB-231, T-47D, and PC3) while the Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>Sm<sub>0.1</sub>O<sub>4</sub> compound (higher particle size) reduced almost 35% of MDA-MB-231 cancer cells. With very low cytotoxicity against normal human cells, the Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>Ho<sub>0.1</sub>O<sub>4</sub> nanoparticles play a significant role in the elimination of cancer cells.https://www.mdpi.com/2073-4352/15/5/482auto-combustionspinel ferritenanoparticlesbreast and prostate cancer cells
spellingShingle Liza Saher
Adel Benali
Saoussen Haddad
Essebti Dhahri
Manuel P. F. Graça
Benilde F. O. Costa
Luisa A. Helguero
Artur M. S. Silva
Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological Approach
Crystals
auto-combustion
spinel ferrite
nanoparticles
breast and prostate cancer cells
title Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological Approach
title_full Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological Approach
title_fullStr Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological Approach
title_full_unstemmed Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological Approach
title_short Co<sub>0.85</sub>Bi<sub>0.15</sub>Fe<sub>1.9</sub>X<sub>0.1</sub>O<sub>4</sub> (X = Ce<sup>4+</sup>, Sm<sup>3+</sup>, Ho<sup>3+</sup>, and Er<sup>3+</sup>) Nanoparticles with Selective Anticancer Activity: A Structural and Morphological Approach
title_sort co sub 0 85 sub bi sub 0 15 sub fe sub 1 9 sub x sub 0 1 sub o sub 4 sub x ce sup 4 sup sm sup 3 sup ho sup 3 sup and er sup 3 sup nanoparticles with selective anticancer activity a structural and morphological approach
topic auto-combustion
spinel ferrite
nanoparticles
breast and prostate cancer cells
url https://www.mdpi.com/2073-4352/15/5/482
work_keys_str_mv AT lizasaher cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach
AT adelbenali cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach
AT saoussenhaddad cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach
AT essebtidhahri cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach
AT manuelpfgraca cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach
AT benildefocosta cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach
AT luisaahelguero cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach
AT arturmssilva cosub085subbisub015subfesub19subxsub01subosub4subxcesup4supsmsup3suphosup3supandersup3supnanoparticleswithselectiveanticanceractivityastructuralandmorphologicalapproach